• 제목/요약/키워드: coated tube

검색결과 139건 처리시간 0.021초

기능성 미분말의 제조공정에 관한 연구: II. 초임계 분출법에 의한 입자 코팅 (Preparation process of functional particles: II. Particle coating by rapid expansion of supercritical fluid solutions)

  • 류완원;김영도;신건철
    • 한국결정성장학회지
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    • 제8권4호
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    • pp.673-676
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    • 1998
  • 초임계 분출법(RECC)을 미립자 코팅에 이용하였다. 본 실험은 반응관 중심부에 위치한 노즐을 갖고 있는 유동층 내부에서 수행하였다. 핵입자로는 glass beads(500~590$\mu$m, 74$\mu$149$\mu$m)와 brilliant blut로 피복된 glass beads의 두 종류를 사용하였다. paraffin이 용해된 초임계 $CO_2$는 공기에 의해 유동중인 유동층 내부 노즐을 통해 분무시켰다. 핵입자 표면에 코팅물질이 피복됨을 SEM과 FT-IR에 의한 분석을 통하여 확인할 수 있었다. 코팅 전호 brilliant blue의 용출특성을 ABC로 조사한 결과 코팅입자의 용출특성이 향상되었음을 확인하였다.

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페닐기로 치환된 Methoxysilane의 CVD에 의한 실리카 분리막의 제조 및 $CO_2$ 분리 (Preparation of Silica Membrane by CVD of Phenyl-Substituted Methoxysilane and $CO_2$ Separation)

  • 김성수;서봉국;이윤복;박홍채;김태옥
    • 한국재료학회지
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    • 제11권7호
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    • pp.622-624
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    • 2001
  • The CVD film of methoxysilane derived from diphenyldimethoxysilane(DPDMS) was formed on the outer surface of a porous ${\alpha}-alumina$ support tube coated(via dipping-drying-calcining) with a boehmite sol(0.3 mol-Al/L). The resulting silica membrane($500^{\circ}C,\;P_{fe}\;=\;130\;Pa$) showed a permeance of $5.18{\times}10^{-8}\;mol\;{\cdot}\;m^{-2}{\cdot}s^{-1}{\cdot}Pa^{-1}\;for\;CO_2$ and a permselectivity of 13.35 for $CO_2/N_2\;at\;30^{\circ}C$.

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Gas Separation of Pyrolyzed Polymeric Membranes: Effect of Polymer Precursor and Pyrolysis Conditions

  • Jung, Chul-Ho;Kim, Gun-Wook;Han, Sang-Hoon;Lee, Young-Moo
    • Macromolecular Research
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    • 제15권6호
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    • pp.565-574
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    • 2007
  • In this study, five representative, commercially available polymers, Ultem 1000 polyetherimide, Kapton polyimide, phenolic resin, polyacrylonitrile and cellulose acetate, were used to prepare pyrolyzed polymer membranes coated on a porous {\alpha}-alumina$ tube via inert pyrolysis for gas separation. Pyrolysis conditions (i.e., final temperature and thermal dwell time) of each polymer were determined using a thermogravimetric method coupled with real-time mass spectroscopy. The surface area and pore size distribution of the pyrolyzed materials derived from the polymers were estimated from the nitrogen adsorption/desorption isotherms. Pyrolyzed membranes from polymer precursors exhibited type I sorption behavior except cellulose acetate (type IV). The gas permeation of the carbon/{\alpha}-alumina$ tubular membranes was characterized using four gases: helium, carbon dioxide, oxygen and nitrogen. The polyetherimide, polyimide, and phenolic resin pyrolyzed polymer membranes showed typical molecular sieving gas permeation behavior, while membranes from polyacrylonitrile and cellulose acetate exhibited intermediate behavior between Knudsen diffusion and molecular sieving. Pyrolyzed membranes with molecular sieving behavior (e.g., polyetherimide, polyimide, and phenolic resin) had a $CO_2/N_2$ selectivity of greater than 15; however, the membranes from polyacrylonitrile and cellulose acetate with intermediate gas transport behavior had a selectivity slightly greater than unity due to their large pore size.

