• Title/Summary/Keyword: dense morphology

Search Result 256, Processing Time 0.025 seconds

Properties of VN Coatings Deposited by ICP Assisted Sputtering: Effect of ICP Power

  • Chun, Sung-Yong
    • Journal of the Korean Ceramic Society
    • /
    • v.54 no.1
    • /
    • pp.38-42
    • /
    • 2017
  • Vanadium nitride (VN) coatings were deposited using inductively coupled plasma (ICP) assisted sputtering at different ICP powers. Microstructural, crystallographic and mechanical characterizations were performed by FE-SEM, AFM, XRD and nanoindentation. The results show that ICP has significant effects on coating's microstructure, structural and mechanical properties of VN coatings. With an increase in ICP power, coating microstructure evolved from a porous columnar structure to a highly dense one. Single- phase cubic (FCC) VN coatings with different preferential orientations and residual stresses were obtained as a function of ICP power. Average crystal grain sizes of single phase cubic (FCC) VN coatings were decreased from 10.1 nm to 4.0 nm with an increase in ICP power. The maximum hardness of 28.2 GPa was obtained for the coatings deposited at ICP power of 200 W. The smoothest surface morphology with Ra roughness of 1.7 nm was obtained in the VN coating sputtered at ICP power of 200 W.

Anti-reflection Coating of Silicon Nitride Film for Solar Cell by RF Magnetron Sputtering (RF 마그네트론 스퍼터링을 이용한 태양전지용 질화 실리콘 반사방지막)

  • Choi, Kyoon;Choi, Eui-Seok;Hwang, Jin-Ha;Lee, Soo-Hong
    • Journal of the Korean Ceramic Society
    • /
    • v.44 no.10
    • /
    • pp.585-588
    • /
    • 2007
  • Silicon nitride films for an anti-reflection coating were deposited on silicon via RF magnetron sputtering using a $Si_3N4$ target. The best result was obtained at the sputtering condition of 340 W RF power, 5 mtorr Ar atmosphere, $100^{\circ}C$ substrate temperature. The films showed 7.9% reflectance minimum with 2.35 refractive index. 0.21 absorption coefficient at 66.6 nm thickness. The surface morphology showed a smooth and dense film with good adhesion to silicon surface.

SiO IN THE SGR B2 REGION

  • Minh, Y.C.
    • Journal of The Korean Astronomical Society
    • /
    • v.40 no.3
    • /
    • pp.61-65
    • /
    • 2007
  • The 2-1 and 5-4 transitions of SiO have been observed toward the Sgr B2 region, including the Principal Cloud(the GMC containing Sgr B2(M)) and its surroundings. The morphology and velocity structure of the SiO emission show a close resemblance with the HNCO Ring feature, identified by Minh & Irvine(2006), of about 10 pc in diameter, which may be expanding and colliding with the Principal Cloud. Three SiO clumps have been found around the Ring, with total column densities $N_{SiO}{\sim}1{\times}10^{14}cm^{-2}$ at the peak positions of these clumps. The fractional SiO abundance relative to $H_2$ has been estimated to be ${\sim}(0.5-1){\times}10^{-9}$, which is about two orders of magnitude larger than the quiet dense cloud values. Our SiO observational result supports the existence of an expanding ring, which may be triggering active star formations in the Principal Cloud.

Roles for the lipid-signaling enzyme MitoPLD in mitochondrial dynamics, piRNA biogenesis, and spermatogenesis

  • Gao, Qun;Frohman, Michael A.
    • BMB Reports
    • /
    • v.45 no.1
    • /
    • pp.7-13
    • /
    • 2012
  • Phospholipase D (PLD), a superfamily of signaling enzymes that most commonly generate the lipid second messenger Phosphatidic Acid (PA), is found in diverse organisms from bacteria to man and functions in multiple cellular pathways. A fascinating member of the family, MitoPLD, is anchored to the mitochondrial surface and has two reported roles. In the first role, MitoPLD-generated PA regulates mitochondrial shape through facilitating mitochondrial fusion. In the second role, MitoPLD performs a critical function in a pathway that creates a specialized form of RNAi required by developing spermatocytes to suppress transposon mobilization during meiosis. This spermatocyte-specific RNAi, known as piRNA, is generated in the nuage, an electron-dense accumulation of RNA templates and processing proteins that localize adjacent to mitochondria in a structure also called intermitochondrial cement. In this review, we summarize recent findings on these roles for MitoPLD functions, highlighting directions that need to be pursued to define the underlying mechanisms.

Young Stellar Objects and Dense Clouds in the W51 Region

  • Kang, Mi-Ju;Bieging, John H.;Kulesa, Craig A.;Lee, Yong-Ung;Choi, Min-Ho;Peters, William L.
    • The Bulletin of The Korean Astronomical Society
    • /
    • v.35 no.2
    • /
    • pp.72.1-72.1
    • /
    • 2010
  • We present infrared and millimeter observations of the active star-forming complex W51. A $1.25\;deg\times1.00\;deg$ region that includes the W51 complex was covered in the J = 2 - 1 transition of the $^{12}CO$ and $^{13}CO$ molecules with the University of Arizona Heinrich Hertz Submillimeter Telescope. We use a statistical equilibrium code to estimate physical properties of the molecular gas. Using Spitzer data we identify young stellar objects (YSOs) and fit model spectral energy distributions to these sources and constrain their physical properties. We compare the molecular cloud morphology with the distribution of infrared and radio continuum sources and find associations between molecular clouds and YSOs. We estimate that about 1% of the cloud mass is currently in YSOs.

