• 제목/요약/키워드: diffusion treatment

검색결과 789건 처리시간 0.021초

THE FABRICATION OF A PROCESS HEAT EXCHANGER FOR A SO3 DECOMPOSER USING SURFACE-MODIFIED HASTELLOY X MATERIALS

  • Park, Jae-Won;Kim, Hyung-Jin;Kim, Yong-Wan
    • Nuclear Engineering and Technology
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    • 제40권3호
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    • pp.233-238
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    • 2008
  • This study investigates the surface modification of a Hastelloy X plate and diffusion bonding in the assembly of surface modified plates. These types of plates are involved in the key processes in the fabrication of a process heat exchanger (PHE) for a $SO_3$ decomposer. Strong adhesion of a SiC film deposited onto Hastelloy X can be achieved by a thin SiC film deposition and a subsequent N ion beam bombardment followed by an additional deposition of a thicker film that prevents the Hastelloy X surface from becoming exposed to a corrosive environment through the pores. This process not only produces higher corrosion resistance as proved by electrolytic etching but also exhibits higher endurance against thermal stress above 9$900^{\circ}C$. A process for a good bonding between Hastelloy X sheets, which is essential for a good heat exchanger, was developed by diffusion bonding. The diffusion bonding was done by mechanically clamping the sheets under a heat treatment at $900^{\circ}C$. When the clamping jig consisted of materials with a thermal expansion coefficient that was equal to or less than that of the Hastelloy X, sound bonding was achieved.

Mg-Zn-RE/Al1050 클래드재의 제조 및 기계적 특성 (Fabrication and Mechanical Characterization of the Mg-Zn-RE/Al1050 Clad Sheet)

  • 신범수;윤석연;하창성;윤승관;배동현
    • 대한금속재료학회지
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    • 제48권2호
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    • pp.116-121
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    • 2010
  • The Mg-Zn-RE alloy cladded with the thin Al1050 sheet was fabricated by means of a roll bonding process at $280^{\circ}C$.Microstructures and mechanical properties of the clad sheets were investigated. After heat treatment at $230^{\circ}C$ for 30 min, an Mg-rich diffusion layer with about $2{\mu}m$ in thickness was developed at the Mg and Al interface. Tensile tests were carried out in a temperature range up to $300^{\circ}C$. The clad sheet exhibits superior elongation to failure not only at room temperature but also at elevated temperatures compared with those of the Mg alloy sheet. For the deformed specimens, interface debonding does not occur and the diffusion layer shows only a few cracks.

Purification of Therapeutic Serums of Snake Anti-Venom with Caprylic Acid

  • Norouznejad, Nilofar;Zolfagharian, Hossein;Babaie, Mahdi;Ghobeh, Maryam
    • 대한약침학회지
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    • 제25권2호
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    • pp.114-120
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    • 2022
  • Objectives: Antivenom serums have been used extensively for over a century and are the only effective treatment option for snake bites and other dangerous animal envenomations. In therapeutic serum centers, a wide range of antivenoms is made from animal serum, mainly equine and sheep, that are immunized with single or multiple venoms. This work aimed to use caprylic acid (CA) to purify therapeutic snake antivenom. Methods: Plasma was obtained from equine immunized with a mixture of venoms. Immunized plasma was obtained by precipitation of different concentrations (2-5%) of CA. This methodology was compared to that based on ammonium sulfate (AS) precipitation. Sediment plasma proteins were purified by ion-exchange chromatography. Protein assay, SDSPAGE, and agar gel diffusion were performed. Results: The total protein precipitation with AS was higher than precipitation with CA, but the best results were obtained when CA was added to the plasma until a final CA concentration of 5% was reached. Chromatography and electrophoresis indicated a stronger band for the 5% CA, and the gel diffusion assay showed antigen-antibody interaction in the purified serum. Conclusion: The use of CA compared to the routine method for purifying hyperimmune serums is a practical and cost-effective method for preparing and producing therapeutic serums. It constitutes a potentially valuable technology for alleviating the critical shortage of antivenom in Iran.

