• Title/Summary/Keyword: dense morphology

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Sperm Ultrastructure of Pipistrellus savii velox (한국산 검은큰집박쥐(Pipistrellus savii velox)의 정자미세구조)

  • Lee, Yu-Ri;Lee, Jung-Hun
    • Applied Microscopy
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    • v.41 no.2
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    • pp.117-122
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    • 2011
  • Sperm morphology of Pipistrellus savii velox was examined by transmission electron microscope. The sperm head of P. savii velox was bullet in shape. The sperm head was 3.1 ${\mu}m$ in length, whose posterior 3.0 ${\mu}m$ was occupied by a nucleus with 1.8 ${\mu}m$ in width. The segmented columns were about 14~15 in number. The total number of mitochondrial gyres was 57. Number of 1, 5, and 6 of the outer dense fibers were larger than the others. A fibrous sheath and longitudinal column of the principal piece were evidence, but the fibrous sheath was not seen at the end piece. In the present study, the length of the sperm head of P. savii velox were very shorter than those of other bats.

Preparation and Characterization of PSF Membranes by Phosphoric Acid and 2-Butoxyethanol (인산 및 2-부톡시에탄올 첨가에 의한 PSF 고분자 분리막의 제조 및 특성)

  • Kim, Nowon
    • Membrane Journal
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    • v.22 no.3
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    • pp.178-190
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    • 2012
  • Flat sheet membranes were prepared with polysulfone (PSF) by an immersion precipitation phase inversion method. Membranes were prepared with PSF/N-methylpyrrolidone (NMP)/polyvinylpyrrolidone (PVP)/phosphoric acid casting solution and water coagulant. By using the successive process of the vapor-induced phase inversion (VIPS) followed by the nonsolvent-induced phase inversion (NIPS), the effect of phosphoric acid addition to casting solution on morphology and permeability of membrane was studied. The mean pore size, the porosity, and the water flux of membranes were increased by the addition of small amount of phosphoric acid. Furthermore, the morphology of the prepared membranes were changed from a dense sponge-like structure to highly enhanced asymmetric structure. PSF/NMP/PVP/phosphoric acid/2-butoxyethanol (BE) casting solution were prepared and cast the successive VIPS-NIPS process with same experimental condition. Due to the addition of BE to casting solution, the mean pore size and almost 0.1 ${\mu}m$ and the water flux increased about 10 to 12 $L/cm^2{\cdot}min{\cdot}bar$.

Comparison of Pre-Stain Suspension Liquids in the Contrasting Ability of Neutralized Potassium Phosphotungstate for Negative Staining of Bacteria

  • Kim, Ki-Wooh;Jung, Woo-Kyung;Park, Yong-Ho
    • Journal of Microbiology and Biotechnology
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    • v.18 no.11
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    • pp.1762-1767
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    • 2008
  • Image contrast of whole bacteria was compared in Staphylococcus aureus and Escherichia coli depending on pre-stain suspension liquids by energy-filtering transmission electron microscopy. The two bacterial strains were suspended in three most commonly used liquids for negative staining (triple distilled water [DW], phosphate-buffered saline [PBS], and nutrient broth [NB]) and directly observed without staining or stained with neutralized potassium phosphotungstate (PTA), respectively. Even though in low contrast, unstained bacteria were observed owing to their inherent electron density and cell shape in zero-loss (elastic scattering) images. After being suspended in PBS, unstained bacteria appeared to have higher contrast and more refined periphery than DW-suspended ones, and extracellular appendage structures such as fimbriae and flagella could be discerned. The unstained bacteria appeared to be invariably surrounded with electron-lucent precipitates, possibly from PBS. As far as delineation of the structures, the combination of DW or PBS suspension with subsequent staining provided the most satisfactory results, as evidenced by the high contrast of bacterial morphology and appendage structures. However, after being suspended in NB and stained with PTA, bacteria often had too high contrast or poor staining, with electron-dense aggregates around the bacteria. These results suggest that suspension with concentrated organic aliquots including broth media before PTA staining could deteriorate image contrast, and should be used only in dilute form for visualizing bacterial morphology and appendage structures. Moreover the contrast enhancement of unstained bacteria by salt granules would be advantageous in demonstrating bacterial sorption of environmental particles like heavy metals, maintaining minimal contrast for cell imaging.