  • PDF

Preparation of Titanium Carbide Fiber-Reinforced Alumina Ceramic Matrix Composites by Self-Propagating High-Temperature Synthesis

  • Yun, Jondo;Bang, Hwancheol
    • The Korean Journal of Ceramics
    • /
    • v.4 no.3
    • /
    • pp.171-175
    • /
    • 1998
  • $Al_2O_3$-TiC composites were prepared from aluminum, titanium oxide, and carbon fibers by self-propagating high-temperature synthesis(SHS). After the SHS reaction, the TiC phase in the sample was found either fibrous or non-fibrous shape. The fraction of the fibrous TiC phase varied with the amount of $Al_2O_3$ diluent addition. The optimum amount of diluent to make fibrous carbide was determined to be 30%. The fibers were hollow inside and made of multiple grains with a composition of titanium carbide. The hollow fiber formation mechanism was suggested and discussed. The synthesized powders were consolidated to dense composites by hot pressing at $1750^{\circ}C$ under 30 MPa.

  • PDF

Preparation of Yttria Stabilized zirconia Films by the Electrochemical Vapor Deposition (전기화학증착에 의한 이트리아 안정화 지르코니아 박막의 제조)

  • 정지원;박동원;전치훈;최병진;김대룡
    • Journal of the Korean Ceramic Society
    • /
    • v.31 no.5
    • /
    • pp.477-484
    • /
    • 1994
  • The yttria stabilized zirconia(YSZ) thin films for solid oxide fuel cell (SOFC) were fabricated by an electrochemical vapor deposition(EVD) technique using YCl3+ZrCl4+H2O gas system. The YSZ films were deposited under reduced pressure at the temperature of 1000~120$0^{\circ}C$ on the porous alumina substrates. The deposition rate, chemical composition and growth morphology were investigated by SEM, XRD, EDS. The growth rates of the films obeyed a parabolic rate law, representing that the growing process is controlled by an electrochemical transport through the YSZ film. The Y2O3 content of the films was about 10 mol%, equal to the composition of metal chloride reactant gases, approximately. The YSZ films were highly dense, the growing features showed columnar structure and surface morphologies were changed with the EVD conditions.

  • PDF

Effect of Inductively Coupled Plasma (ICP) Power on the Properties of Ultra Hard Nanocrystalline TiN Coatings (유도결합 플라즈마 파워변화에 따른 초경도 나노결정질 TiN 코팅막의 물성변화)

  • Chun, Sung-Yong
    • Journal of the Korean Ceramic Society
    • /
    • v.50 no.3
    • /
    • pp.212-217
    • /
    • 2013
  • Ultra hard TiN coatings were fabricated by DC and ICP (inductively coupled plasma) magnetron sputtering techniques. The effects of ICP power, ranging from 0 to 300 W, on the coating microstructure, crystallographic, and mechanical properties were systematically investigated with FE-SEM, AFM, HR-XRD and nanoindentation. The results show that ICP power has a significant influence on the coating microstructure and mechanical properties of TiN coatings. With an increasing ICP power, the film microstructure evolves from an apparent columnar structure to a highly dense one. Grain sizes of TiN coatings decreased from 12.6 nm to 8.7 nm with an increase of the ICP power. A maximum nanohardness of 67.6 GPa was obtained for the coatings deposited at an ICP power of 300 W. The crystal structure and preferred orientation in the TiN coatings also varied with the ICP power, exerting an effective influence on film nanohardness.

Synthesis of spherical phosphors (Y,Gd)$BO_3$:Eu from Precursors in Polymeric Form by Aerosol Pyrolysis

  • Jeoung, Byung-Woo;Yoo, Won-Tae;Hong, Gun-Young;Yoo, Jae-Soo
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 2002.08a
    • /
    • pp.788-791
    • /
    • 2002
  • The phosphors of high luminous efficiency for PDP application must have high purity, single phase, and dense surface. In this work, the polymeric reaction was applied to preparation of spherical phosphor by aerosol pyrolysis in order to enhance mechanical and optical characteristics. The red phosphor of (Y,Gd)$BO_3$:Eu was prepared from polymeric precursor, in which citric acid and ethylene glycol were used as ion carriers, i.e monomers. For enhancing the luminescence intensity and mechanical characteristics. optimum synthesizing condition were investigated through concentration of monomers, synthetic temperature. doped activator concentrations, and annealing process. The phosphors synthesized with monomers showed quite different morphology from those without monomers. It was observed that polymeric precursor made an effect on particle formation mechanism and status of particles surface. The resultant spherical phosphors show the comparable luminescent properties to the commercial product (product by Nichia co.). Also, they were observed to have the rigid surface.

  • PDF

Epitaxy of Self-assembled InAs Quantum Dots on Si Substrates by Atmospheric Pressure Metalorganic Chemical Vapor Deposition (대기압 MOCVD 시스템을 이용하여 Si 기판 위에 자발적으로 형성된 InAs 양자점에 대한 연구)

  • Yoo, Choong-Hyun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.18 no.6
    • /
    • pp.527-531
    • /
    • 2005
  • Fully coherent self-assembled InAs quantum dots(QDs) grown on Si (100) substrates by atmospheric pressure metalorganic chemical vapor deposition(APMOCVD) were grown and the effect of growth conditions such as growth rate and growth time on quantum dots' morphology such as densities and sizes was investigated. InAs QDs of 30 - 80 nm in diameters with densities in the range of (0.6 - 1.7) x $10^{10}\;cm^{-2}$ were achieved on Si substrates and InAs layer was changed from 2 dimensional growth to 3 dimensional one at a nominal thickness less than 0.48 ML. This is attributed to the higher ambient pressure of APMOCVD suppressing of In segregation from the 2 dimensional InAs layer. This In segregation looked to disturb the dot formation especially when the growth rate was low so that the dots became less dense and bigger as the growth rate was lower.