• Title/Summary/Keyword: curing cycles

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BOND STRENGTH BETWEEN COBALT-CHROMIUM ALLOY AND DENTURE BASE RESIN ACCORDING TO ADHESIVE PRIMERS (금속표면처리제에 따른 코발트-크롬 합금과 의치상용 레진의 결합강도)

  • Park, Jong-Il;Kwon, Ju-Hong;Lee, Hae-Hyeung;Cho, Hay-Won
    • The Journal of Korean Academy of Prosthodontics
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    • v.38 no.2
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    • pp.160-168
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    • 2000
  • This study evaluated the effects of four adhesive metal primers on the shear bond strength of a heat curing denture base resin(Lucitone 199) to cobalt-chromium alloy(Biosil-f). The adhesive metal primers were Cesead Opaque Primer, Metal Primer, MR Bond, and Super-Bond liquid. The metal surface primed or nonprimed was filled with the heat-curing methyl methacrylate resin. The specimens were stored in water at $37^{\circ}C$ for 24 hours and the alternately immersed in water bath at $5^{\circ}C\;and\;55^{\circ}C$ for up to 2,000 thermal cycles. Shear bond strengths were measured using UTM at a crosshead speed of 0.5mm/min. Failure surface were examined under magnifying glasses. All the primers examined improved the shear bond strength between denture base resin and cobalt-chromium alloy compared with nonprimed specimens before thermal cycling. The bond strength of Cesead Opaque Primer was greatest. And after 2,000 thermal cycles, the bond strengths between resin and cobalt-chromium alloy were decreased but the difference between thermal cycling 0 and 2,000 at Cesead Opaque primer and Metal Primer were not significant. This study indicated that Cesead Opaque Primer & Metal Primer is effective primers to obtain higher bond strength between heat cured denture base resin and cobalt-chromium alloy.

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Evaluation of marginal leakage of bulk fill flowable composite resin filling with different curing time using micro-computed tomography technology (Bulk fill 유동성 복합레진의 변연 누출에서 다른 중합시간의 영향에 대해 마이크로시티를 이용한 평가)

  • Kim, Eun-Ji;Lee, Kyu-Bok;Jin, Myoung-Uk
    • Journal of Dental Rehabilitation and Applied Science
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    • v.32 no.3
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    • pp.184-193
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    • 2016
  • Purpose: To evaluate marginal leakage of bulk fill flowable composite resin filling with different curing time by using microcomputed tomography technology. Materials and Methods: 30 previously extracted human molars were randomly divided into 6 groups based upon restorative system and different curing time. Class II cavities (vertical slot cavities) were prepared. An individual metallic matrix was used to build up the proximal wall. The SonicFill or SureFil SDR flow was inserted into the preparation by using 1 bulk increment, followed by light polymerization for different curing times. The different exposure times were 20, 40, and 60 seconds. All specimens were submitted to 5,000 thermal cycles for artificial aging. Micro-CT scanning was performed by using SkyScan 1272. One evaluator assessed microleakage of silver nitrated solution at the resin-dentin interface. The 3D image of each leakage around the restoration was reconstructed with CT-Analyser V.1.14.4. The leakage was analyzed with the Mann-Whitney test. Results: Significant differences were observed between the light curing times, but no significant differences were found between the bulk fill composite resins. Increasing in the photoactivation time resulted in greater microleakage in all the experimental groups. Those subjected to 60 seconds of light curing showed higher microleakage means than those exposed for 20 seconds and 40 seconds. Conclusion: Increasing the photoactivation time is factor that may increase marginal microlekage of the bulk fill composite resins. Further, micro-CT can nondestructively detect leakage around the resin composite restoration in three dimensions.

Effect of Disperse Dyeing on UV-curable Flame-retardant Finish of PET Fabrics (분산염료 염색공정이 PET직물의 UV경화형 방염가공에 미치는 영향)

  • Jeong, Yong-Kyun;Jang, Jin-Ho
    • Textile Coloration and Finishing
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    • v.20 no.2
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    • pp.66-74
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    • 2008
  • Effect of disperse dyeing on flame retardant finishing of PET fabrics via UV curing using three UV curable phosphorous-containing methacrylates and ammonium polyphosphate(APP) was investigated. The dye fixation and flame retardancy of PET fabrics did not change significantly with excellent durability to five laundering cycles irrespective of the dyeing and finishing sequence. However, the flame retardancy of Pekoflam-treated fabrics was lower than that of the UV treated and decreased substantially when heat treatment was carried out before the dyeing. The dyeability of the flame-retardant PET fabrics was not affected in the case of UV curing of the methacrylates alone. However, UV finishing after the dyeing caused significant decrease in K/S and ${\Delta}E$ due to changed refraction and inherent color of surface coating of the UV curable monomers and APP. Whereas the heat treatment with Pekoflam decreased both color fastness to laundering and sublimation, surprisingly the UV finish of PET fabrics before and after the dyeing increased the color fastness probably resulting from the presence of photopolymerized surface layer on the fabrics.

