• Title/Summary/Keyword: coating quality

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New MOD solution for the preparation of high $J_c$ REBCO superconducting films (고특성 REBCO 초전도 박막 제조를 위한 새로운 MOD 전구 용액 제조)

  • Kim, Byeong-Joo;Hong, Gye-Won;Lee, Hee-Gyoun
    • Proceedings of the KIEE Conference
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    • 2005.07c
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    • pp.2001-2003
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    • 2005
  • Various organic acid were used in order to prepare new metalorganic deposition solution for high quality $REBa_2Cu_3O_{7-{\delta}}$ (RE=Y, Eu, Gd) films. Prepared fluorine free MO precursor solution was coated on single crystal (001) $LaAlO_3$ (LAO) by dip coating method. Processing parameters such as oxygen partial pressure, water vapor, ramping rate and pyrolysis temperature etc havebeen controlled in order to make high $J_c$ films with a good epitaxial relationship with substrate. 0.5 micron-thick film was obtained by single coating and no crack appeared after calcination. Oxygen partial pressure was varied in the range of $100{\sim}1,000 ppm$ and conversion heat treatment was carried out at the temperature of $725{\sim}765^{\circ}C$. A critical transition temperature $(T_{c0})$ of 90K and a critical transport current density $(J_c)$ of $>0.5MA/cm^2$ (77K and self-field) were demonstrated for the YBCO film on (001) oriented LAO substrates with a thickness of 0.5 micron. $I_c$ was determined by utilizing a transport measurement. SEM and XRD investigations confirmed that films were grown epitaxially onto the LAO single crystal substrate. It is thought that fluorine free new MOD solutionis promising for high quality REBCO films.

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Effect of HF and Plasma Treated Glass Surface on Vapor Phase-Polymerized Poly(3,4-ethylenedioxythiophene) Thin Film : Part II

  • Lee, Joonwoo;Kim, Sungsoo
    • Journal of Integrative Natural Science
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    • v.6 no.4
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    • pp.215-219
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    • 2013
  • In this study, in order to investigate how consecutive treatments of glass surface with HF acid and water vapor/Ar plasma affect the quality of 3-aminopropyltriethoxysilane self-assembled monolayer (APS-SAM), poly(3,4-ethylenedioxythiophene) (PEDOT) thin films were vapor phase-polymerized immediately after spin coating of FeCl3 and poly-urethane diol-mixed oxidant solution on the monolayer surfaces prepared at various treatment conditions. For the film characterization, various poweful tools were used, e.g., FE-SEM, an optical microscope, four point probe, and a contact angle analyzer. The characterization revealed that a well prepared APS-SAM on a glass surface treated with water vapor/Ar plasma is very useful for uniform coating of FeCl3 and DUDO mixed oxidant solution, regardless of HF treatment. On the other hand, a bare glass surface without APS-SAM but treated with HF and water vapor/Ar plasma generally led to a very poor oxidant film. As a result, PEDOT films vapor phase-polymerized on APS-SAM surfaces are far superior to those on bare glass surfaces in the quality and electrical characteristics aspects.

Cause of Surface voids in Concrete Attached to an Aluminum Form, and Measures for Prevention

  • Noh, Sang-Kyun;Lee, Seung-Hoon;Han, Cheon-Goo
    • Journal of the Korea Institute of Building Construction
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    • v.13 no.5
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    • pp.457-464
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    • 2013
  • Traditionally, the material used for the form in reinforced concrete construction has been wood or steel. But recently, aluminum forms have been widely used in wall structures such as apartment buildings. Aluminum is light, easy to handle, and economically advantageous, but the hydrogen gas created due to its reaction with the alkali component in concrete gives rise to air pockets on the concrete's surface, and deteriorates the surface's finishability. In this research, to determine the influence of aluminum material on concrete, the cement paste W/C and its chemical reactivity in alkali and acid solution were analyzed. As a prevention plan, the influence of the number of applications of calcium hydroxide and various surface coating materials was analyzed. Through the analysis, it was found that the surface voids on the aluminum form are the result of the reaction of hydrogen gas with an alkali such as $Ca(OH)_2$. This can be prevented by the surface treatment of $Ca(OH)_2$, separating material and coating material. However, poor surface form and damages to the form are expected to cause quality degradation because of the aluminum-concrete interaction. Therefore, thorough surface treatment, rather than the type of separating material or coating material, is considered the most important target of management.

