• Title/Summary/Keyword: cured method

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A STUDY ON THE PHYSICAL PROPERTIES AND VOLUMETRIC STABILITY OF SR-IVOCAP RESIN SYSTEM (SR-Ivocap resin system의 물리적 특성과 체적 안정성에 관한 연구)

  • Eun, Sung-Sik;Kweon, Hyeog-Sin;Chung, Chae-Heon
    • The Journal of Korean Academy of Prosthodontics
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    • v.36 no.3
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    • pp.453-467
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    • 1998
  • This study helps to clarify conflicting reports by comparing the physical properties and accuracy of complete denture processed by the pack and press technique, continuous- pressure injection technique(SR-Ivocap system) and Mark press technique. The 6 different specimens have been evaluated using the SEM, Impact test, DSC (Differential Scanning Calorimetry) and DMTA (Dynamic Mechanical Thermal Analysis). Each sample was made of SR-Ivocap resin and QC-20 resin by different processing methods. The results were as follows ; 1. As the result of the observation on the fracture surface of resin by use of SEM, sample SR-Ivocap resin cured by continuous pressure injection method showed the most homogeneous structure. This is why molecules in SR-Ivocap resin have no orientation. 2. As the result of the Impact test in order to measure the deformity, fracture energy and impact resistance of resin, the samples with QC-20 acrylic resin and SR-Ivocap resin cured by continuous pressure injection method were exellent. 3. In consequence of measuring ${\alpha}$-glass transition temperature by use of DSC on the basis of temperature change, the glass transition temperatures of sample QC-20 resin cured by pack and press method and sample SR-Ivocap resin cured by continuous pressure injection method were very similar. Thus volumetric stability could not be evaluated only by glass transition temperature. 4. In comparing volumetric stability data by DMTA, the glass transition temperature(Tg) showed $137.88^{\circ}C$ at sample QC-20 resin cured by pack and press method and $139.78^{\circ}C$ at sample SR-Ivocap resin cured by continuous pressure injection method. Therefore sample SR-Ivocap resin cured by continuous pressure injection method seems to be superior to sample QC-20 resin cured by pack and press method in the dimensional stability at high temperature. 5. In comparing storage modulus data by DMTA, the storage modulus of sample SR-Ivocap resin cured by continuous pressure injection method was higher than that of sample QC-20 resin cured by pack and press method. So. sample SR-Ivocap resin cured by continuous pressure injection method seems to be superior to sample QC-20 resin cured by pack and press method in impact strength.

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Effect of Stem Drying Method during Curing Process on Physico-chemical Properties in Bulk Cured Leaves (Bulk건조에서 주맥건조방법이 잎담배 이화학성에 미치는 영향)

  • 이철환;이병철;진정의
    • Journal of the Korean Society of Tobacco Science
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    • v.22 no.2
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    • pp.133-137
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    • 2000
  • The bulk curing experiment to improve the quality of flue-cured leaves were carried out to evaluate relationship between the modified(3 step-up) drying and conventional drying method in bulk curing process. Modified drying method was somewhat higher values in yellowing color index of cured leaves, and less brittle than those in conventional drying program. As to the chemical properties, there was no difference in chemical component levels in cured leaves between the modified and the conventional methods, while the major chemical compounds in relation to aromatic essential oil of cured leaves showed mostly higher level in the modified method than that in conventional drying method. Additionally 3 step-up drying method increased the tobacco quality by 2 % in price per kg compared with conventional drying method.

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Design parameters on the tensile load bearing capacity of a co-cured lap joint with steel and carbon fiber/epoxy composite adherends (강철재료와 탄소섬유/에폭시 복합재료를 이용한 동시경화 조인트의 인장하중 전달용량에 미치는 설계변수에 관한 연구)

  • 신금철;이정주
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2001.05a
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    • pp.172-175
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    • 2001
  • The co-cured Joining method, which is regarded as an adhesively bonded Joining method, is an efficient joining technique because both curing and bonding processes for the composite structures can be achieved simultaneously. It requires neither surface treatment onto the composite adherend nor an additional adhesive joining process because the excess resin, which is extracted from composite materials during consolidation, accomplishes the co-cured Joining process. Since the adhesive of the co-cured joint is the same material as the resin of the composite adherend, the analysis and design of the co-cured joint for composite structures are simpler than those of an adhesively bonded joint, which uses an additional adhesive. In this paper, effects of the manufacturing parameters, namely surface roughness, stacking sequence of the composite adherend, and manufacturing pressure in the autoclave during curing process, on the tensile load bearing capacity of the co-cured single lap joint will be experimentally investigated.