Corrosion Behavior of Cr-bearing Corrosion Resistant Rebar in Concrete with Chloride Ion Content

  • Tae, Sung Ho
    • Architectural research
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    • v.7 no.1
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    • pp.49-54
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    • 2005
  • Conventional studies have focused on the reduction in the water-cement ratio, the use of various admixtures, etc., to ensure the durability of reinforced concrete structures against such deterioration factors as carbonation and chloride attack. However, improvement in the concrete quality alone is not considered sufficient or realistic for meeting the recent demand for a service life of over 100 years. This study intends to improve the durability of reinforced concrete structures by improvement in the reinforcing steel, which has remained untouched due to cost problems, through subtle adjustment of the steel components to keep the cost low. As a fundamental study on the performance of Cr-bearing rebars in steel reinforced concrete structures exposed to corrosive environments, The test specimens were made by installing 8 types of rebars in concretes with a chloride ion content of 0.3, 0.6, 1.2, 2.4 and $24kg/m^3$. Corrosion accelerated curing were then conducted with them. The corrosion resistance of Cr-bearing rebars was examined by measuring crack widths, half-cell potential, corrosion area and weight loss after 155 cycles of corrosion-accelerating curing. The results of the study showed that the corrosion resistance increased as the Cr content increased regardless of the content of chloride ions, and that the Cr-bearing rebars with a Cr content of 5% and 9% showed high corrosion resistance in concretes with a chloride ion content of 1.2 and $2.4kg/m^3$, respectively.

Development of Elastic Composites Using Waste Tire Chip and Epoxy Resin - Focused on Strength and Durability - (폐타이어 칩 및 에폭시를 활용한 탄성 복합체의 개발 - 강도와 내구성을 중심으로 -)

  • Sung, Chan Yong;Noh, Jin Yong
    • Journal of The Korean Society of Agricultural Engineers
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    • v.58 no.1
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    • pp.19-26
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    • 2016
  • This study was performed to evaluate the strength and durability properties of modified epoxy composites with waste tire chip, recycled coarse aggregate, filler and modified epoxy to improve elongation and elasticity of epoxy. Additionally, for comparing to modified epoxy and unsaturated polyester resin as a binder, unsaturated polyester resin composites were developed in the same condition. The mix proportions were determined to satisfy the requirement for the workability and slump according to aggregate size and binder content. Tests for the compressive and flexural strength, freezing and thawing and durability for 20 % sulfuric solution were performed. The compressive and flexural strength of modified epoxy composites were in the range of 34.9~61.6 MPa and 10.2~18.3 MPa at the curing 7 days, respectively. Also, the compressive and flexural strength of unsaturated polyester resin composites were in the range of 44.2~77.8 MPa and 11.3~20.8 MPa at the curing 7 days, respectively. After 300 cycles of freezing and thawing, weight decrease ratio and durability factor of modified epoxy composites were in the range of 0.8~1.9 % and 95~98, respectively. Accordingly, modified epoxy composites will greatly improve the durability of concrete.

Characteristic of Resilient Modulus and Unconfined Compressive Strength for Recycled Materials blend with Cement Kiln Dust (CKD 혼합에 따른 Recycled Material의 회복탄성계수와 일축압축강도 특성)

  • Son, Young-Hwan
    • Journal of The Korean Society of Agricultural Engineers
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    • v.52 no.2
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    • pp.19-25
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    • 2010
  • This study was conducted to determine the resilient modulus (Mr) and the unconfined compressive strength (UCS) of two recycled roadway materials such as recycled pavement material (RPM) and road surface gravel (RSG) with or without cement kiln dust (CKD). The recycled materials were blended with two CKD contents (5, 10 %) and 28 day curing time. Mr and UCS tests were also conducted after 10cycles of freezing and thawing to asses the impact of freeze-thaw cycling. Mr was determined conducting by the laboratory test method described by NCHRP 1-28A. Stabilized RPM and RSG had a modulus and a strength higher than unstabilized RPM and RSG. Mr and UCS of RPM and RSG mixed with CKD increased with increasing CKD content. The results indicated that the addition of CKD could be improved the strength and the stiffness of RPM and RSG. Therefore, RPM, RSG and CKD could be used as an effective materials in the reconstruction of roads.