Optimal Design of Optical Filter Recognizing Financial Account with Multiple Attribute Using Analytic Hierarchy Process (계층적 분석 과정을 이용한 다중 속성의 금융통장 인식용 광학 필터의 최적 설계)

  • Yu, Hyeung Keun;Lee, Kang Won
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.27 no.6
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    • pp.407-416
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    • 2014
  • Five factors are identified, which affect the performance of optical filter: 1) type of optical glass, 2) existence of Fe, 3) photo pic coating type, 4) coating form, and 5) coating thickness. If we consider all the levels of five factors, there are 360 possible candidates. We determined five evaluation criteria, which can be used to evaluate possible candidates. For the performance measures we selected white-state avearge voltage, black-state average voltage, and black-state error rate. And we added economic criterion and quality and maintenance criterion. Through the two-step statistical analysis of white-state avearge voltage, black-state average voltage, and black-state error rates, we selected final four candidates. Based on the five criteria we finally determined optimal optical filter using AHP.

Effect of Coating Materials on Surface Layer Structures of Austenitic Stainless Steel Castings in Evaporative Pattern Process (소실모형 주조법에서 도형제가 오스테나이트 스테인레스강 주물의 표면층조직에 미치는 영향)

  • Kim, Ji-Youn;Cho, Nam-Don
    • Journal of Korea Foundry Society
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    • v.15 no.6
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    • pp.604-615
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    • 1995
  • Austenitic stainless steel castings using expandable polystylene(referred to hereafter as EPS) patterns are often affected by distinctive defects associated with incomplete decomposition of the EPS as the molds are filled with metal. The quality of the castings, with particular reference to carbon pick-up in austenitic stainless steel is further influenced to a significant extent by such factors as reduced pressure, the additive by adding $Na_2CO_3$ in coating. The steel composition and microstructure were examined at the surface layer of castings, at depths of 1mm, by taking successive layers of swarf and analysis. In experiments, the carburizing atmosphere was neutralized, showing that the coating performed efficiently by decomposing almost instantly on heating and liberating $CO_2$. The upper parts of castings obtained using EPS patterns were slightly higher in carbon pick-up than other parts. Comparing the 316L and 304 stainless steel castings, qualitative and quantative differences could be found between the carbon pick-up behaviours as influence of the carbon content and alloying elements. Carbide former such as Cr makes carbon more soluble in the steel. This must make carbon pick-up in the surface layer but at the same time richer in carbon especially in the 304 stainless steel castings.

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Design and Properties Related to Anti-reflection of 1.3μm Distributed Feedback Laser Diode (1.3μm 분포 괴환형 레이저 다이오드의 무반사 설계 및 특성)

  • Ki, Hyun-Chul;Kim, Seon-Hoon;Hong, Kyung-Jin;Kim, Hwe-Jong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.3
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    • pp.248-251
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    • 2009
  • We have investigated the effect of the quality of 1.3 um distributed feed back laser diode (DFB-LD) on the design of anti-reflection (AR) coatings. Optimal condition of AR coating to prevent internal feedback from both facets and reduce the reflection-induced intensity noise of laser diode was simulated with Macleod Simulator. Coating materials used in this work were ${Ti_3}{O_5}$ and $SiO_2$, of which design thickness were 105 nm and 165 nm, respectively. AR coating films were deposited by Ion-Assisted Deposition system. The electrical and optical properties of 1.3 um laser diode were characterized by Bar tester and Chip tester. Threshold current and slop-efficiency of DFB-LD were 27.56 mA 0.302 W/A. Far field pattern and wavelength of DFB-LD were $22.3^{\circ}(Horizontal){\times}24.4^{\circ}$ (Vertical), 1313.8 nm, respectively.

