• Title/Summary/Keyword: data calibration

Search Result 1,823, Processing Time 0.032 seconds

Comparison of linear and non-linear equation for the calibration of roxithromycin analysis using liquid chromatography/mass spectrometry

  • Lim, Jong-Hwan;Yun, Hyo-In
    • Korean Journal of Veterinary Research
    • /
    • v.50 no.1
    • /
    • pp.11-17
    • /
    • 2010
  • Linear and non-linear regressions were used to derive the calibration function for the measurement of roxithromycin plasma concentration. Their results were compared with weighted least squares regression by usual weight factors. In this paper the performance of a non-linear calibration equation with the capacity to account empirically for the curvature, y = ax$^{b}$ + c (b $\neq$ 1) is compared with the commonly used linear equation, y = ax + b, as well as the quadratic equation, y = ax$^{2}$+ bx + c. In the calibration curve (range of 0.01 to 10 ${\mu}g/mL$) of roxithromycin, both heteroscedasticity and nonlinearity were present therefore linear least squares regression methods could result in large errors in the determination of roxithromycin concentration. By the non-linear and weighted least squares regression, the accuracy of the analytical method was improved at the lower end of the calibration curve. This study suggests that the non-linear calibration equation should be considered when a curve is required to be fitted to low dose calibration data which exhibit slight curvature.

Estimation of the Hapcheon Dam Inflow Using HSPF Model (HSPF 모형을 이용한 합천댐 유입량 추정)

  • Cho, Hyun Kyung;Kim, Sang Min
    • Journal of The Korean Society of Agricultural Engineers
    • /
    • v.61 no.5
    • /
    • pp.69-77
    • /
    • 2019
  • The objective of this study was to calibrate and validate the HSPF (Hydrological Simulation Program-Fortran) model for estimating the runoff of the Hapcheon dam watershed. Spatial data, such as watershed, stream, land use, and a digital elevation map, were used as input data for the HSPF model. Observed runoff data from 2000 to 2016 in study watershed were used for calibration and validation. Hydrologic parameters for runoff calibration were selected based on the user's manual and references, and trial and error method was used for parameter calibration. The $R^2$, RMSE (root-mean-square error), RMAE (relative mean absolute error), and NSE (Nash-Sutcliffe efficiency coefficient) were used to evaluate the model's performance. Calibration and validation results showed that annual mean runoff was within ${\pm}4%$ error. The model performance criteria for calibration and validation showed that $R^2$ was in the rang of 0.78 to 0.83, RMSE was 2.55 to 2.76 mm/day, RMAE was 0.46 to 0.48 mm/day, and NSE was 0.81 to 0.82 for daily runoff. The amount of inflow to Hapcheon Dam was calculated from the calibrated HSPF model and the result was compared with observed inflow, which was -0.9% error. As a result of analyzing the relation between inflow and storage capacity, it was found that as the inflow increases, the storage increases, and when the inflow decreases, the storage also decreases. As a result of correlation between inflow and storage, $R^2$ of the measured inflow and storage was 0.67, and the simulated inflow and storage was 0.61.

Development of Calibration Model for Firmness Evaluation of Apple Fruit using Near-infrared Reflectance Spectroscopy (사과 경도의 비파괴측정을 위한 검량식 개발 및 정확도 향상을 위한 연구)

  • 손미령;조래광
    • Food Science and Preservation
    • /
    • v.6 no.1
    • /
    • pp.29-36
    • /
    • 1999
  • Using Fuji apple fruits cultivated in Kyungpook prefecture, the calibration model for firmness evaluation of fruits by near infrared(NIR) reflectance spectroscopy was developed, and the various influence factors such as instrument variety, measuring method, sample group, apple peel and selection of firmness point were investigated. Spectra of sample were recorded in wavelength range of 1100∼2500nm using NIR spectrometer (InfraAlyzer 500), and data were analyzed by stepwise multiple linear regression of IDAS program. The accuracy of calibration model was the highest when using sample group with wide range, and the firmness mean values obtained in graph by texture analyser(TA) were used as standard data. Chemometrics models were developed using a calibration set of 324 samples and an independent validation set of 216 samples to evaluate the predictive ability of the models. The correlation coefficients and standard error of prediction were 0.84 and 0.094kg, respectively. Using developed calibration model, it was possible to monitor the firmness change of fruits during storage frequently. Time, which was reached to firmness high value in graph by TA, is possible to use as new parameter for freshness of fruit surface during storage.

  • PDF

Calibration Techniques for Low-Level Current Measurement in the Characteristic Analysis System for Semiconductor Devices (저전류 측정을 위한 반도체 소자 특성 분석 시스템에서의 보상 기법)

  • Choi, In-Kyu;Park, Jong-Sik
    • Journal of Sensor Science and Technology
    • /
    • v.11 no.2
    • /
    • pp.111-117
    • /
    • 2002
  • In this paper, we proposed calibration techniques to improve measurement accuracy in the characteristic analysis system for semiconductor devices. Systematic errors can be reduced using proposed calibration techniques. Also, error current reduction procedures including leakage current and offset current are proposed to measure low-level current in pA level. Calibration parameters are calculated and stored by microprocessor using least-square fitting with measured sample data. During measurement time microprocessor corrects measured data using stored calibration parameters. Experimental results show that current measurement error above nA level is less than 0.02%. And they also show that current measurement in pA level can be performed with about 0.2% accuracy.