Evaluation of Mechanical Properties of Carbon Fabrics Composite with Thermal Shock (열 충격에 따른 탄소 직물 복합재료의 역학적 특성 평가)

  • Kim, Jae-Hong;Lee, Jung-Ho;Jung, Kyung-Ho;Kang, Tae-Jin
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.79-82
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    • 2005
  • In this study, mechanical properties of carbon fabrics composite under the thermal shock cycling were evaluated. Due to the interactions between fiber and polymer matrix, it is reasonable to conclude that both thermal cycles of thermal shock result in improvement of interlaminar shear strength(ILSS) for the longer conditioning time duration. The rise in ILSS may be attributed to the improved adhesion by cryogenic compressive stress and also by the post-curing strengthening effect. However, the flexural and tensile strength were decreased with increasing conditioning time of thermal cycle.

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Dielectric Cure Monitoring for Glass/Polyester Prepreg Composites (유리섬유/폴리에스터 복합재료를 위한 유전 경화 모니터링)

  • Kim, Hyoung-Geun;Kim, Jin-Kook;Lee, Dai-Gil
    • Proceedings of the KSME Conference
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    • 2001.11a
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    • pp.797-803
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    • 2001
  • The on-line cure monitoring of fiber reinforced thermosetting resin matrix composite material was performed for the better quality and productivity during manufacturing. Since the dissipation factor measured by dielectrometry method is dependent on the degree of cure and temperature of resin, in this study, a new method to obtain the degree of cure during on-line cure monitoring for glass/polyester composites was developed by employing a combination function of the temperature and the dissipation factor. Two sensor signals from a K-type thermocouple and an interdigitated dielectric sensor were processed during curing process under various cure cycles. The DSC (Differential Scanning Calorimetry) data was also used for the reference of degree of cure.

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Digital System for Analyging Oriental Pulse Signals Designed (한방 맥파 분석을 위한 디지틸 시스템 설계)

  • 이준영;서현우;이정환;김정훈;이명호
    • 제어로봇시스템학회:학술대회논문집
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    • 2000.10a
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    • pp.544-544
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    • 2000
  • From ancient times. the diagnosis method of the oriental medicine has been Performed by curing diseases by means of rectifying and adjusting the unbalance in the Physiological function of the five viscera and the six bowels of a human body. Diseases have been diagnosed by the condition of blood circulation that cycles a human body through blood vessels by dint of the vitality of the heart, Based on such a systematic pulse diagnosis method, the article presents parameters that will be beneficial to clinical application on the basis of its analysis of the filtering for eliminating noises from pulse signals inputted from sensor group the digital hardware dealing with signals necessary for recognition algorithm. and the structure of diagnosis algorithm and components of pulse waveform.

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Drying Properties of Cashew Film by Thinning Conditions (희석조건과 카슈도막의 건조성)

  • 노정관
    • Journal of the Korea Furniture Society
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    • v.11 no.1
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    • pp.37-44
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    • 2000
  • This work was done to investigate problems of cashew coating in a wooden-art industry such as ritual vessels and to improve a curing property of cashew film. The main problem in the cashew coating industry was a small-scale business, insufficiency of facilities, lack of knowledge about cashew resin and painting, and lack of a technology of productivity improvement by accelerated drying time of cashew film. In present, cashew coating for ritual vessels mostly used the petroleum as a thinner. The time of set to touch of cashew film thinning with petroleum on glass plates was increased with the increasement of the thinning proportion, but retarded from 3 to 11 times compared to that of an exclusive thinner according to thinning level. The addition of 20% aceton to petroleum contributed to the high reduction rate up to about 60% at the thinning level of 100%, which was effective to accelerate the drying time of cashew film. Even though only the petroleum or the petroleum-aceton(20%) mixture was used as a thinner, it did not exhibit any distinguishable differences in crack and appearance of cashew-film coated on Frexinus rhynchophylla after 5 cycles of soak under the vacuum-drying treatment.

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