Characterization of microtip emitters based on titanium carbide-coated carbon nanotubes (티타늄 카바이드가 코팅된 탄소나노튜브 미세팁 이미터의 전계방출 특성 분석)

  • Kim, Young-Kwang;Kim, Jong-Pil;Park, Chang-Kyun;Park, Jin-Seok
    • Proceedings of the KIEE Conference
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    • 2008.07a
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    • pp.1218-1219
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    • 2008
  • Thin films (< 30 nm) of titanium carbide (TiC) are coated on carbon nanotubes (CNTs), which are directly grown on nano-sized ($\sim$ 500 nm in diameter) conical-type tungsten (W) tips, by employing an inductively coupled plasma-chemical vapor deposition (ICP-CVD) technique. Any modification in structural properties (such as length to diameter ratio, crystal quality, and growth behavior) of CNTs due to TiC-coating has been monitored by using high-resolution TEM, field-emission SEM, and Raman spectroscopy. Driving voltage for obtaining the same level of emission current in CNTs-emitter is significantly reduced by TiC-coating. It is also worthy of being noted that the degradation of emission current due to prolonged operation (up to 30 h) is remarkably suppressed by TiC-coating.

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Improvement of Optical 3D Scanner Performance Using Atomization-Based Spray Coating

  • Valinasab, Behzad;Rukosuyev, Maxym;Lee, Jason;Ko, Junghyuk;Jun, Martin B.G.
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.24 no.1
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    • pp.23-30
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    • 2015
  • The scanning quality can be influenced by reflective abilities of a surface. Transparency and glossiness of a surface can highly limit the scanning results. Various techniques have been developed to solve problems of reflective and transparent surfaces. As one of the most feasible and convenient solutions, a thin layer of coating with proper specifications is sprayed on surface for eliminating the problems of the surfaces. As the main goal is to keep the object geometry unchanged, then it is important to coat the surface with layers less than one micrometer in thickness. For this purpose, a newly designed atomization-based spray system has been developed and tested in sets of experiments to study its efficiency on scanning results while objects with the surface are in use. This paper presents the spray design process and then studies and compares the 3D scanning results of the surfaces coated with atomization-based and aerosol sprays.

Automatic Focusing Vision System for Inspection of Size and Shape of Small Hole (소형(1mm이하) hole의 형태 및 크기 측정을 위한 자동초점 비젼검사기)

  • Han, Moon-Yong;Han, Hern-Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.16 no.10
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    • pp.80-86
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    • 1999
  • Since the quality of the coated wires is in various applications dependant on the coating depth, accuracy of hole size of dies used for coating wires must be maintained precisely, in general within one micron. This paper proposes a new vision system which measures automatically the size and shape of small holes having diameters less than 1mm within an error limit of 1 micron. To quickly obtain the focused image, this paper proposes an estimation method of the camera position using only a couple of defocused hole images. It measures the distributions of light intensity around the image boundary and decides the direction and distance of a camera motion. The proposed system measures the size, shape distortion, inclination of the hole against the axis of the dies structure, to decides the acceptability of the dies for use. The proposed algorithm has been implemented using a cheap 640${\times}$480 image system and has shown an average size error of 1micron when measuring the dieses having 0.1mm to 1.0mm diameters. It can be applied to the inspection of the size and position of holes in PCB, too.

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Design Research of the Natural Leather using a Marbling Technique (I) (Marbling 기법을 응용한 천연가죽의 디자인 연구 (I))

  • Lee, Sang-Chul;Shin, Eun-Chul;Kim, Won-Ju;Park, Soo-Min
    • Textile Coloration and Finishing
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    • v.20 no.1
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    • pp.1-7
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    • 2008
  • The study has attempted to introduce a new coating than the conventional standardized method of spray, padding and roll coating. The study has focused on finding condition for separating water and organic layer in marble bath and surface effects according to kind of raw hide. It was found that dyestuff-free was to be used in water layer and the input amount of initial insoluble pigment to be added in marble bath should be adjusted following the change of surface area of the marble bath in order to get efficient marble effect while preventing coagulation of water and organic layers. Eventually, amorphous high value-added leather could be obtained treated in process other than the conventional standardized method. Even raw hides of low grades($C{\sim}E$ grades) could be processed into amorphous marble effect that could conceal or shield surface scratches by the colorant, which eventually eliminated necessity of using excessive amount of chemicals in the coating process leading to achieving high quality marble leather of natural look.