• Journal of the Korean Crystal Growth and Crystal Technology
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• v.24 no.4
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• pp.151-157
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• 2014

The degradation mechanisms of thermal barrier coatings (TBCs) were investigated in different thermal fatigue condition in terms of microstructural analyses. The isothermal and cyclic oxidation tests were conducted to atmospheric plasma sprayed-TBCs on NIMONIC 263 substrates. The delamination occurred by the oxide layer formation at the interface, the Ni/Cr-based oxide was formed after Al-based oxide layer grew up to ${\sim}10{\mu}m$ in the isothermal condition. In the cyclic oxidation with dwell time, the failure occurred earlier (500 hr) than in the isothermal oxidation (900 hr) at same temperature. The thickness of Al-based oxide layer of the delaminated specimen in the cyclic condition was ${\sim}4{\mu}m$ and the interfacial cracks were observed. The acoustic emission method revealed that the cracks generated during the cooling step. It was considered that the specimens were prevented from the formation of the Al-based oxide by cooling treatment, and the degradation mode in the cyclic test was dominantly interfacial cracking by the difference of thermal expansion coefficients of the coating layers.

• Bulletin of the Korean Chemical Society
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• v.33 no.2
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• pp.601-607
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• 2012

An aspect of organophilic modification for the delamination is described for the layered rare-earth hydroxides in this paper. The interlayer property of $RE_2(OH)_5NO_3{\cdot}nH_2O$, where RE=Eu (LEuH) and Tb (LTbH), was modified by the exchange reaction of nitrate ion with oleate anion that is one of the representative dispersion agents in nonpolar solvents. The bilayer arrangement of long oleate anions in the gallery of $RE_2(OH)_5NO_3{\cdot}nH_2O$ could effectively weaken the stacking of the hydroxide layers. Highly organophilic environment of the interlayer space promoted the introduction of toluene to delaminate the layered structure into their individual sheets. When irradiated with 365 nm UV, the resulting transparent colloidal solutions of toluene containing LEuH and LTbH nanosheets yielded typical red and green emissions, respectively, which are visible to the naked eye.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.3
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• pp.806-815
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• 1996

The interlaminar fracture behavior of woven laminates under static and cyclic loadings has been studied using DCB(double cantilever beam) specimens. The effects of surface treatment and stiching on the fracture behavior of composite laminates are investigated experimentally. Fracture toughness has been improved by surface treatment because the surface treatment can change the fracture mechanism of laminates. SCB(stitched cantilever beam) model has been proposed to quantify the effect of through-thickness resinforcement(stiching) in improving the delamination crack growth resistance. Distributed loads which are transfered to through-thickness fibers can be calculated by the SCB model. And fracture energy increase due to the distributed load can be predicted by a power function of the distributed load. A new parameter agreed well proposed predict fatigue crack growth rate. The predictions using this parameter agreed well with the experimental data.

• Journal of the Korean Society of Propulsion Engineers
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• v.16 no.2
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• pp.65-72
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• 2012

A defect analysis program for a composite motor case was developed to apply the ultrasonic signal processing method, based on the ultrasonic pulse-echo method. With the proposed defect analysis program, defects of FRP delamination and FRP/Rubber disbond in the composite motor case could be quantitatively measured. The defects detected in the composite motor case were in good agreement with the results measured with the computed tomography and video microscope. This paper described the development process of the defect analysis program to convert the ultrasonic test data into the C-Scan images.

• Journal of Institute of Control, Robotics and Systems
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• v.13 no.11
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• pp.1060-1066
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• 2007

When a high-energy ultrasound propagates through a solid body that contains a crack or a delamination, the two faces of the defect do not ordinarily vibrate in unison, and dissipative phenomena such as friction, rubbing and clapping between the faces will convert some of the vibrational energy to heat. By combining this heating effect with infrared imaging, one can detect a subsurface defect in material efficiently. In this paper a detection of the welding defect of thin SUS 304 plates using the UIR (ultrasonic infrared imaging) technology is described. A low frequency (20kHz) ultrasonic transducer was used to infuse the welded thin SUS 304 plates with a short pulse of sound for 280ms. The ultrasonic source has a maximum power of 2kW. The surface temperature of the area under inspection is imaged by a thermal infrared camera that is coupled to a fast frame grabber in a computer. The hot spots, which are a small area around the defect tip and heated up highly, are observed. From the sequence of the thermosonic images, the location of defective or inhomogeneous regions in the welded thin SUS 304 plates can be detected easily.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.14 no.4
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• pp.469-479
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• 2001

In the present study, free vibration analysis of multi-delaminated beams is performed. In order to investigate the effects of mu1ti-delaminations on the dynamic characteristics of multi-delaminated beams, the general kinematic continuity conditions are derived from the assumption of constant curvature at the multi-delamination tip. Frequency equations of multi-delaminated beams are obtained by dividing the global multi-delaminated beam into beam segments and by imposing recurrence relation from the continuity conditions un each sub-beam. The comparisons between the results of numerical analysis obtained by finite element analysis and those of present analysis give good agreement with each other. It is shown that the effects of multi-delaminations on free vibration characteristics of laminated beams could be used to detect their sizes, types and locations from the results.

