• Title/Summary/Keyword: coating defects

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Thickness measurements of a Cr coating deposited on Zr-Nb alloy plates using an ECT pancake sensor

  • Jeong Won Park;Bonggyu Ji;Daegyun Ko;Hun Jang;Wonjae Choi
    • Nuclear Engineering and Technology
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    • v.55 no.9
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    • pp.3260-3267
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    • 2023
  • Zr-Nb alloy have been widely used as fuel rods in nuclear power plants. However, from the Fukushima nuclear accident, the weakness of the rod was revealed under harsh conditions, and research on the safety of these types of rods was conducted after the disaster. The method of depositing chromium onto the existing Zr-Nb alloy fuel rods is being considered as a means by which to compensate for the weakness of Zr-Nb alloy rods because chromium is strong against oxidation at high temperatures and has high strength. In order to secure these advantages, it is important to maintain the Cr thickness of the rods and properly inspect the rods before and during their use in power generation. Eddy current testing is a typical means of evaluating the thickness of thin metals and detecting surface defects. Depending on the size and shape of the inspected object, various eddy current sensors can be applied. In particular, because pancake sensors can be manufactured in very small sizes, they can be used for inspections even in narrow spaces, such as a nuclear fuel assembly. In this study, an eddy current technique was developed to confirm the feasibility of Cr coating thickness evaluations. After determining the design parameters of the pancake sensor by means of a FEM simulation, a FPCB pancake sensor was manufactured and the optimal frequency was selected by measuring minute changes in the Cr-coating thickness using the developed sensor.

The discharge characteristic of Li ion doped MgO film in a flat fluorescent lamp structure

  • Ryu, Si-Hong;Lee, Seong-Eui;Ahn, Sung-Il;Choi, Kyung-Cheol
    • 한국정보디스플레이학회:학술대회논문집
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    • 2007.08b
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    • pp.1388-1390
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    • 2007
  • This paper investigates how various concentrations of lithium ion influence on crystallization of MgO in thin films formed by spin coating and an the discharge characteristic in a flat fluorescent lamp structure. The XRD results indicate $Li^+$ ion enhances the growth of MgO crystal in a spin coated thin film. The discharge property with the $Li^+$ ion doped MgO films show the lithium ion in MgO film clearly reduce the initial discharge voltages of test devices. Interestingly, the test panels with various doped MgO film have somewhat higher static memory margin of than that of pure-MgO owing probably to the pore structure of spin coated MgO films. The CL spectra, which confirm that the doping creates defects energy levels in the band gap of MgO, show the $F^+$ center is the main defects in doped MgO films.

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Phenomena of Hyperbolic Heat Conduction in the Hot Mold with an Inner Defect (내부결함이 있는 고온 금형에서의 쌍곡선형 열전도 현상)

  • Lee, Gwan-Su;Im, Gwang-Ok;Jo, Hyeong-Cheol;Kim, U-Seung
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.25 no.7
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    • pp.952-957
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    • 2001
  • In the glass forming process, the phenomena of hyperbolic heat conduction in the hot mold with an inner defect are studied analytically. It is shown that the temperature predicted by the parabolic model is underestimated compared to the one by the hyperbolic model. As the rmal wave is reflected from the area with defects and then arrives at the surface supplied by the heat flux, it is expected that there exists thermal shock in the materials. The area with defects is assumed to be adiabatic since its thermal conductivity is much lower compared to the one of the material. The results also indicate that the sudden temperature -jump in the mold surface can cause diverse problems such as glass defect (embryo mark, etc), oxidation of mold and coating, and change of material properties.

