• Title/Summary/Keyword: degradation analysis

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Degradation of Properties and Loss of Nutrients in Gelatin Soft Capsules the Manufacturing Process

  • Lee, Jin Kyoung
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.22 no.1
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    • pp.15-23
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    • 2016
  • Gelatin soft capsules, manufactured by the press through package(PTP) process, are widely used in the production of multivitamin dietary supplements and other health functional foods. Gelatin capsules can prevent light and air from having a direct contact with the contents in the capsule, and the nutrients inside the capsules are preserved without any loss. In the present study, on the basis of the results on the safety of gelatin capsules. The parameters investigated included degradation of the capsules before their shelf life, capsule deformation, and changes in specific nutrients. Moisture and heat in the production and storage environments of the capsules caused the gelatin to swell and attach some of the inorganic salts in the vitamin contents. Nutritional component analysis showed that B1, B5, B9, and B12 contents were decreased, while mineral elemental analysis shown calcium, chloride, and zinc compound were found to be infused into the gelatin of the capsule shell.

Capability of Thermal Field-Flow Fractionation for Analysis of Processed Natural Rubber

  • Lee, Seong Ho;Eun, Cheol Hun;Anthony R. Plepys
    • Bulletin of the Korean Chemical Society
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    • v.21 no.1
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    • pp.69-74
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    • 2000
  • Applicability of Thermal field flow fractionation (ThFFF) was investigated for the analysis of masticated natural rubber (NR) adhesives produced bya hot melt mastication process. An optimum ThFFF condition for NR analysis was found by using tetrahydrofuran (THF) as a solvent/carrier and a field-programming. Low flowrate (0.3 mL/min) was used to avoid stopping the flow for the sample relaxation. Measured molecular weight distribution was used to monitor degradation of rubber during the mastication process. Rubber samples collected at three different stages of the mastication process and were analyzed by ThFFF. It was found that in an anaerobic process rubber degradation occurs at the resin-mixing (compounding) zone as well as in the initial break-down zone, while in an aerobic process most of degradation occurs at the initial breakdown zone. It was also found that E-beam radiation on NR causes a slight increase in the NR molecular weight due to the formation of a branched structure.

Experimental Analysis of GDL Degradation in PEM Fuel Cell (고분자전해질형 연료전지 가스확산층의 내구 성능 저하에 관한 실험적 분석)

  • Ha, Tae-Hun;Park, Jae-Man;Cho, Jun-Hyun;Min, Kyoung-Doug;Lee, Eun-Suk;Jung, Ji-Young;Kim, Do-Hun;Jin, Yong-Won;Lee, Dae-Han
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.132-132
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    • 2009
  • To achieve the commercialization of PEM fuel cell, the durability problem must be solved. Recently, many researchers have focused on this durability problem and degradation studies about membrane and electrode have been reported. But durability characteristics of gas diffusion layer is not much reported yet. Durability of GDL is very important to maintain the performance of PEM fuel cell because the main function of GDL is a path of fuel and water and the GDL degradation causes the loss of the GDL function. In this study, the degradation of GDL, especially, the mechanical degradation process was investigated with the leaching test. The effect of water dissolution was observed through the test and the amount of GDL degradation was measured with various measurement methods such as weight measurement, static contact angle measurement, scanning electron microscope. After 2,000 hours test, the GDL showed structural damage and loss of hydrophobicity.

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Application of UV-Vis Spectroscopic Analysis for Transformer Insulating Paper Degradation (UV-Vis 분광분석에 의한 전기변압기 내 절연지 열화도 측정)

  • Kong, Hosung;Han, Hung-Gu
    • Tribology and Lubricants
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    • v.35 no.3
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    • pp.151-157
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    • 2019
  • Insulated oil degradation produces charged by-products, such as acids and hydro-peroxides, which tend to reduce the insulating properties of the oil. In this study, UV-vis spectroscopy measurement technology is developed and experimentally compared with other measurement methods, such as the titration method and IR spectroscopy, to validate its ability to monitor the degradation of electrical insulating paper. The degradation characteristics of the insulating paper are appropriately represented through various types of measurement methods, such as the Tan (delta) method, $CO_2$ gas production measurement, the titration method, and IR spectroscopy. The results are demonstrated to be well comparable to a change in the fluorescence emission ratio (FER), which is defined as the shift in fluorescence intensity in the measured wavelength range, and also to the chromatic ratio, which is defined as a color shift to longer wavelength ranges. The results also show that, by using UV-vis spectroscopy, it is possible to detect the degradation of the insulating paper. This study suggests that UV-vis spectroscopy can be applied as an alternative to high-performance liquid chromatography, which is the internationally recognized measurement technology for cellulose paper degradation. The FER detector is also verified to be useful as an effective condition-monitoring device for power transformers.

