• Title/Summary/Keyword: compounding

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Determination of Analytical Method for the Insecticide Clothianidin and its Metabolites in Soil and Surface Water (토양 및 토양수 중 살충제 Clothianidin 및 대사산물 잔류분석법 확립)

  • Choi, Young-Joon;Kwon, Chan-Hyeok;Han, Byung-Soo;Lee, Young-Deuk
    • Korean Journal of Environmental Agriculture
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    • v.33 no.2
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    • pp.69-77
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    • 2014
  • BACKGROUND: The purpose of this study was to investigate the effects of clothianidin on the soil in terms of clothianidin dissipation and degradation to evaluate its safety in order to provide an analytical foundation for clothianidin and the 5 metabolites related to it. METHODS AND RESULTS: High-performance liquid chromatography(HPLC) was used to separate clothianidin and its metabolites in this study. In soil, after suppressing dissociation-proned ions with weak alkalic $NH_4OH$ and extracting the metabolites with methanol, clothianidin, Methylaminoimidazole(MAI), Methylnitroguanidine(MNG), Thiazolylmethylurea(TZMU) and Thiazolylnitroguanidine(TZNG). Thiazolylmethylguanidine(TMG) were extracted with the addition of neutral $NH_4OAC$ to increasing the intensity of ions. Compounding elements were separated by using Hydrometrix ($ChemElut^{TM}$) and ion-exchanging Solid-phase extraction(SPE) Strong cation-exchanger(SCX) and C18 were used. The recovery rates of clothianidin and 5 metabolites in soil and water ranged from 87.4% to 104.3%. A standard deviation of our analysis for the soil and water samples were less than 5%. CONCLUSION: Well accepted detection limits for clothianidin and 5 metabolites in soil samples based on a dissipation analysis is 0.005 mg/kg and 0.001 mg/L in water samples. The dissipation concentration of this study was decided to be enough to evaluate the dissipation levels of clothianidin and its metabolites.

Preparation of Mg(OH)2-Melamine Core-Shell Particle and Its Flame Retardant Property (멜라민이 코팅된 수산화마그네슘 입자의 제조와 그 복합입자의 난연특성)

  • Lim, Hyung-Mi;Yoon, Joon-Ho;Jeong, Sang-Ok;Lee, Dong-Jin;Lee, Seung-Ho
    • Korean Journal of Materials Research
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    • v.20 no.12
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    • pp.691-698
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    • 2010
  • Magnesium hydroxide-melamine core-shell particles were prepared through the coating of melamine monomer on the surface of magnesium hydroxide in the presence of phosphoric acid. The melamine monomer was dissolved in hot water but recrystallized on the surface of magnesium hydroxide by quenching to room temperature in the presence of phosphoric acid. The core-shell particle was applied to low-density polyethylene/ ethylene vinyl acetate (LDPE/EVA) resin by melt-compounding at $180^{\circ}C$ as flame retardant. The effect of magnesium hydroxide and melamine content has been studied on the flame retardancy of the core-shell particles in LDPE/EVA resin according to the preparation process and purity of magnesium hydroxide. Magnesium hydroxide prepared with sodium hydroxide rather than with ammonia solution revealed higher flame retardancy in core-shell particles with LDPE/EVA resin. At 50 wt% loading of flame retardant, core-shell particles revealed higher flame retardancy compared to that of the exclusive magnesium hydroxide in LDPE/EVA composite, and it was possible to satisfy the V0 grade in the UL-94 vertical test. The synergistic flame retardant effect of magnesium hydroxide and melamine core-shell particles was explained as being due to the endothermic decomposition of magnesium hydroxide and melamine, which was followed by the evolution of water from the magnesium hydroxide and porous char formation due to reactive nitrogen compounds, and carbon dioxide generated from melamine.

Carbon Nanotubes Reinforced Poly(ethylene terephthalate) Nanocomposites (탄소나노튜브로 강화시킨 Poly(ethylene terephthalate) 나노복합재료)

  • Choi, Soohee;Jeong, Youngjin
    • Polymer(Korea)
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    • v.38 no.2
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    • pp.240-249
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    • 2014
  • Multi-walled carbon nanotube (MWNT) reinforced poly(ethylene terephthalate) (PET) composites are studied. To increase the interfacial interactions between PET and MWNTs, the MWNTs are functionalized with bishydroxy-ethylene-terephthalate (BHET). The functionalized MWNTs are melt blended into PET matrix using a twin screw extruder. The amount of MWNTs loaded in PET matrix ranges from 0.5 to 2.0 wt%. After compounding and spinning, the filaments are post-drawn and annealed. To verify the chemical modifications of carbon nanotubes, Raman, $^1H$ NMR, XPS, TGA and FE-SEM are used. The nanocomposites are also analyzed with DSC, TGA, and UTM. These tests show that crystallization temperature and thermal degradation temperature increase due to the functionalized MWNTs. Also, tensile test shows that yield strength and toughness increase more than 30% with addition of only 1 wt% of MWNTs. These results show that the introduction of BHET onto the MWNTs is a very effective way in manufacturing MWNT/PET composite.