Analysis of Partial Discharge in High Voltage Motor Model Coils (고압전동기 모델 코일에서 부분방전 분석)

  • Kim, Hee-Dong
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.55 no.4
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    • pp.178-182
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    • 2006
  • Five model coils of 6.6 kV motor were manufactured with several defects. These stator coils have artificial defects such as void of groundwall insulation, removal of semi-conductive coating and damage of strand insulation. Epoxy-mica coupler(80 pF) was connected to five model coil terminals. The voltage applied to the coils was 3.81 kV, 4.76 kV, 6.0 kV and 6.6 kV, respectively. Partial discharge(PD) tests performed in the laboratory and shield room. Digital PD detector(PDD) and turbine generator analyzer(TGA) were used to measure PD activity. TGA summarizes each plot with two quantities such as the normalized quantity number(NQN) and the peak PD magnitude(Qm). The PD levels in pC were measured with PDD. PD patterns of model coils were indicated the internal and slot discharges. PD patterns are consistent with the result of measurement using PDD and TGA instruments. AC breakdown test was performed on five model coils in order to confirm the result of PD measurements. All the failures were located in a line-end coil at the exit from the core slot.

A Study on Zirconia/Metal.Functionally Gradient Materials by Sintering Method(1) (소결법에 의한 $ZrO_2/Metal$계 경사기능재료에 관한 연구(1))

  • 정연길;최성철
    • Journal of the Korean Ceramic Society
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    • v.31 no.3
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    • pp.321-329
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    • 1994
  • Functionally gradient materials(FGM), which have the continuous or stepwise variation in a composition and microstructure, are being noticed as the material that solves problems caused by heterogeneous interface of coating or joining. And these materials also expect new functions occured by gradient composition itself. Therefore, to examine possibility of thermal barrier materials, TZP/Mo·FGM and TZP/Ni·FGM were fabricated by sintering method. As to the sintered specimens, sintering shrinkage, relative density and Vicker's hardness in each composition were examined. The phenomena due to the difference of sintering shrinkage velocity during sintering process and the thermal stress induced through differences of thermal expansion coefficient in FGM were discussed. And the structure changes at interface and microsturcture of FGM were investigated. As a results, the difference of shrinkage between ceramic and metal was about 14% in TZP/Mo and 7% in TZP/Ni. The relative density and hardness were considerably influenced by metal content changes. Owing to unbalance of sintering shrinkage velocity between ceramic and metal, various sintering defects were occured. To control these sintering defects and thermal stress, gradient composition of FGM should be narrow. The microstructure changes of FGM depended on the ceramic or metal volume percents and were analogous to the theoretical design.

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Influence of Selective Oxidation Phenomena in CGLs on Galvanized Coating Defects Formation

  • Gong, Y.F.;Birosca, S.;Kim, Han S.;De Cooman, B.C.
    • Corrosion Science and Technology
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    • v.7 no.1
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    • pp.1-5
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    • 2008
  • The gas atmosphere in continuous annealing and galvanizing lines alters both composition and microstructure of the surface and sub-surface of sheet steel. The formation and morphology of the oxides of alloying elements in High Strength Interstitial Free (HS-IF), Dual Phase (DP) and Transformation-Induced Plasticity (TRIP) steels are strongly influenced by the furnace dew point, and the presence of specific oxide may result in surface defects and bare areas on galvanized sheet products. The present contribution reviews the progress made recently in understanding the selective formation of surface and subsurface oxides during annealing in hot dip galvanizing and conventional continuous annealing lines. It is believed that the surface and sub-surface composition and microstructure have a pronounced influence on galvanized sheet product surface quality. In the present study, it is shown that the understanding of the relevant phenomena requires a combination of precise laboratory-scale simulations of the relevant technological processes and the use of advanced surface analytical tools.

Polysulfone/nanocomposites mixed matrix ultrafiltration membrane for the recovery of Maillard reaction products

  • Basu, Subhankar;Mukherjee, Sanghamitra;Balakrishnan, Malini;Deepthi, M.V.;Sailaja, R.R.N.
    • Membrane and Water Treatment
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    • v.9 no.2
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    • pp.105-113
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    • 2018
  • Maillard reaction products like melanoidins present in industrial fermentation wastewaters are complex compounds with various functional properties. In this work, novel ultrafiltration (UF) mixed matrix membrane (MMM) composed of polysulfone (PSF) and nanocomposites was prepared through a phase inversion process for the recovery of melanoidins. Nanocomposites were prepared with acid functionalized multiwalled carbon nanotubes (MWCNTs) as the reinforcing filler for chitosan-thermoplastic starch blend. Higher nanocomposites content in the PSF matrix reduced the membrane permeability and melanoidins retention indicating tighter membrane with surface defects. The membrane surface defects could be sealed with dilute polyvinyl alcohol (PVA) solution. The best performing membrane (1% nanocomposites in 18% PSF membrane sealed with 0.25% PVA coating) resulted in uniform melanoidins retention of 98% and permeability of 3.6 L/m2 h bar over a period of 8h. This demonstrates a low fouling PSF membrane for high melanoidins recovery.