• Advances in aircraft and spacecraft science
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• v.4 no.6
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• pp.679-699
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• 2017

The aim of this study is to perform a finite element analysis of the Von Mises stresses distribution in the adhesive layer and of the J-Integral for a damaged plate repaired by a composite patch. Firstly, we study the effect of the fiber orientation, especially the position of the layers that have orientation angle different of $0^{\circ}$ from the first layer which is in all cases of our study oriented at ($0^{\circ}$) on the J-Integral. Secondly, we evaluate the effects of the mechanical properties of the patch and the use of a hybrid patch on the reduction of stresses distribution and J-Integral. The results show clearly that the stacking sequence for the composite patch must be selected to absorb optimally the stresses from the damaged area and to position the various layers of the composite under the first layer whose fibers orientation will remain in all cases equal to $0^{\circ}$. The use of a hybrid composite reduces significantly the J-Integral and the stresses in both damaged plate and the adhesive layer.

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.200.1-200.1
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• 2016

Tungsten coatings on the graphite (CX-2320) were successfully deposited using the vacuum plasma spraying (VPS) method. An optimum coating procedure was developed and coating thicknesses of $409{\mu}m$ (without an interlayer) and $378{\mu}m$ (with an interlayer) were obtained with no cracks and no signs of delamination. The mechanical characteristics and microstructure of the tungsten coating layers were investigated using a Vickers hardness tester, FE-SEM, EDS, and XRD. The effect of a titanium interlayer on the properties of the tungsten coating was investigated. It was shown that the titanium interlayer prevented the diffusion of carbon to the tungsten layer, thereby suppressing the formation of tungsten carbide. Vickers hardness data yielded values that were 62.5 ~ 80.46% of those for bulk tungsten, indicating that tungsten coatings on graphite can be utilized as a plasma-facing material. High heat flux tests were performed by using thermal plasma with a maximum flux of $10MW/^2$. Vickers hardness after the heat flux test is performed to see a change in the mechanical properties. The formationof a tungsten carbide and the effect of the titanium interlayer for the diffusion barrier are investigated by using energy dispersion spectroscopy (EDS).

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.237.2-237.2
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• 2016

A pure hafnium-carbide (HfC) coating layer was deposited onto carbon/carbon (C.C) composites using a vacuum plasma spray system. By adopting a SiC buffer layer, we successfully integrated C.C composites with a $100-{\mu}m-thick$ protective coating layer of HfC. Compared to the conventional chemical vapor deposition process, the HfC coating process by VPS showed increased growth rate, thickness, and hardness. The growth behavior and morphology of HfC coatings were investigated by FE-SEM, EDX, and XRD. From these results, it was shown that the addition of a SiC intermediate layer provided optimal surface conditions during the VPS procedure to enhance adhesion between C.C and HfC (without delamination). The thermal ablation test results shows that the HfC coating layer perfectly protected inner C.C layer from thermal ablation and oxidation. Consequently, we expect that this ultra-high temperature ceramic coating method, and the subsequent microstructure that it creates, can be widely applied to improve the thermal shock and oxidation resistance of materials under ultra-high temperature environments.

• Composites Research
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• v.30 no.2
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• pp.149-157
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• 2017

In this paper, fracture behavior of laminated composites with notch was studied by cohesive zone modeling approach. The numerical modeling proceeded by first generating 3 dimensional solid element meshes for notched laminated composite coupon configurations. Then cohesive elements representing failure modes of fiber fracture, matrix cracking and delamination were inserted between bulk elements in all regions where the corresponding failures were likely to occur. Next, progressive failure analyses were performed simulating uniaxial tensile tests. The numerical results were compared to those by experiment available in the literature for verification of the analysis approach. Finally, notched laminated composite configurations with selected stacking sequences were analyzed and the failure behavior was carefully examined focusing on the failure initiation and progression and the dominating failure modes.