Evaluation of the Optimum Band When Estimate the Density of Chlorophyll-a In Landsat ETM+ Image (Landsat ETM+ 영상에서 클로로필a 농도 추정시의 최적밴드 평가)

  • Choi, Seung-Pil;Park, Jong-Sun
    • Journal of Korean Society for Geospatial Information Science
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    • v.14 no.2 s.36
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    • pp.63-68
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    • 2006
  • Although it is more recommended to use satellite images for an accurate understanding of the natural environment over a large area, what should proceed obtaining such satellite images is to make basic model equations based firmly upon the on-land experiments and field experiments. It may be more accurate and objective to investigate correlations between satellite images and actual water quality factors obtained for the same area. Thus, this study was conducted in order to determined which band of Landsat ETM+ images is appropriate to estimate the density of chlorophyll-a in a closed laboratory without atmospheric interference, using pure water and sea water. As a result of this study, it was found that the best band that exhibited the highest degree of correlations among the compounded bands rated (B3-B4)/B2 in pure water and (B2+B4)/B3 in sea water. The correlation coefficient here is 0.9747 and 0.9892 respectively. Thus, compounding this band ran be quite useful for estimation density of Chlorophyll-a using Landsat ETM+ image data.

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Development of Standard Body Measurement for Elderly Women(II) - Somatotype Classification & Standard Body Measurement - (노년 여성의 표준 신체치수 설정에 관한 연구(제2보) -체형분류와 표준 신체치수-)

  • 이정임;주소령;남윤자;류영실
    • Journal of the Korean Society of Clothing and Textiles
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    • v.28 no.3_4
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    • pp.377-386
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    • 2004
  • This report is the second study to develop the standard tables of body measurements to be used for improving the fit of garments and patterns for women aged 60 and older. The purpose of this study is to suggest the new sizing system proper to the women aged 60 and older by classifying their somatotype and developing the standard tables of body measurements for each somatotype. The data are the anthropometric measurements of 329 women aged 60 and older measured in 2001 and the 1997 National Somatometry Survey data. The major contents of this study are as follows. The applicability of KS K 0051 and ISO 3637 sizing systems to the women aged 60 and older was investigated by analyzing the distribution of height and drop index the difference of hipgirth and bustgirth. In this result, we certified the two sizing systems were not so proper to elderly women and the new sizing system proper to them was required. So, we classified the somatotype of the women aged 60 and older to 3 groups, 135cm$\leq$H(height)<145cm, 145cm$\leq$H<155cm, 155cm$\leq$H<165cm by height and classified to 3 groups, -4cm$\leq$D(drop)<16cm, -4cm$\leq$D<4cm, -l6cm$\leq$D<-4cm by drop index, and we suggested more proper sizing system for women aged 60 and older by compounding height and drop groups. We also developed the standard tables of body measurements every bustgirth groups of 9 somatotypes. We expect the standard tables of body measurements to applicate to manufacture clothing for elderly women.

Development of a Reflective Collaborative Work System for e-Learning Contents Development (e-Learning 콘텐츠 개발을 위한 성찰적 협력작업시스템 개발)

  • Cho Eun-Soon;Kim In-Sook
    • The Journal of the Korea Contents Association
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    • v.6 no.3
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    • pp.108-115
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    • 2006
  • e-Learning contents are composed of compounding multimedia data. It requires many professionals in contents development stage. The process of e-learning contents development can be seen as a collaborative work. In the perspective of a collaborative work process, the whole process of e-learning contents development would be regarded as collaborative work process for each participant as well as for whole group members. Most of collaborative works in contents development field are widely distributed. Members of work groups require workspaces for sharing information and communicating each other. In addition to workspaces, it also needs to support collaborative reflection such as planning for collaborative work and monitoring for work process. This paper is intended to develop the reflective collaborative work system for e-Learning contents development in order to support the systemic process of e-learning contents development. The reflective collaborative work system is composed of four supportive parts: work flow management, personal workspace, collaborative workspace, and collaborative reflection.