Effect of Reaction Conditions on the Particle Properties for Synthesis of Stabilized Zirconia by Modified Oxalate Method

  • Park, Hyun-wook;Lee, Young Jin;Kim, Jin-Ho;Jeon, Dae-Woo;Hwang, Hae Jin;Lee, Mi Jai
    • Journal of the Korean Ceramic Society
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    • v.53 no.5
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    • pp.529-534
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    • 2016
  • Nanocrystalline powder of zirconia stabilized with 8 mol% yttria (YSZ) has been synthesized through oxalate process using $ZrOCl_2{\cdot}8H_2O$ and $Y(NO_3)_3{\cdot}6H_2O$ as starting materials. Understanding of the characteristic changes of YSZ powder as a function of processing conditions is crucial in developing dense and porous microstructures required for fuel cell applications. In this research, microstructure change, surface area, particle shape and particle size were measured as a function of different processing conditions such as calcination temperature, stirring speed and concentration of starting materials. The resultant crystallite sizes were calculated by XRD-LB (X-Ray Diffraction Line-Broadening) method, BET method, and morphology of the crystal was observed in TEM and FE-SEM. The TEM examination showed that the powder synthesized with 0.7 M of YSZ concentration had a spherical morphology with sizes ranging from 20 to 40 nm. However, the powder was gradually aggregated above 1.0 M of YSZ concentration with the aggregation being intensified as the YSZ concentration was increased.

Composition Control of a Light Absorbing Layer of CuInSe2 Thin Film Solar Cells Prepared by Electrodeposition (전착법을 이용한 CuInSe2 박막태양전지 광활성층의 조성 조절)

  • Park, Young-Il;Kim, Donghwan;Seo, Kyungwon;Jeong, Jeung-Hyun;Kim, Honggon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.3
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    • pp.232-239
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    • 2013
  • Thin light-active layers of the $CuInSe_2$ solar cell were prepared on Mo-coated sodalime glass substrates by one-step electrodeposition and post-annealing. The structure, morphology, and composition of $CuInSe_2$ film could be controlled by deposition parameters, such as the composition of metallic precursors, the concentration of complexing agents, and the temperature of post-annealing with elemental selenium. A dense and uniform Cu-poor $CuInSe_2$ film was successfully obtained in a range of parametric variation of electrodeposition with a constant voltage of -0.5 V vs. a Ag/AgCl reference electrode. The post-annealing of the film at high temperature above $500^{\circ}C$ induced crystallization of $CuInSe_2$ with well-developed grains. The KCN-treatment of the annealed $CuInSe_2$ films further induced Cu-poor $CuInSe_2$ films without secondary phases, such as $Cu_2Se$. The structure, morphology, and composition of $CuInSe_2$ films were compared with respect to the conditions of electrodeposition and post-annealing using SEM, XRD, Raman, AES and EDS analysis. And the conditions for preparing device-quality $CuInSe_2$ films by electrodeposition were proposed.

Taxonomic study on the achene morphology of Korean Aster L. and its allied taxa (한국산 개미취속 및 근연 분류군의 열매 형태에 관한 분류학적 연구)

  • 정규영;정형진
    • Korean Journal of Plant Resources
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    • v.13 no.3
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    • pp.179-187
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    • 2000
  • The achene morphology about 16 taxa of Korean Aster L. sensu lato were investigated to estimate its taxonomic values. The achene shapes were divided into four types; oblanceolate-oblong, obovate, oblong and obovate-oblong. The trichome shape on achene six types; uniseriate-conical, filiform, cylindrical, capitate type, long stalk capitate and globular. Their distributional features on upper part of achene four types; absent, sparse distribution of conical trichome, dense distribution of conical trichome and mixed distribution of conical and capitate trichome. The achene shapes and trichome characteristics were regarded to be a good characters in delimiting taxa because these did not differ among individuals in same taxa, but differ among the taxa. If Korean Aster L. sensu late were divided into Kalimeris, Heteropappus, Aster, Cymnaster, the capitate forms and mixed distribution of conical and capitate trichome were recognized as the good characters in delimting above section such as genus Kalimeris and Heteropappus, section Pseudocalimeris of Aster L. sensu stricto.

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A Comparative Study of Nanocrystalline TiAlN Coatings Fabricated by Direct Current and Inductively Coupled Plasma Assisted Magnetron Sputtering (DC 스퍼터법과 유도결합 플라즈마를 이용한 마그네트론 스퍼터링으로 제작된 나노결정질 TiAlN 코팅막의 물성 비교 연구)

  • Chun, Sung-Yong;Kim, Se-Chul
    • Journal of the Korean Ceramic Society
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    • v.51 no.5
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    • pp.375-379
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    • 2014
  • Nanocrystalline TiAlN coatings were prepared by reactively sputtering TiAl metal target with $N_2$ gas. This was done using a magnetron sputtering system operated in DC and ICP (inductively coupled plasma) conditions at various power levels. The effect of ICP power (from 0 to 300 W) on the coating microstructure, corrosion and mechanical properties were systematically investigated using FE-SEM, AFM and nanoindentation. The results show that ICP power has a significant influence on coating microstructure and mechanical properties of TiAlN coatings. With increasing ICP power, the coating microstructure evolved from the columnar structure typical of DC sputtering processes to a highly dense one. Average grain size of TiAlN coatings decreased from 15.6 to 5.9 nm with increasing ICP power. The maximum nano-hardness (67.9 GPa) was obtained for the coatings deposited at 300 W of ICP power. The smoothest surface morphology (Ra roughness 5.1 nm) was obtained for the TiAlN coating sputtered at 300 W ICP power.