Effect of Evaporative Pattern on the Surface Layer Structures of Carbon Steel and Gray Iron Castings. (소실모형이 탄소강 및 회주철 주물의 표면층 조직에 미치는 영향)

  • Kim, Ji-Youn;Cho, Nam-Don
    • Journal of Korea Foundry Society
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    • v.12 no.4
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    • pp.305-316
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    • 1992
  • Steel and iron castings made with expandable polystylene (referred to hereafter as EPS) patterns are often affected by distinctive defects associated with incomplete decomposition of the EPS as the molds are filled with metal. The effects of practical factors on carbon pick-up were investigated on the specimens, by taking successive layers of swarf and analysis, whereas the lustrous carbon is determined by using combustion analysis. The quality of the castings, with particular reference to carbon pick-up in low carbon steel and lustrous carbon on gray iron, is further influenced to a significant extent by such practical factors as reduced pressure, the pouring temperature, the density of EPS pattern, the additive in coating and in pattern and the casting thickness. The rate at which carbon pick-up and lustrous carbon deposites are formed can be reduced by reducing the density of the pattern and also reducing pressure, especially by adding $Na_2CO_3$ in coating and in pattern to promote $CO_2$ evolution. The upper parts of castings obtained using EPS patterns are slightly higher in carbon pick-up and in lustrous carbon than other parts.

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Finite Element Analysis of Deformation Behavior During ECAP for an Aluminum Alloy Composite Model containing a SiC Particle and Porosities (강화상과 기공이 포함된 금속기지 복합재 모델의 ECAP 거동에 대한 유한요소해석)

  • Lee, Sung-Chul;Han, Sang-Yul;Kim, Ki-Tae;Hwang, Sang-Moo;Huh, Lyun-Min;Chung, Hyung-Sik
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.6
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    • pp.739-746
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    • 2004
  • The plastic deformation behavior of an aluminum alloy containing a particle and porosities was investigated at room temperature during equal channel angular pressing (ECAP). Finite element analysis by using ABAQUS shows that ECAP is a useful tool for eliminating residual porosity in the specimen, and more effective under friction condition. The simulation, however, shows considerably low density distributions for matrix near a particle at which many defects may occur during severe deformation. Finite element results of effective strains and deformed shapes for matrix with a particle were compared with theoretical calculations under simple shear stress. Also, based on the distribution of the maximum principal stress in the specimen, Weibull fracture probability was obtained for particle sizes and particle-coating layer materials. The probability was useful to predict the trend of more susceptible failure of a brittle coating layer than a particle without an interphase in metal matrix composites.

Risering of Steel Castings in Vacuum Molding Process (진공흡입주형 주조법에서 주강의 압탕 방안 설계)

  • Kang, Bok-Hyun;Kim, Ki-Young;Kim, Myung-Han;Hong, Young-Myung
    • Journal of Korea Foundry Society
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    • v.27 no.2
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    • pp.88-94
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    • 2007
  • General criteria for the risering design of steel castings and commercial codes for the flow and solidification analysis were used to design the optimized risering in V-process. Three type of specimens were chosen including thin plates and a thick disc. Sided riser installed in the front of a plate casting was effective to prevent the shrinkage defects and to increase the casting yield ratio. Exothennic sleeve and chill were also effective. It was possible to apply the general criteria for the risering design of steel castings to V-process. Temperature of a mold surface was expected to rise over $1,000^{\circ}C$ in the temperature calculation considering radiation effect of molten metal in the mold. Since weakening temperature of the vinyl used in V-process is about $70^{\circ}C$, it should be emphasized that a proper coating of the vinyl film is necessary to prevent the possibility of burning out of the vinyl by the molten metal.