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Estimation of Compressive Strength of Concrete with Granitic Aggregates : Rebound hammer and Ultrasonic Methods (화강암 골재를 사용한 콘크리트의 비파괴 시험에 의한 강도평가)

  • 김현우;이종태;윤기원;김병극;김무한;한천구
    • Proceedings of the Korea Concrete Institute Conference
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    • 1999.10a
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    • pp.651-654
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    • 1999
  • It is required that the compressive strength of concrete should be estimated accurately from the view point of efficient quality control and maintenance of buildings. In this paper, the equations to estimate the compressive strength of concrete using granite aggregates were suggested for both rebound hammer method and ultrasonic pulse velocity method. The results were compared with those for different age or curing condition. The rebound numbers for concrete cured in air were larger than for concrete cured in water. The difference between rebound numbers for concrete cured in water and in air was larger than for concrete cured in water. The difference between rebound numbers for concrete cured in water and in air was larger when water cement ratio was high. Also, with the increase of age, the velocity of ultrasonic pulse for concrete cured in air was measured larger when compared with that in water.

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Tensile load bearing capacities of co-cured single and double lap joints (외면 및 양면겹치기 동시경화조인트의 인장하중 전달용량에 관한 연구)

  • 신금철;이정주
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2001.10a
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    • pp.95-98
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    • 2001
  • Co-cured joining method is an efficient joining technique because both curing and bonding processes for the composite structures can be achieved simultaneously. It requires neither an adhesive nor a surface treatment of the composite adherend because the excess resin, which is extracted from composite materials during consolidation, accomplishes the co-cured joining process. In this paper, we considered three bond parameters, affecting tensile load bearing capacity of the co-cured single and double lap joints. Filially, we nave presented optimal bonding conditions for co-cured single and double lap joints with steel and composite adherends under tensile loads.

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A Study on the Linear Distoration of Self-Curing Resin by Various Curing Technics (다양한 온성방법에 따른 즉시 중합 수지의 선변형에 관한 연구)

  • Lee, Do-Kyung
    • Journal of Technologic Dentistry
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    • v.14 no.1
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    • pp.91-94
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    • 1992
  • This study was made to change dimension of self-curing resin by various curing technics. Specimens were fabricated 45 by 7 curing method. Six measurements(distances AB,BC,CD, AD, AC, and BD) were made of mold section and recorded with micrometer(1/20 mm). The results of the experiment were as follows : 1. The air pressure cured specimens exhibited more distoration than the bench-cured, watercured, and monomer atmosphere-cured specimens(P < 0.05). 2. The water pressure cured specimens exhibited more distoration sphere-cured specimens (P < 0.(15).

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Effect of Cyclic Change of Wet Bulb Temperature During Yellowing Stage on Physical Properties of Flue-Cured Tobacco (황색종 연초 황변기 cyclic건조가 건조엽의 물리성에 미치는 영향)

  • Lee, Chul-Hwan;Jin, Jeong-Eui;Han, Chul-Soo
    • Journal of the Korean Society of Tobacco Science
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    • v.20 no.1
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    • pp.13-18
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    • 1998
  • In the flue curing process, the wet bulb temperature is usually controlled at a constant level. To improve the quality of flue cured leaves, we studied the effect of the cyclic change of wet bulb temperature at the yellowing stage of flue curing on physical properties of cured leaves. The wet bulb temperature was automatically controlled between preset high (38℃) and low point (35℃) every one hour cyclically. As a result, the acceleration of the increase in the physical properties of cured leaves were observed. The leaves cured by this method were more or less orange in color, better bodied, and less brittle compared with the leaves produced by conventional curing. However, the leaves cured by this method had a little sharpness and harshness. As to the physical properties, there was decreased in occurrence of flat leaves than that of conventional ones. On the other hand, in case of cyclic curing method, increase of price per kg reached to 2-3% compared with those of conventional ones.