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Development and Application of a Novel Tomato Sauce Using Natural Seasoning (천연조미료 이용 토마토소스 개발 및 적용)

  • Kim, Jung-Hee;Lee, Young-Mee;Joo, Na-Mi;Choi, Kyung-Suk;Sohn, Cheong-Min;Park, Sang-Hyun;Chung, Chung-Soon;Do, Hae-Ja;Ryou, Hyun-Joo
    • Korean journal of food and cookery science
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    • v.26 no.2
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    • pp.138-145
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    • 2010
  • This study was conducted to develop a novel tomato sauce using natural seasoning. The data was analyzed using SPSS for Windows (version 14.0). Two factors of the tomato sauce were varied was tomato paste and sugar. Nine tomato sauces were produced with various compounding ratios of tomato paste and sugar. The color, viscosity and sensory evaluations of the nine tomato sauces were determined. Items examined in the sensory evaluation were color, sweetness, viscosity and overall quality. Sweetness($4.44{\pm}1.36$), viscosity($5.16{\pm}1.28$) and overall quality($4.68{\pm}1.11$) of the tomato paste 340g and sugar 100 g sample got highest scores. Therefore, this composition was used as tomato spaghetti sauce. Tomato spaghetti sauce using a natural tomato sauce and artificial tomato sauce was prepared and subjected to a sensory evaluation. Items included in the sensory evaluation were taste, flavor, harmony, overall quality. In this analysis, all sensory item scores of the tomato spaghetti sauce using natural seasoning were significantly higher than when artificial seasoning was used. Therefore, the potential of commercialization of tomato sauces using natural seasoning was confirmed.

A Wind Tunnel Study on the Static Stability Characteristics of Light Sport Aircraft (스포츠급 경항공기의 정안정 특성 풍동시험 연구)

  • Kim, Jong-Bum;Jang, Young-Il;Kwon, Ky-Beom;Chung, Hyoung-Seog;Cho, Hwan-Kee;Kim, Sang-Ho;Lee, Jae-Woo
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.40 no.8
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    • pp.711-717
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    • 2012
  • During the conceptual design phase of a light sport aircraft, the wind tunnel tests were conducted to investigate the static stability of newly-designed configuration. The 1/5 scale-down wind tunnel model consisted of fuselage, main wing, vertical tail and horizontal tail. The main wing and tails were able to be attached or detached from the fuselage. The aerodynamic forces and moments acting on the 6 different configurations compounding each component were measured by using the internal balance system and their static stability derivatives were derived. With these experimental data, the baseline lift and drag characteristics as well as the effects of each component to the longitudinal, directional and lateral static stability were quantitatively analyzed.

Characterization and Fatigue Life Evaluation of Rubber/Clay Nanocomposites (고무-점토 나노복합체 물성 및 피로내구성 평가)

  • Woo, Chang-Su;Park, Hyun-Sung;Joe, Deug-Hwan;Jun, Young-Sig
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.35 no.10
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    • pp.1199-1203
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    • 2011
  • Nanocomposites were prepared through the compounding of rubber and clay. Measurements of the static and dynamic mechanical properties of different compositions over a temperature range $70-100^{\circ}C$ showed that the mechanical properties of these rubber/clay nanocomposites are superior to those of existing rubber materials. In this study, by using the parameter of the maximum Green.Lagrange strain appearing at certain locations, the relationship between fatigue life and maximum Green.Lagrange strain, and the correlations between test-piece tests and bench tests of actual rubber components are proved. In order to predict the fatigue life of rubber components at the design stage, a simple procedure of life prediction is suggested. The predicted fatigue lives of the rubber engine mounts agree fairly well with the fatigue lives determined experimentally.

$\alpha$ Scaling Parameter Optimization On Watermarking Using Autostereogram (오토스테레오그램을 이용한 워터마킹에서 $\alpha$스켈링 파라미터 최적화)

  • 허덕규;이인정;김성옥
    • Journal of Internet Computing and Services
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    • v.2 no.4
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    • pp.101-109
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    • 2001
  • In recent year, the use of digital picture information and general picture information has been increased, However, numerous copyright infringement and pirate copy of picture information through Internet and CD-ROM happen very often, As a result, several methods of watermarking have been presented to solve and verify distortion of the original data, In addition, watermark data have been suggested to resolve the vastness of the original data, Watermarking methods are often used to protect the right of ownership of a copyright, However, these Watermarking methods have brought the obscurity of recognition caused by the complexity of verification procedure and the increase of magnitude computation occurrence, This paper mainly mentions about the local optimization of scaling parameter, the maximization of hiding of Watermark information and maximization of watermark information in case of restoration that determine the amount of inserted information which is used for preventing distortion and transformation of the original data caused by insertion and hiding of Watermark information on compounding Autostereogram into JPEG picture information.

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