필터방식을 이용한 이산화질소 및 호흡성 분진의 동시 측정 (Simultaneous NO2 and RSP Measurements Using Filtration Method)

  • 양원호;임성국;김문현
    • 한국환경보건학회지
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    • 제34권2호
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    • pp.148-152
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    • 2008
  • Coated filters were developed to replace the glass impinger methods that use reagent solutions. The purpose of this study was to simultaneously measure nitrogen dioxide ($NO_2$) and respirable suspended particles (RSP) by a filtration method with a cyclone connected to a pump. A first pre-filter for RSP and second filter for $NO_2$, which was soaked in a TEA (Triethanolamine) solution, were loaded into a filter cassette with a pump flow rate of 1.7 l/m. After sampling, the TEA soaked filter was removed from the cassette, placed in a large test tube (10 ml), mixed, and allowed time to develop. The absorbance (abs) of the diazo compound of the $NO_2$ and N-(1-Napthylethylenediamine dihydrochloride) in the color reagent was measured at 545 nm on a spectrophotometer. The collection efficiency(%) of $NO_2$ by each 3 filter soaked in TEA solution and used in the cyclone with a pump flow rate 1.7 l/m was $89{\pm}3%$ and the correlation coefficient between the true $NO_2$ concentration and that determined by the TEA soaked filters was 0.993(p<0.001).

Y211 및 BaCO$_3$ 분말로 Screen Printing 법을 이용한 Cu-sheath의 YBCO 후막 제조 (Fabrication of Cu-Sheathed YBCO Thick Films by Screen Printing Method Using $Y_2$BaCu$O_5$ and BaC$O_3$ Powders)

  • 김경진;한상철;한영희;박병삼;정년호;윤희중;오제명;최희락;성태현
    • Progress in Superconductivity
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    • 제5권2호
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    • pp.132-135
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    • 2004
  • We fabricated YBCO thick films by using a screen printing method with $Y_2$BaCuO$_{5}$(Y211) and BaCO$_3$ powders on Cu-substrate in $N_2$ atmosphere. Cu-sheathed YBCO thick film process is more simple and economic than YBCO coated conductor methods. The heat treatment is performed in the range of 860 - 875 $^{\circ}C$ for 5 min in the tube furnace of $N_2$ atmosphere. The flow rate of $N_2$ gas is fixed 60 $m\ell$/min. Microstructure and phases of thick films were investigated by optical microscope, X-ray diffraction(XRD) and SEM. At heat-treatment temperature, the thick films were partially melted by liquid reaction between CuO of oxidized copper substrate and the powders screen-printed on Cu-sheath. During the heat-treatment procedure, YBCO superconducting grains nucleate.e.

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유체의 흐름이 있는 엔진 흡기계용 직조관의 음향 임피던스 측정 및 전달손실 예측 (Measurement of acoustic impedance of porous woven hoses in engine intake systems in the presence of mean flow)

  • 이정권;박철민
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2002년도 춘계학술대회논문집
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    • pp.996-1000
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    • 2002
  • A porous tube, comprised of a resin-coated woven fabric has recently been used as an effective component for use in intake systems of internal combustion engines to reduce the intake roaring. For the prediction of the acoustic performance of an engine intake system with a porous woven hose, the acoustic wall impedance of the hose must be known. Because of its peculiar acoustical and structural characteristics, the accurate measurement of the wall impedance ofa porous woven hose is not easy. A new measurement technique is proposed herein, that is valid over the low to mid frequency ranges. The acoustics impedance is inversely estimated from an overdetermined set of measured pressure transmission coefficients for specimens of different lengths and the reflection coefficient of end termination. The method involves only one measurement, and, as a result, it is very simple. The measured TL for samples with arbitrary conditions, arbitrary porous frequency, arbitrary length, and arbitrary mean flow condition, are in reasonably good agreement with values predicted from curve-fitted impedance data.

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SPM을 이용한 반도체 포토레지스트 제거 공정 대체를 위한 DIW-$O_3$ 방식 세정기술 개발 (Development of the DIW-$O_3$ Cleaning Technology Substituted for the Semiconductor Photoresist Strip Process using the SPM)

  • 손영수;함상용
    • 연구논문집
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    • 통권33호
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    • pp.99-109
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    • 2003
  • Recently the utilization of the ozone dissolved de-ionized water(DIW-$O_3$) in semiconductor wet cleaning process and photoresist stripping process to replace the conventional sulfuric acid and hydro peroxide mixture(SPM) method has been studied. In this paper, we propose the water-electrode type ozone generator which has the characteristics of the high concentration and purity to produce the high concentration DIW-$O_3$ for the photoresist strip process in the semiconductor fabrication. The proposed ozone generator has the dual dielectric tube structure of silent discharge type and the water is both used to electrode and cooling water. Through this study, we obtained the results of the 10.3 wt% of ozone gas concentration at the oxygen gas of 0.5 [liter/min.] and the DIW-$O_3$ concentration of 79.5 ppm.. Through the photoresist stripping test using the produced DIW-$O_3$, we confirmed that the photoresist coated on the silicon wafer was removed effectively in the 12 minutes.

