• Title/Summary/Keyword: densification

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Mechanical Properties and Fabrication of Nanostructured Mg2SiO4-MgAl2O4 Composites by High-Frequency Induction Heated Combustion (기계적 활성화된 분말로부터 고주파유도 가열 연소합성에 의한 나노구조 Mg2SiO4-MgAl2O4 복합재료 제조 및 기계적 특성)

  • Shon, In-Jin;Kang, Hyun-Su;Hong, Kyung-Tae;Doh, Jung-Mann;Yoon, Jin-Kook
    • Korean Journal of Metals and Materials
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    • v.49 no.8
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    • pp.614-618
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    • 2011
  • Nanopowders of MgO, $Al_2O_3$ and $SiO_2$ were made by high energy ball milling. The rapid sintering of nanostructured $MgAl_2O_4-Mg_2SiO_4$ composites was investigated by a high-frequency induction heating sintering process. The advantage of this process is that it allows very quick densification to near theoretical density and inhibition of grain growth. Nanocrystalline materials have received much attention as advanced engineering materials with improved physical and mechanical properties. As nanomaterials possess high strength, high hardness, excellent ductility and toughness, undoubtedly, more attention has been paid for the application of nanomaterials. Highly dense nanostructured $MgAl_2O_4-Mg_2SiO_4$ composites were produced with simultaneous application of 80MPa pressure and induced output current of total power capacity (15 kW) within 2min. The sintering behavior, gain size and mechanical properties of $MgAl_2O_4-Mg_2SiO_4$ composites were investigated.

Rapid Synthesis and Sintering of Nanostructured MgTiO3 Compound by High-Frequency Induction Heating (고주파 유도 가열에 의한 급속 나노구조 MgTiO3 화합물 합성 및 소결)

  • Kang, Hyun-Su;Doh, Jung-Mann;Yoon, Jin-Kook;Park, Bang-Ju;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.50 no.12
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    • pp.891-896
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    • 2012
  • Nanopowders of MgO and $TiO_2$ were made by high energy ball milling. The rapid synthesis and sintering of the nanostructured $MgTiO_3$ compound was investigated by the high-frequency induction heated sintering process. The advantage of this process is that it allows very quick densification to near theoretical density and inhibition grain growth. Nanocrystalline materials have received much attention as advanced engineering materials with improved physical and mechanical properties. As nanomaterials possess high strength, high hardness, excellent ductility and toughness, undoubtedly, more attention has been paid for the application of nanomaterials. A highly dense nanostructured $MgTiO_3$ compound was produced with simultaneous application of 80 MPa pressure and induced current within 2 min. The sintering behavior, gain size and mechanical properties of $MgTiO_3$ compound were investigated.

Mechanical Properties and Consolidation of Ultra-Fine WC-10Co and WC-10Fe Hard Materials by Rapid Sintering Process (급속 소결 공정에 의한 초미립 WC-10Co와 WC-10Fe 초경재료 제조와 기계적 성질)

  • Jeong, In Kyoon;Park, Jung-Hwan;Doh, Jung-Mann;Kim, Ki-Youl;Woo, Kee-Do;Ko, In-Young;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.46 no.4
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    • pp.223-226
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    • 2008
  • The comparison of sintering behavior and mechanical properties of ultra-fine WC-10wt.%Co and WC-10wt.%Fe hard materials produced by high-frequency induction heated sintering (HFIHS) was accomplished using ultra fine powder of WC and binders(Co, Fe). The advantage of this process allows very quick densification to near theoretical density and prohibition of grain growth in nano-structured materials. Highly dense WC-10Co and WC-10Fe with a relative density of up to 99% could be obtained with simultaneous application of 60 MPa pressure and induced current within 1 minute without significant change in grain size. The hardness and fracture toughness of the dense WC-10Co and WC-10Fe composites produced by HFIHS were investigated.

Effect of Tert-Butyl Alcohol Template on the Pore Structure of Porous Tungsten in Freeze Drying Process (동결건조 공정에서 Tert-butyl alcohol 기공형성제가 텅스텐 다공체의 기공구조에 미치는 영향)

  • Lee, Eui Seon;Heo, Youn Ji;Ko, Yun Taek;Park, Jin Gyeong;Cho, Yong-Ho;Oh, Sung-Tag
    • Journal of Powder Materials
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    • v.28 no.3
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    • pp.216-220
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    • 2021
  • The effect of tert-butyl alcohol (TBA) as a freezing solvent on the pore structure of a porous tungsten body prepared by freeze-drying is analyzed. TBA slurries with a WO3 content of 10 vol% are prepared by mixing with a small amount of dispersant and binder at 30℃. The slurries are frozen at -25℃, and pores are formed in the frozen specimens by the sublimation of TBA during drying in air. After hydrogen reduction at 800℃ and sintering at 1000℃, the green body of WO3 is completely converted to porous W with various pore structures. Directional pores from the center of the specimen to the outside are observed in the sintered bodies because of the columnar growth of TBA. A decrease in pore directionality and porosity is observed in the specimens prepared by long-duration drying and sintering. The change in pore structure is explained by the growth of the freezing solvent and densification.