The temperature and density distribution of molecular gas in a galaxy undergoing strong ram pressure: a case study of NGC 4402

  • Lee, Bumhyun;Chung, Aeree
    • The Bulletin of The Korean Astronomical Society
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    • v.40 no.1
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    • pp.77.2-77.2
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    • 2015
  • Galaxies are known to evolve passively in the cluster environment. Indeed, much evidence for HI stripping has been found in cluster galaxies to date, which is likely to be connected to their low star formation rate. What is still puzzling however, is that the molecular gas, which is believed to be more directly related to star formation, shows no significant difference in its fraction between the cluster population and the field galaxies. Therefore, HI stripping alone does not seem to be enough to fully understand how galaxies become passive in galaxy clusters. Intriguingly, our recent high resolution CO study of a subsample of Virgo spirals which are undergoing strong ICM pressure has revealed a highly disturbed molecular gas morphology and kinematics. The morphological and kinematical peculiarities in their CO data have many properties in common with those of HI gas in the sample, indicating that strong ICM pressure in fact can have impacts on dense gas deep inside of a galaxy. This implies that it is the molecular gas conditions rather than the molecular gas stripping which is more responsible for quenching of star formation in cluster galaxies. In this study, using multi transitions of 12CO and 13CO, we investigate the density and temperature distributions of CO gas of a Virgo spiral galaxy, NGC 4402 to probe the physical and chemical properties of molecular gas and their relations to star formation activities.

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Recycling Method of Used Indium Tin Oxide Targets (폐 인듐주석산화물 타겟의 재활용 기술)

  • Lee, Young-In;Choa, Yong-Ho
    • Korean Journal of Materials Research
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    • v.22 no.4
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    • pp.174-179
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    • 2012
  • In this study, we demonstrated a simple and eco-friendly method, including mechanical polishing and attrition milling processes, to recycle sputtered indium tin oxide targets to indium tin oxide nanopowders and targets for sputtered transparent conductive films. The utilized indium tin oxide target was first pulverized to a powder of sub- to a few- micrometer size by polishing using a diamond particle coated polishing wheel. The calcination of the crushed indium tin oxide powder was carried out at $1000^{\circ}C$ for 1 h, based on the thermal behavior of the indium tin oxide powder; then, the powders were downsized to nanometer size by attrition milling. The average particle size of the indium tin oxide nanopowder was decreased by increasing attrition milling time and was approximately 30 nm after attrition milling for 15 h. The morphology, chemical composition, and microstructure of the recycled indium tin oxide nanopowder were investigated by FE-SEM, EDX, and TEM. A fully dense indium tin oxide sintered specimen with 97.4% of relative density was fabricated using the recycled indium tin oxide nanopowders under atmospheric pressure at $1500^{\circ}C$ for 4 h. The microstructure, phase, and purity of the indium tin oxide target were examined by FE-SEM, XRD, and ICP-MS.

C2H5OH Sensor Using Porous Cr2O3 Nano-Hexaprisms (다공성 Cr2O3 나노육각기둥을 이용한 C2H5OH 센서)

  • Jeong, Hyun-Mook;Lee, Jong-Heun
    • Journal of Sensor Science and Technology
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    • v.21 no.6
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    • pp.451-455
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    • 2012
  • Dense Cr-precursor nano-hexaprisms were prepared by heating the Cr-nitrate aqueous solution containing Hexamethylenetetramine and polyvinylpyrrolidone, which were converted into porous $Cr_2O_3$ nano-hexaprisms containing nanoparticles by heat treatment of Cr-precursors at $600^{\circ}C$ for 2 h in air atmosphere. At the sensor temperature of $300^{\circ}C$, porous $Cr_2O_3$ nano-hexaprism showed the high response ($R_g/R_a$, $R_g$: resistance in gas, $R_a$: resistance in air) to 100 ppm $C_2H_5OH$ ($R_g/R_a=69.8$) with negligible cross-responses to 100 ppm CO and 5 ppm $C_6H_6$. The sensitive and selective detection of $C_2H_5OH$ in porous $Cr_2O_3$ nano-hexaprism were discussed in relation to the morphology of nanostructures.