• Title/Summary/Keyword: delamination.

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INFLUENCE OF INVESTMENT/CERAMIC INTERACTION LAYER ON INTERFACIAL TOUGHNESS OF BODY CERAMIC BONDED TO LITHIA-BASED CERAMIC

  • Park, Ju-Mi
    • The Journal of Korean Academy of Prosthodontics
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    • v.44 no.6
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    • pp.683-689
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    • 2006
  • Statement of problem. Interfacial toughness is important in the mechanical property of layered dental ceramics such as core-veneered all-ceramic dental materials. The interfaces between adjacent layers must be strongly bonded to prevent delamination, however the weak interface makes delamination by the growth of lateral cracks along the interface. Purpose. The purpose of this study was to determine the effect of the reaction layer on the interfacial fracture toughness of the core/veneer structure according to the five different divesting. Materials and methods. Thirty five heat-pressed Lithia-based ceramic core bars (IPS Empress 2), $20mm{\times}3mm{\times}2mm$ were made following the five different surface divesting conditions. G1 was no dissolution or sandblasting of the interaction layer. G2 and G3 were dissolved layer with 0.2% HF in an ultrasonic unit for 15min and 30 min. G4 and G5 were dissolved layer for 15min and 30min and then same sandblasting for 60s each. We veneered bilayered ceramic bars, $20mm{\times}2.8mm{\times}3.8mm$(2mm core and 1.8mm veneer), according to the manufacturer's instruction. After polishing the specimens through $1{\mu}m$ alumina, we induced five cracks for each of five groups within the veneer close to interface under an applied indenter load of 19.6N with a Vickers microhardness indenter. Results. The results from Vickers hardness were the percentage of delamination G1:55%, G2:50%, G3:35%, G4:0% and G5:0%. SEM examination showed that the mean thickness of the reaction layer were G1 $93.5{\pm}20.6{\mu}m$, G2 $69.9{\pm}14.3{\mu}m$, G3 $59.2{\pm}20.2{\mu}m$, G4 $0.61{\pm}1.44{\mu}m$ G5 $0{\pm}0{\mu}m$. The mean interfacial delamination crack lengths were G1 $131{\pm}54.5{\mu}m$, G2 $85.2{\pm}51.3{\mu}m$, and G3 $94.9{\pm}81.8{\mu}m$. One-way ANOVA showed that there was no statistically significant difference in interfacial crack length among G1, G2 and G3(p> 0.05). Conclusion. The investment reaction layer played important role at the interfacial toughness of body ceramic bonded to Lithia-based ceramic.

Application of Stress Optimization for Preventing the Delamination of the Plastic IC Package in Reflow Soldering Process (리플로 납땜과정에서 플라스틱 IC 패키지의 박리방지를 위한 응력최적설계의 적용)

  • Kim, Geun-Woo;Lee, Kang-Yong;Kim, Ok-Whan
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.6
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    • pp.709-716
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    • 2004
  • In order to prevent the interface delamination of an plastic IC package in the infrared (IR) soldering process, we tried to reduce stress by parameterization, sensitivity analysis and unconstraint optimization. The design variables of dimensions and material properties are determined among all the possible variables from the parametric study. Their optimized values are determined by applying the unconstraint optimization to the parameterized IC package. The maximum von-Mises stress value decreases greatly by optimum design.

Graphite/Epoxy로 만든 두꺼운 관의 저속 충격손상에 관한 연구

  • 김형원;윤영주;나성엽
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2000.04a
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    • pp.24-24
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    • 2000
  • 작업 중 공구를 관에 떨어뜨리거나 작업하기 위해 관을 이동하던 중 다른 물체에 부딪힐 경우 복합재로 만들어진 관이 손상을 입게 되는 경우가 생기는데 관이 상황에 따라 얼마나 손상을 입었는지가 본 연구의 관심이다. 충격자는 직경이 25.4mm와 12.7mm인 반구형 2종류와 모서리의 직경이 15mm인 원추형 1종류로 각각 무게가 다르며, 떨어뜨리는 자유낙하 높이는 120mm에서 700mm로 종류에 따라 간격을 달리했다. 실험 장치로는 Dynatup 8250을 사용했으며 충격에너지, 최대충격하중, 충격변위, contact diameter를 측정했다. 시험 후 시편은 방사선 촬영을 하여 충격자의 종류에 따라 손상의 정도가 어떻게 다른지를 파악했다. 직경이 25.4mm인 반구형의 충격자는 표면의 손상은 적었으나 복합재 관의 내부에 delamination이 많이 생겼으며 직경이 12.7mm인 반구형의 충격자는 표면의 손상이 심했으나 내부의 delamination이 상대적으로 적었다. Contact diameter와 최대충격하중과의 관계는 실험치와 이론치가 잘 일치했으나 Kinetic energy와 최대충격하중과의 관계는 실험치와 이론치의 차이가 있었다.