Progressive Filure Analysis of Composite Double Bolted Joints using Gradual Degradation Model (점진적 강성 저하 모델을 이용한 복합재 이중 볼트 체결부의 점진적 파손 해석 연구)

  • Kim, Pyunghwa;Kim, Sungmin;Doh, Sungchul;Yoon, Donghyun;Park, Jungsun
    • Journal of Aerospace System Engineering
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    • v.13 no.6
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    • pp.26-35
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    • 2019
  • In this paper, progressive failure analysis is performed on composite joints widely used in various industries such as the aerospace industry. The analysis was conducted on single bolted joints to confirm its reliability and in succession on double-bolted composite joints as well to study the characteristics of progressive failure. Hashin failure criteria and EGDM (energy based gradual degradation model) were used for the analysis. Failure variables are defined by four failure modes, respectively. According to the variables, stiffness degradation has been calculated. As a result of comparing the test and analysis results of single-bolted joints, the error was below 5% and it showed that the analytical results are rather credible. Also, the parametric analysis consequences were obtained conducting the process-progressive failure analysis on the double-bolted composite joints considering edge-distance ratio (e/d ratio) and bolt spacing.

Modeling of coupled THMC processes in porous media

  • Kowalsky, Ursula;Bente, Sonja;Dinkler, Dieter
    • Coupled systems mechanics
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    • v.3 no.1
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    • pp.27-52
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    • 2014
  • For landfill monitoring and aftercare, long-term prognoses of emission and deformation behaviour are required. Landfills may be considered as heterogeneous porous soil-like structures, in which flow and transport processes of gases and liquids interact with local material degradation and mechanical deformation of the solid skeleton. Therefore, in the framework of continuous porous media mechanics a model is developed that permits the investigation of coupled mechanical, hydraulical and biochemical processes in municipal solid waste landfills.

Optimal Design of PV Module with Bypass Diode to Reduce Degradation due to Reverse Excess Current

  • Jung, Tae-Hee;Kang, Gi-Hwan;Ahn, Hyung-Keun
    • Transactions on Electrical and Electronic Materials
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    • v.15 no.5
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    • pp.279-283
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    • 2014
  • In this paper, we present an economical and practical standard to install a bypass diode in a thin-film PV module. This method helps to reduce heat generation and to prevent module degradation due to excess current from reverse bias. The experimental results confirm that for different numbers of solar cells, there is a relation between the excess reverse current and the degradation of solar cells in a-Si:H modules. The optimal number of solar cells that can be connected per bypass diode could be obtained through an analysis of the results to effectively suppress the degradation and to reduce the heat generated by the module. This technique could be expanded for use in high power crystalline Si PV modules.

Evaluation of Static Stability of Hybrid Carbody Structures of Korean Tilting Train eXpress Including Degradation Effects of Composite Materials under Ground Environments (지상환경하에서 복합재료의 물성저하를 고려한 한국형 틸팅열차 하이브리드 차체 구조물의 정적안정성 평가)

  • Shin, Kwang-Bok;Hahn, Seong-Ho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.6
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    • pp.807-815
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    • 2004
  • In order to evaluate the static stability of hybrid carbody structures of Korean Tilting Train eXpress(TTX) caused by degradation of composites under ground environments, T300/AD6005 graphite/epoxy composite specimens were exposed to accelerated environmental conditions including ultraviolet radiation, temperature and moisture fer 2000 hours. It was found that the stiffness and strength of composites after aging were lower than those of unexposed specimens, and decreased as the aging time increases. The values of the degraded properties were used in the static analysis to check the static stability of hybrid carbody structures caused by environmental degradation of composites. The results shown that the structural stability of hybrid carbody structures was affected by the degradation of composites after exposure to accelerated aging environments.

Reliability Analysis of Degradation Data Based on Accelerated Model -With Photointerrupter Used in Home VCR(Video Cassette Recorder)- (가속 모델에 기초한 열화 데이터의 신뢰성 해석 -가정용 영상 재생기에 사용되는 광센서를 중심으로-)

  • Kwon, Soo-Ho;Huh, Yang-Hyun;Lim, Tae-Jin
    • IE interfaces
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    • v.12 no.3
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    • pp.448-457
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    • 1999
  • Accelerated degradation is concerned with models and data analyses for degradation of product performance over time at overstress and design conditions. Although there have been numerous studies with accelerated degradation theory in reliability, very few actually apply to parametric statistical analyses. This paper shows how to analyze degradation data, provides tests for how well the assumptions hold. Reel sensors, a sort of photointerrupters in home VCR, hive been tested, and least-square analyses are used to illustrate our approach. Tests for linearity of the performance-time relationship, dependence of the lognormal distribution, and the standard deviation on time are performed. The mean life of tested sensors is assessed at about 414,000 hours, and the Arrhenius activation energy of this reaction is concluded to be 0.39 eV as results.

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Analysis of Field Reliability Data with Supplementary Information on Degradation Data and Covariates (열화자료와 설명변수 정보를 고려한 사용현장 신뢰성 자료의 분석)

  • 서순근;하천수
    • Journal of Applied Reliability
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    • v.2 no.2
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    • pp.63-83
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    • 2002
  • Degradation data can provide more reliability information than traditional failure-time data, especially products with few or no failures. This paper is concerned with a method of estimating lifetime distribution from field data with supplementary information on degradation data and covariates. When a distribution of degradation rate obtained by follow-up study for a portion of products that survive after-warranty follows a reciprocal-Weibull or lognormal distribution. A time-to-failure distribution of the product follows Weibull or lognormal distribution, respectively. A method of estimating lifetime parameters for this kind of data and their asymptotic properties are studied. Effects of after-warranty report probability, follow-up rate, and proportion of degradation data on pseudo maximum likelihood estimators of these parameters are investigated.

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