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스프링클러 구리배관의 공식 파손 억제 (Inhibition of Pitting Corrosion Failure of Copper Tubes in Wet Sprinkler Systems)

  • 서상희;서영준;이종혁;권혁상
    • Corrosion Science and Technology
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    • 제19권2호
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    • pp.89-99
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    • 2020
  • The inhibition of pitting corrosion failure of copper sprinkler tubes in wet sprinkler systems was studied. First, an apparatus and technology for removing air in the sprinkler tubes by vacuum pumping and then filling the tubes with water were developed. Using this apparatus and technology, three methods for inhibiting the pitting corrosion of the copper sprinkler tubes installed in several apartment complexes were tested. The first one was filling the sprinkler tubes with water bubbled by high-pressure nitrogen gas to reduce the dissolved oxygen concentration to lower than 2 ppm. In the second method, the dissolved oxygen concentration of water was further reduced to lower than 0.01 ppm by sodium sulfite. In the third method, the sprinkler tubes were filled with benzotriazole (BTAH) dissolved in water. The third method was the most effective, reducing the failure frequency of the sprinkler tubes due to pitting corrosion by more than 80%. X-ray photoelectron spectroscopy analyses confirmed that a Cu-BTA layer was well coated on the inside surface of the corrosion pit, protecting it from corrosion. A potentiodynamic polarization test showed that BTAH should be very effective in reducing the corrosion rate of copper in the acidic environment of the corrosion pit.

낙지 (Octopus minor)의 산란과 부화 (Spawning and Hatching of Octopus minor)

  • 김동수;김재만
    • 한국수산과학회지
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    • 제40권4호
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    • pp.243-247
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    • 2007
  • We investigated the reproductive behavior of Octopus minor, order Octopoda, class Cephalopoda under laboratory conditions. Each mature female octopus was kept in an aquarium with a plastic tube for shelter, and one mature male was introduced for the purpose of copulation. Before spawning, the female coated the roof of the shelter with a light-green material, upon which it then fixed its eggs one by one. This spawning behavior lasted 1 to 3 days. Fertilized females spawned 54 eggs on average, ranging from 21 to 112 eggs at 72 to 98 days after copulation. The attached eggs were 18.1-19.0 mm in length, 5.0-6.1 mm in width, and 0.30-0.38 g in weight. The mother octopods did not feed; they attended to the eggs by using their arms to rub the egg surfaces and used their funnel to blow sediments off of the eggs. At water temperatures of $20.9-21.5^{\circ}C$, the fertilized eggs hatched within 73 to 90 days after being spawned. The effective cumulative water temperature was $1,569-1,892^{\circ}C$. At the end of incubation, the body weight of the mother octopods was reduced to approximately 56% of the initial weight, and most mother octopods died soon after the young hatched.

광파이프 시스템의 조명기술 및 건축적 활용 연구 (A study on light pipe system technology and its application)

  • 신주영;김곤;김정태
    • KIEAE Journal
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    • 제9권1호
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    • pp.69-76
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    • 2009
  • The use of natural light can improve the quality of indoor environment and also occupants health. In recent years, with an increasing awareness of sustainable development, various innovative methods of integrating daylight into the building have been developed. One such device is the light pipe system. The light pipes are innovative daylighting system that allow the transmission of daylight into the hard-to-reach indoor space. The system consist of mainly three parts. First, a top collector which is mounted on the outside of the roof and gathers skylight and sunlight. Second, light-reflective tube which is coated with highly reflective mirror finish material to transmit the daylight into the diffuser. Third, a diffuser which is installed on the ceiling in the room and spread the daylight into the room. Light pipes have been widely used and researched in many countries such as Australia, America, Canada and Britain. However, despite the significant daylight potential, little work have been carried out in Korea compare to the other countries. In this study, recent lighting technology and application of light pipe system in both Korea and other countries have been compared. For the results, the benefits of each light pipe system and suitable application in Korea is also discussed.