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Detection of Real Defects in Composite Structures by Using Laser Measuring System (레이저 계측시스템을 이용한 복합재료 구조물의 실제결함 검출)

  • 김태형;정성균;김경석;장호섭
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.05a
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    • pp.35-38
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    • 2002
  • Real defects in composite structures were detected by using laser measuring system. Four types of specimens, that is, a composite laminate, a honeycomb structure, a free-edge delamination and an adhesive joint, were used to study the applicability of ESPI and Shearography to composite structures. Thermal loading method, which can easily induce the surface deformation of specimen, was used to detect defects. Experimental results show that defects in composite structures can be easily detected by ESPI and Shearography. Moreover, it shows that ESPI and Shearography can be usefully applied to the detection of defects in various kinds of composite structures.

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Low velocity Impact Characteristics of Non-flamable Composite Laminates (난연성 복합적층재의 저속충격특성)

  • 김재훈;김후식;조정미;박병준
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2001.10a
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    • pp.179-182
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    • 2001
  • Impacter tester was build of to evaluate the characterization of non-flamable Glass/phenol laminate plates under the low velocity impact. The damage of composite laminates are matrix cracking, delamination, and fiber breakage for impact energy. In this study, this is to find impact properties of Glass/phenol in used in a forehead part of lighting subway. To determine impact damage characteristics which is made in a laminate, use the UT C-scan after- macrography. And then evaluated the reduction of strength in a rate of impact energy with CAI(Compression After Impact) test

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The Development of Pattern Classification for Inner Defects in Semiconductor Packages by Self-Organizing Map (자기조직화 지도를 이용한 반도체 패키지 내부결함의 패턴분류 알고리즘 개발)

  • 김재열;윤성운;김훈조;김창현;양동조;송경석
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.12 no.2
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    • pp.65-70
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    • 2003
  • In this study, researchers developed the estimative algorithm for artificial defect in semiconductor packages and performed it by pattern recognition technology. For this purpose, the estimative algorithm was included that researchers made software with MATLAB. The software consists of some procedures including ultrasonic image acquisition, equalization filtering, Self-Organizing Map and Backpropagation Neural Network. Self-organizing Map and Backpropagation Neural Network are belong to methods of Neural Networks. And the pattern recognition technology has applied to classify three kinds of detective patterns in semiconductor packages : Crack, Delamination and Normal. According to the results, we were confirmed that estimative algerian was provided the recognition rates of 75.7% (for Crack) and 83.4% (for Delamination) and 87.2 % (for Normal).

Fatigue Damage of Quasi-Isotropic Composite Laminates Under Tensile Loading in Different Directions (인장하중방향 변화를 받는 의사등방성 복합재 적층판의 피로손상)

  • 김택현
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.8 no.2
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    • pp.80-85
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    • 1999
  • The purpose of this work is to investigate fatigue damage of quasi-isotropic laminates under tensile loading in different directions. Low cycle fatigue tests of [0/-60/+60]a laminates and [+30/-30/90]s lamina tes were carried out. Material systems used are AS4/Epoxy and AS4/PEEK. The fatigue damage of [+30/-30/90]s is very different from that of [0/-60/+60]s. The position of delamination generated at AS4/Epoxy and AS$/PEEK laminates were differentiated by the matrix difference that is, we suppose, the value of both GIcr(critical energy release rate of mode-I) and GIIIcr(critical energy release rate of mode-III) difference.

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A Study on the Impact Damage and Residual Bending Strength of CF/EPOXY Composite Laminate Plates Under High Temperature (고온분위기하에서 탄소섬유강화 복합재적층판의 충격손상과 잔류굽힘강도)

  • 양인영;박정수
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.8
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    • pp.1930-1938
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    • 1994
  • In this paper, the effects of temperature change on the impact of CFRP laminates was experimentally studied. Composite laminates used for this experiment are CFRP orthotropic laminated plates, which have two-interfaces$[0_6^{\circ}/90_7^{\circ}]_s$ and four-interfaces$[0_3^{\circ}/90_6^{\circ}/0_3^{\circ}]_s$. The interrelations between the impact energy vs. delamination area, the impact energy vs. residual bending strength, and the interlayer delamination area vs. the decrease of the residual flexural strength of carbon fiber epoxy composite laminates subjected to FOD(Foreign Object Damage) under high temperatures were experimentally observed.