Experimental Research of Characteristic of Pool Boiling Heat Transfer of Saturated Liquid Nitrogen with Helical Coil Type Heat Exchanger (나선형 튜브 열교환 방식의 포화 상태 액체질소의 비등열전달 특성에 대한 실험적 연구)

  • Seo, Mansu;Lee, Jisung;Kim, Junghan;Kang, Sunil
    • Journal of the Korean Society of Propulsion Engineers
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    • v.24 no.3
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    • pp.59-70
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    • 2020
  • Obtaining external forced convection heat transfer from bubble boiling and validating it with experimental results using cryogenic liquids are suggested to derive total heat transfer coefficient with pool boiling condition in the case of coil type heat exchanger with a bundle of tubes and to overcome the limitation of using the empirical correlation. Experiment is conducted with pool boiling heat transfer of saturate liquid nitrogen with helical coil type heat exchanger using liquid oxygen as hot stream fluid. Experimentally measured heat transfer coefficient is well-agreed with the estimated curve considering nucleate boiling and forced convection induced by bubble rise.

A Study on the Visualization of Urban Wind Flow by Using Thermochromic Pigment (열변색성 염료를 이용한 도심 공기 유동 시각화에 관한 연구)

  • Kim, Hong-Seok
    • Journal of the Korea Convergence Society
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    • v.12 no.11
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    • pp.291-299
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    • 2021
  • Recently, due to environmental problems caused by densification and high rise of urban areas, interests in air flow is increasing and appropriate shape and layout design of buildings is required. Therefore, in this study, we intend to propose an experimental method that can observe the air flow around a building using thermochromic pigment. Thermochromic pigments have limitations in observing precise temperature changes due to the characteristic that the color changes only with respect to a specific temperature, but they have the advantages of easy configuration of experimental equipment and short time required for experiments. In this study, the air flow tendencies around a building was examined by performing CFD analysis for a simple model and then compared with the thermochromic experiment results in order to review the usefulness of the proposed experimental method. As a result of the experiment, it was possible to observe the formation of separated flow and vortex region generated by buildings using the charateristics of thermochromic pigment and it was confirmed that the proposed method can be useful for buildings design and urban city planning.

Sintering Behavior and Mechanical Property of Transition Metal Carbide-Based Cermets by Spark Plasma Sintering (방전플라즈마 소결 공정 적용 전이금속 카바이드 서멧의 소결 및 기계적 특성)

  • Lee, Jeong-Han;Park, Hyun-Kuk;Hong, Sung-Kil
    • Korean Journal of Materials Research
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    • v.32 no.1
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    • pp.44-50
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    • 2022
  • Transition metal carbides (TMCs) are used to process difficult-to-cut materials due to the trend of requiring superior wear and corrosion properties compared to those of cemented carbides used in the cutting industry. In this study, TMC (TiC, TaC, Mo2C, and NbC)-based cermets were consolidated by spark plasma sintering at 1,300 ℃ (60 ℃min) with a pressure of 60 MPa with Co addition. The sintering behavior of TMCs depended exponentially on the function of the sintering exponent. The Mo2C-6Co cermet was fully densified, with a relative density of 100.0 %. The Co-binder penetrated the hard phase (carbides) by dissolving and re-precipitating, which completely densified the material. The mechanical properties of the TMCs were determined according to their grain size and elastic modulus: TiC-6Co showed the highest hardness of 1,872.9 MPa, while NbC-6Co showed the highest fracture toughness of 10.6 MPa*m1/2. The strengthened grain boundaries due to high interfacial energy could cause a high elastic modules; therefore, TiC-6Co showed a value of 452 ± 12 GPa.

