• Macromolecular Research
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• v.12 no.5
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• pp.478-483
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• 2004

Two different diene monomers [dicyclopentadiene (DCPD) and 5-ethylidene-2-norbornene (ENB)] as self-healing agents for polymeric composites were microencapsuled by in situ polymerization of urea and formaldehyde. We obtained plots of the storage modulus (G') and tan $\delta$ as a function of cure time by using dynamic mechanical analysis to investigate the cure behavior of the unreacted self-healing agent mixture in the presence of a catalyst. Glass transition temperatures (T$\_$g/) and exothermic reactions of samples cured for 5 and 120 min in the presence of different amounts of the catalyst were analyzed by differential scanning calorimetry. Of the two dienes, ENB may have advantages as a self-healing agent because, when cured under same conditions as DCPD, it reacts much faster in the presence of a much lower amount of catalyst, has no melting point, and produces a resin that has a higher value of T$\_$g/. Microcapsules containing the healing agent were successfully formed from both of the diene monomers and were characterized by thermogravimetric analysis. Optical microscopy and a particle size analyzer were employed to observe the morphology and size distribution, respectively, of the microcapsules. The microcapsules exhibited similar thermal properties as well as particle shapes and sizes.

• The Journal of Korea Institute of Information, Electronics, and Communication Technology
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• v.4 no.4
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• pp.231-235
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• 2011

In these day, the number of people who have an abnormal posture caused by bad habit are increasing. Therefore, people suffer various disease and symptoms. For correcting the posture to cure, we need continuous monitor, expenditure of time and money. In this study, we develop a posture correcting aid system in other to monitor a posture continuously and leads to pose correctly and records postural variation which are attached to the neck and the waist. The devised system showed good potential for the correct posture guide and a cure of postural defect.

• Korean Journal of Metals and Materials
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• v.47 no.7
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• pp.447-453
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• 2009

Isotropic conductive adhesives (ICAs) have been used or considered as an interconnect material for radio frequency identification (RFID) inlays or other flip chip assemblies due to the advantages of having a low temperature and high-speed bonding. In this work, the curing properties of commercial ICAs for the RFID tag application and the signal transmission in conductive lines that contained the ICA joints were evaluated as a function of the degree of cure at 900 MHz frequency range. The ICAs showed adequate signal transmission only after the curing process passed over the critical time. It was also found that the insertion loss of signal was more dependent on the contact states of Ag fillers in the bondline in preference to the electrical resistance of the ICA itself.

• Elastomers and Composites
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• v.58 no.3
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• pp.136-141
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• 2023

Polyacrylic rubber (ACM) is well known for its excellent heat resistance and chemical stability. Additionally, its performance can be readily manipulated by modifying its functional groups, rendering it highly attractive to various industries. However, extreme climate changes have necessitated an expansion of the operating temperature range and lifespan of ACM products. This requires the optimization of both the compounding process and functional-group design. Hence, we investigated the relationship between the cross-linking system and mechanical properties of an ACM with a carboxylic cure site. The crosslink density is determined by chemical kinetics according to the structure of additives, such as diamine crosslinkers and guanidine accelerators. This interaction enables the manipulation of the scotch time and mechanical properties of the compound. This fundamental study on the correlation analysis between cross-linking systems, physical properties, and storage stability can provide a foundation for material research aimed at satisfying the increasingly demanding service conditions of rubber products.

• Proceedings of the IEEK Conference
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• 2004.08c
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• pp.460-462
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• 2004

The control of the data retention time is a main issue for realizing future high density dynamic random access memory. There are several leakage current mechanisms in which the stored data disappears. The mechanisms of data disappear is as follow, 1 )Junction leakage current between the junction, 2) Junction leakage current from the capacitor node contact, 3)Sub-threshold leakage current if the transfer transistor is affected by gate etch damage etc. In this paper we showed the plasma edge damage effect to find out data retention time effectiveness. First we measured the transistor characteristics of forward and reverse bias. And junction leakage characteristics are measured with/without plasma damage by HP4145. Finally, we showed the comparison TRET with etch damage, damage_cure_RTP and hydrogen_treatment. As a result, hydrogen_treatment is superior than any other method in a curing plasma etch damage side.

• Macromolecular Research
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• v.9 no.1
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• pp.37-44
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• 2001

A premixing effect for the properties of carbon black-filled rubber compounds was investigated using biblends of natural rubber (NR), styrene-butadiene rubber (SBR), and butadiene rubber (BR). Degree of mixing of the biblends was controlled by preblending time of 0.0, 2.5, and 5.0 min. Mooney viscosities of the compounds decreased by increasing the preblending time. Of three carbon black-filled compounds of NR/SBR, NR/BR, and SBR/BR compounds, only the SBR/BR blends showed a specific cure characteristics depending on the preblending time. For the bound rubber composition, the NR content was higher than SBR and BR. The difference in the rubber composition ratio of the bound rubber became smaller with increasing the preblending time. Physical properties of the vulcanizates such as hardness, modulus, tensile property, abrasion loss, and tans were also compared. Differences in properties of the compounds were discussed with miscibility of the dissimilar rubbers and degree of mixing.

• Elastomers and Composites
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• v.31 no.5
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• pp.347-352
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• 1996

A natural rubber was blended with a butadiene rubber with different ratios. A natural rubber, along with three different blends, its ratio varying from 10 to 15 to 20 weight %, were prepared and tested. It was found that inclusion of the butadiene rubber increased cure time, compared to the natural rubber. It is speculated that increased free volume due to the inclusion of butadiene rubber contributed to this effect. Furthermore, inclusion of butadiene rubber led to increase hardness of a sphere, and as a result, the extent of rebound increased sharply.

• Proceedings of the KIEE Conference
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• 1990.07a
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• pp.275-278
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• 1990

This study investigated electrical characteristics of solid and liquid epoxy rosins by measuring dielectric breakdown and dielectric loss when epoxy resins were exposed to a mixing cure, i.e., Fusion Blend Method. It was found that mixing epoxy resins were superior to dielectric breakdown and has shorter curing time compare with those of pure liquid epoxy resins.

• Proceedings of the KSR Conference
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• 2000.05a
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• pp.143-150
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• 2000

Like conventional railways, improving running performance of vehicle in curve is more effective than improving maximum speed to reduce traveling time. But some vehicles have problems concerning running performance in cure because of insufficient study for our conventional railway characteristics. So, these problems brought about increasement of maintenance cost. This study was started to deliberate several plans to solve problems concerning running performance in curve. Some modifications of primary suspension and tests were carried out to improve curve negotiation. Here, we describe some results.

• Structural Engineering and Mechanics
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• v.5 no.6
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• pp.705-713
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• 1997

The residual thermal stresses at the interface corner between the elastic fiber and the viscoelastic matrix of a two-dimensional unidirectional laminate due to cooling from cure temperature down to room temperature were studied. The matrix material was assumed to be thermorheologically simple. The time-domain boundary element method was employed to investigate the nature of stresses on the interface. Numerical results show that very large stress gradients are present at the interface corner and this stress singularity might lead to local yielding or fiber-matrix debonding.