[ $Sm_2Fe_{17}$ ] Prepared by Calciothermic Reduction-Diffusion Using Different Iron Powders

  • Boareto, J.C.;Soyama, J.;Felisberto, M.D.V.;Hesse, R.;Pinto, A.V.A.;Taylor, T.R.;Wendhausen, P.A.P.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1187-1188
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    • 2006
  • This paper compares the effect of using different types of iron powders for the preparation of $Sm_2Fe_{17}$ by calciothermic reduction-diffusion (CRD). Three types of iron powder were used: carbonyl, sponge and water atomized. The results show that, when immediately nitrogenated after the CRD process, $Sm_2Fe_{17}$ prepared from sponge and water atomized iron powders yield $Sm_2Fe_{17}N_3$-magnets with a high degree of texture. However, after a suitable treatment with hydrogen followed by nitrogenation, $Sm_2Fe_{17}$-powders made from Carbonyl iron produce magnets with the best quality regarding coercivity, remanence and degree of texture.

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생활배수처리시설의 정비와 금후의 방향 (Estabilishment of Community plant)

  • 김경호
    • 환경위생공학
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    • 제6권1호
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    • pp.27-30
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    • 1991
  • Since the diffusion rate of sewage treatment plant is about 30% of the country. It is not enough to cope with entire sewage treatment of the community. Therefore, the septic tank is introduced which is connected with water flush toilet only. It is estimated that the large portion of water pollution has occured due to untreated sewage such as pollutants of kitchen, laundry and bathtub water, etc., which are not go through the existing septic tank. However, the construction of community plant which is could treat most of household run sewage should have flexibility in type, treatment method, effectiveness and economy which are adoption of the community. Without the treatment of combined household run sewage, the improvement of water pollution will be hardly expected.

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차량용 헬리컬기어의 침탄 열처리 변형해석 (Analysis of Deformation of Automotive Helical Gear in Heat Treatment of Carburized Quenching)

  • 배강열;양영수;박병옥
    • 한국정밀공학회지
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    • 제27권11호
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    • pp.84-91
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    • 2010
  • Heat treatment with carburized quenching process is widely used for automotive helical gear to improve its surface properties of hardness and strength. However, the gear can be deformed with the process over the allowable tolerance, which possibly makes noise, vibration and heat problems in operation. In this study, deformation of helical gear during heat treatment of carburized quenching was analyzed with a numerical method, incorporating coupled calculations of thermal conduction, carbon diffusion, phase transformation and thermal stresses. With the analysis, the effect of coolant temperature in quenching on the deformation was investigated. The result of the analysis revealed that the higher the coolant temperature became, the more change of helix angle and the more compressive stresses in the surface generated, because of delayed generation of martensite in the part.

회소강의 기계적 성질을 개선하기 위한 이온질화 처리의 응용에 관한 연구 (Study on the Application of Ion-nitrided Treatment to Improve the Mechanical Properties of Carbon Steel)

  • 강명순;윤종학;이원평
    • 오토저널
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    • 제9권2호
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    • pp.28-33
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    • 1987
  • This thesis is to improve the mechanical properties of carbon steel by the ion-nitriding, and post-heat treatment. The structures of ion-nitrided SM45C steel were changed to martensite by quenching from 730.deg. C and 800.deg. C. And then a few of the quenched specimens was tempered at 200.deg. C for 120 min. The emphasis in this study is focussed on Comparison of hardness and fatigue strength with the ion-nitrided steel. The results obtained are summerized as follows. 1. To improve the hardness and fatigue strength of ion-nitrided steels, it is effective to under take diffusion treatment for a short time at the austenite temperature(800.deg. C). 2. If ion-nitrided steel is heated for a long time at high temperature, de-nitriding occure. 3. The quenching treatment after nitriding on the carbon steel is necessary to improve the mechanical properties of the steels.