Effects of Powder Property and Sintering Atmosphere on the Properties of Burnable Absorber Fuel : I. $UO_2-Gd_2O_3$ Fuel

  • K. W. Song;Kim, K. S.;H. S. Yoo;Kim, J. H.
    • Proceedings of the Korean Nuclear Society Conference
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    • 1997.05b
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    • pp.171-176
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    • 1997
  • UO$_2$-Gd$_2$O$_3$fuel has been sintered to study the effect of powder property and sintering atmospheres on densification and microstructure. Three types of powders have been used; AUC-UO$_2$ powder and ADU-UO$_2$ powder were mixed with Gd$_2$O$_3$ Powder, and co-milled AUC-UO$_2$ and Gd$_2$O$_3$ powder. UO$_2$-(2, 5, 10)wt% Gd$_2$O$_3$pellets have been sintered at 168$0^{\circ}C$ for 4 hours in the mixture of H$_2$ and $CO_2$ gases, of which oxygen potential has been controlled by the ratio of $CO_2$ to H$_2$ gas. Densities of UO$_2$-Gd$_2$O$_3$ fuel pellets are quite dependent on powder types, and UO$_2$-Gd$_2$O$_3$ fuel using co-milled UO$_2$ powder yields the highest density. A long range homogeneity of Gd is determined by powder mixing. As the oxygen potential of sintered atmosphere increases, the sintered densities of UO$_2$-Gd$_2$O$_3$ pellets decrease but grain size increases. In addition, (U, Gd)O$_2$ solid solution becomes more homogeneous. The UO$_2$-Gd$_2$O$_3$fuel having adequate density and homogeneous microstructure can be fabricated by co-milling powder and by high oxygen potential.

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Continuous W-Cu functional gradient material from pure W to W-Cu layer prepared by a modified sedimentation method

  • Bangzheng Wei;Rui Zhou;Dang Xu;Ruizhi Chen;Xinxi Yu;Pengqi Chen;Jigui Cheng
    • Nuclear Engineering and Technology
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    • v.54 no.12
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    • pp.4491-4498
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    • 2022
  • The thermal stress between W plasma-facing material (PFM) and Cu heat sink in fusion reactors can be significantly reduced by using a W-Cu functionally graded material (W-Cu FGM) interlayer. However, there is still considerable stress at the joining interface between W and W-Cu FGM in the W/W-Cu FGM/Cu portions. In this work, we fabricate W skeletons with continuous gradients in porosity by a modified sedimentation method. Sintering densification behavior and pore characteristics of the sedimented W skeletons at different sintering temperatures were investigated. After Cu infiltration, the final W-Cu FGM was obtained. The results indicate that the pore size and porosity in the W skeleton decrease gradually with the increase of sintering temperature, but the increase of skeleton sintering temperature does not reduce the gradient range of composition distribution of the final prepared W-Cu FGM. And W-Cu FGM with composition distribution from pure W to W-20.5wt.% Cu layer across the section was successfully obtained. The thickness of the pure W layer is about one-fifth of the whole sample thickness. In addition, the prepared W-Cu FGM has a relative density of 94.5 % and thermal conductivity of 185 W/(m·K). The W-Cu FGM prepared in this work may provide a good solution to alleviate the thermal stress between W PFM and Cu heat sink in the fusion reactors.

Analyzing the Spatial Transformation of Johannesburg: Background, Process and Effectiveness (约翰内斯堡空间转型的背景, 进程与效果研究)

  • Tang, Wei
    • Analyses & Alternatives
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    • v.2 no.2
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    • pp.93-110
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    • 2018
  • Due to its speciality, Johannesburg has drawn wide attention from the international academia, which the existing urban theory cannot easily explain. This paper focuses on the spatial pattern of Johannesburg, and finds that it is highly fragmented: first North-South Division due to apartheid and gold mining, secondly, the continuous sprawl due to population densification, and thirdly formation of city-region due to the fill-in spatial policy. The fragmented spatial pattern undermines the social integration and weakens the potential economic sustainability, which make the balanced multi-core spatial pattern inevitable under the influence of the international planning thought. The Johannesburg's spatial transformation comes not only from social integration, but also from the development vison of world-class status of an African city. In reality, since the collapse of apartheid, the municipal government has released series of strategic planning in different executive phase. These different plannings unanimously focus on the world class status although since 2008, the social inclusiveness is more emphasized. Thus, Johannesburg implements some spatial policies, as promoting the corridor of freedom, identifying the key nodes in the city then developing with high density, implementing the in-filling policy, managing the urban growth boundary, effectively preserving the natural system. However, the industrial structure in Johannesburg is already quite high-ended which cannot produce many jobs and also require much investment in advanced infrastructure. Thus, the strategic goals of world-class status of an African city and social inclusiveness which really need widely shared public services to some extent are in tension. After evaluation, we can see that spatial transformation is quite limited. Obviously spatial transformation largely depends on the social-economy. The population is still in flow. In this sense Johannesburg must energetically support the employment-based industry, effectively control the spatial sprawl and carry out institutional innovation which further incentive investment, gradually build an integrated regional governance. In general, how Johannesburg combines globalization and its own condition is still worth thinking in both theory and practice.

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