Discriminant analysis based on a calibration model (Calibration 모형을 이용한 판별분석)

  • 이석훈;박래현;복혜영
    • The Korean Journal of Applied Statistics
    • /
    • v.10 no.2
    • /
    • pp.261-274
    • /
    • 1997
  • Most of the data sets to which the conventional discriminant rules have been applied contain only those which belong to one and only one class among the classes of interest. However the extension of the bivalence to multivlaence like Fuzzy concepts strongly influence the traditional view that an object must belong to only class. Thus the goal of this paper is to develop new discriminant rules which can handle the data each object of which may belong to moer than two classes with certain degrees of belongings. A calibration model is used for the relationship between the feature vector of an object and the degree of belongings and a Bayesian inference is made with the Metropolis algorithm on the degree of belongings when a feature vector of an object whose membership is unknown is given. An evalution criterion is suggested for the rules developed in this paper and comparision study is carried using two training data sets.

  • PDF

The Laser Calibration Based On Triangulation Method (삼각법을 기반으로 한 레이저 캘리브레이션)

  • 주기세
    • Journal of the Korea Institute of Information and Communication Engineering
    • /
    • v.3 no.4
    • /
    • pp.859-865
    • /
    • 1999
  • Many sensors such as a laser, and CCD camera to obtain 3D information have been used, but most of algorithms for laser calibration are inefficient since a huge memory and experiment data are required. This method saves a memory and an experimental data since the 3D information are obtained simply triangulation method. In this paper, the calibration algorithm of a slit km laser based on triangulation method is introduced to calculate 3D information in the real world. The laser beam orthogonally mounted on the XY table is projected on the floor. A CCD camera observes the intersection plane of a light and an object plane. The 3D information is calculated using observed and calibration data.

  • PDF

A Clock and Data Recovery Circuit with Adaptive Loop Bandwidth Calibration and Idle Power Saved Frequency Acquisition

  • Lee, Won-Young;Jung, Chae Young;Cho, Ara
    • JSTS:Journal of Semiconductor Technology and Science
    • /
    • v.17 no.4
    • /
    • pp.568-576
    • /
    • 2017
  • This paper presents a clock and data recovery circuit with an adaptive loop bandwidth calibration scheme and the idle power saved frequency acquisition. The loop bandwidth calibration adaptively controls injection currents of the main loop with a trimmable bandgap reference circuit and trains the VCO to operate in the linear frequency control range. For stand-by power reduction of the phase detector, a clock gating circuit blocks 8-phase clock signals from the VCO and cuts off the current paths of current mode D-flip flops and latches during the frequency acquisition. 77.96% reduction has been accomplished in idle power consumption of the phase detector. In the jitter experiment, the proposed scheme reduces the jitter tolerance variation from 0.45-UI to 0.2-UI at 1-MHz as compared with the conventional circuit.

Calibration Method of Vehicle Weight Data from Weigh-In-Motion System According to Temperature Effects (온도의 영향에 대한 Weigh-In-Motion 시스템의 차량중량자료 보정기법)

  • Hwan, Eui-Seung;Lee, Sang-Woo
    • International Journal of Highway Engineering
    • /
    • v.12 no.4
    • /
    • pp.187-196
    • /
    • 2010
  • The purpose of this study is to develop the calibration method for temperature effects to improve the accuracy of the Weigh-In-Motion(WIM) system for collecting long-term truck weight data. WIM system was installed at a location where the truck traffic volume is high and weight data has been collected from January 2010. In this study, as a calibration measure, the first axle weight of Truck Type 10, the semi tractor-trailer is used based on the fact that the first axle weight is relatively constant, independent of the cargo weight. From this fact, calibration equations are developed from the relationship between the axle weight and the temperature(daily mean, maximum and minimum). Analysis on calibrated weight data shows adequacy of the proposed calibration method. Results of this study can be used to improve the accuracy of the WIM system and to carry out more rational design of pavement and bridge structures.

An Accurate Extrinsic Calibration of Laser Range Finder and Vision Camera Using 3D Edges of Multiple Planes (다중 평면의 3차원 모서리를 이용한 레이저 거리센서 및 카메라의 정밀 보정)

  • Choi, Sung-In;Park, Soon-Yong
    • KIPS Transactions on Software and Data Engineering
    • /
    • v.4 no.4
    • /
    • pp.177-186
    • /
    • 2015
  • For data fusion of laser range finder (LRF) and vision camera, accurate calibration of external parameters which describe relative pose between two sensors is necessary. This paper proposes a new calibration method which can acquires more accurate external parameters between a LRF and a vision camera compared to other existing methods. The main motivation of the proposed method is that any corner data of a known 3D structure which is acquired by the LRF should be projected on a straight line in the camera image. To satisfy such constraint, we propose a 3D geometric model and a numerical solution to minimize the energy function of the model. In addition, we describe the implementation steps of the data acquisition of LRF and camera images which are necessary in accurate calibration results. In the experiment results, it is shown that the performance of the proposed method are better in terms of accuracy compared to other conventional methods.

Measurement of Traceability Error for Calibration Service Center Using Type S Thermocouples (S형 열전대를 이용한 교정검사기관의 소급성 오차측정)

  • Gam, Kee-Sool;Kim, Yong-Gyoo;Kim, Sun-Gon
    • Journal of Sensor Science and Technology
    • /
    • v.4 no.1
    • /
    • pp.43-50
    • /
    • 1995
  • We measured the traceability error for nine high temperature calibration service centers including KRISS through the round-robin test. In this test the type S thermocouple, which used as a calibration standard thermometer commonly, was accommodated as a test thermocouple. Intercomparison data of three institutions were coincident with KRISS's data within ${\pm}0.5^{\circ}C$, which was the calibration uncertainty of the type S thermocouple, but the remaining six institution's data were deviated from the assigned uncertainty level. Deviation of the intercomparison data increased gradually according to the increase of the test temperature. and the maximum difference was so large as about $2.0^{\circ}C$ at the highest test temperature, gold point. In this study we found the traceability error of high temperature calibration service center for a high temperature standard was within $2.0^{\circ}C$.

  • PDF