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Surgical Outcomes of Thalamic Tumors in Children: The Importance of Diffusion Tensor Imaging, Neuro-Navigation and Intraoperative Neurophysiological Monitoring

  • Kim, Jun-Hoe;Phi, Ji Hoon;Lee, Ji Yeoun;Kim, Kyung Hyun;Park, Sung-Hye;Choi, Young Hun;Cho, Byung-Kyu;Kim, Seung-Ki
    • Brain Tumor Research and Treatment
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    • 제6권2호
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    • pp.60-67
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    • 2018
  • Background Recently, modern technology such as diffusion tensor imaging (DTI), neuro-navigation and intraoperative neurophysiological monitoring (IOM) have been actively adopted for the treatment of thalamic tumors. We evaluated surgical outcomes and efficacy of the aforementioned technologies for the treatment of pediatric thalamic tumors. Methods We retrospectively reviewed clinical data from 37 children with thalamic tumors between 2004 and 2017. There were 44 operations (27 tumor resections, 17 biopsies). DTI was employed in 17 cases, neuro-navigation in 23 cases and IOM in 14 cases. All diagnoses were revised according to the 2016 World Health Organization Classification of Tumors of the Central Nervous System. Progression-free survival (PFS) and overall survival (OS) rates were calculated, and relevant prognostic factors were analyzed. The median follow-up duration was 19 months. Results Fifteen cases were gross total resections (GTR), 6 subtotal resections (STR), and 6 partial resections (PR). Neurological status did not worsen after 22 tumor resections. There were statistically significant differences in terms of the extent of resection between the groups with DTI, neuro-navigation and IOM (n=12, GTR or STR=12) and the group without at least one of the three techniques (n= 15, GTR or STR=9, p=0.020). The mean PFS was $87.2{\pm}38.0$ months, and the mean OS $90.7{\pm}36.1$ months. The 5-year PFS was 37%, and the 5-year OS 47%. The histological grade ($p{\leq}0.001$) and adjuvant therapy (done vs. not done, p=0.016) were significantly related to longer PFS. The histological grade (p=0.002) and the extent of removal (GTR/STR vs. PR/biopsy, p=0.047) were significantly related to longer OS. Conclusion Maximal surgical resection was achieved with acceptable morbidity in children with thalamic tumors by employing DTI, neuro-navigation and IOM. Maximal tumor resection was a relevant clinical factor affecting OS; therefore, it should be considered the initial therapeutic option for pediatric thalamic tumors.

YSZ 전해질과 은 전극을 이용한 저온 산소센서에 대한 연구 (Oxygen sensor for the low temperature-measurement using yttria stabilized zirconia(YSZ) electrolyte and Ag electrode)

  • 양영창;박종욱
    • 센서학회지
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    • 제15권2호
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    • pp.97-101
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    • 2006
  • Silver electrode having a high Electrocatalytic activity is oxygen-permeable electrode, in which oxygen ad-atoms are adsorbed and moved toward YSZ electrolyte by bulk diffusion. It is the different point in comparison to usual porous electrodes, especially platinum, which react with oxygen only in TPBs(Three Phase Boundaries). Also ad-atoms at TPBs of Pt are diffused to YSZ electrolyte by interfacial diffusion mechanism. These properties were used for turning down the operating temperature of YSZ from over $600^{\circ}C$ to below $450^{\circ}C$. The different heat-treatment temperature between a working electrode and a reference electrode suppresses the formation of silver oxides and reduces a volatility of Ag as well. Above all, these own characteristics and special processes of Ag improved a long-term stability of a oxygen sensor.

중앙분공형 보염기 후류에 안정된 난류확산화염의 구조에 관한 연구(I) (A study on the Structure of Turbulent Diffusion Flame Behind the Hollowed Flame Holder)

  • 강인구;이우섭;김태한;이도형
    • 동력기계공학회지
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    • 제2권2호
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    • pp.13-19
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    • 1998
  • The purpose of study is to investigate the flame stability and Structure of turbulent diffusion flame behind the hollowed flame holder, which is located on the waste gas coming out from the test furnace. Fluctuating temperature and ion current measurement and their statistical treatment were used for the purpose. Three types of flame were stabilized and each of which were changed by adequate equivalence ration. And we found that have no periodicity near reacting zone.

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