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Effect of cyclic Change of Wet Bulb Temperature During Yellowing Stage on Chemical Properties of Flue-Cured Tobacco (황색종 cyclic 건조엽의 화학성분 특성)

  • Lee, Chul-Hwan;Jin, Jeong-Eui;Han, Chul-Soo
    • Journal of the Korean Society of Tobacco Science
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    • v.20 no.1
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    • pp.19-25
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    • 1998
  • The bulk curing experiment to the improve the quality of flue-cured leaves were carried out to evaluate relationship between cyclic curing and conventional curing method. We studied the effect of the cyclic change of wet bulb temperature at the yellowing stage of flue curing on chemical properties of cured leaves. The wet bulb temperature was automatically controlled between preset high($38^{\circ}C$) and low point ($35^{\circ}C$) everyone hour cyclically during 12 hours after starting luring. As a result, the acceleration of the increase in the chemical properties of cured leaves were observed. As to the chemical properties, there was decreased in citric acid, increased in malic acid of the nonvolatile organic acids and all higher fatty acids content of leaves cured by this method compared with in that of conventional curing method, while a major chemical compounds in relation to aromatic essence of cigarette smoke in essential oil components of lured leaves was mostly higher in this method than those of conventional ones, and it was evaluated that there was decreased in CO, TPM, Tar, and $CO_2$ content of the cigarette smoke comparing to the conventional luring method.

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AN EXPERIMENTAL STUDY ON THE PHYSICAL PROPERTIES OF THE DENTURE BASE RESINS CURED BY MICROWAVE IRRADIATION (마이크로파 중합에 의한 의치상 레진의 물리적 성질에 관한 연구)

  • Kim, Hak Sun;Kim, Kwang Nam;Chang, Ik Tae
    • The Journal of Korean Academy of Prosthodontics
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    • v.28 no.2
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    • pp.109-124
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    • 1990
  • The purpose of this study was to investigate the physical propertise and determine whether three were any differences in the amount of porosity of the denture base resins cured by microwave irradiation and conventional water bath heating. The resins used in this study were K-33 resin and Acron MC resin. The properties selected were transverse strength, Knoop hardness, and density. A ten-power eyepiece and scanning electron microscope(Magnification of ${\times}$ 30and ${\times}$150)were used to examine the specimens for porosity. Through analyses of the data from this study, the following conclusions were obtained. 1. Microwave energy can be effectively use dtopolymerize poly(methylmethacrylate) denture base resins. 2. In the transverse strength, K-33 resin cured by microwave irradiation was the first highest, water bath cured K-33 resin the second, microwave cured Acron MC resin the third, water bath cured Acron MC resin the fourth. 3. In the Knoop hardness, K-33 resin cured by microwave irradiation was the first hardest, water bath cured K-33 resin the second, water bath cured Acron MC resin the third, microwave cured Acron MC resin the the fourth. 4. No significant difference was found between the density of resin denture bases polymerized by either method. 5. K-33 resin showed the most porosity for the microwave curing. But there was no significant difference in the Acron MC resin and other curing method.

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Effect of Air Flow During Curing Process on Physical Properties of Bulk Cured Leaves (황색종 Bulk건조시 송풍량 조절에 따른 건조엽의 물리성 변화)

  • 이철환;진정의;한철수
    • Journal of the Korean Society of Tobacco Science
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    • v.21 no.1
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    • pp.5-9
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    • 1999
  • In recent years, the line of increase in policy on tobacco production triggered a rise in the loading volume per bulk curing barn, and manufacturers boosted the output of their blowers in order to prevent dirty leaves in the process of curing. for this reason, we studied the effect of the reducing air flow in bulk curing chamber from the color fixing stage to the stem drying stage of flue curing process on physical properties of cured leaves. The control of air flow was composed of the reducing air velocity of blower by means of a voltage regulator (slidac), and condition before color fixing stage was all the same with the conventional curing method. As a result, an effectiveness of improvement in the physical properties of cured leaves were observed. The leaves cured by this method were somewhat orange in color of upper stalk position, better bodied, and less brittle compared with the leaves produced by conventional curing. However, the leaves cured by this method had a little sharpness and harshness. As to the physical properties, there was decreased in occurrence of flat leaves than that of conventional ones. On the other hand, in case of reducing air flow during the curing process, increase of price per kg reached to about 5 % compared with those of conventional curing method.

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