• Composites Research
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• v.34 no.1
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• pp.47-50
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• 2021

In this paper, the Curing process for Epoxy Molding Compound (EMC) Package was developed by comparing the performance of the EMC/Cu Bi-layer package manufactured by the conventional Hot Press process system and Carbon Nanotubes (CNT) Heater process system of the surface heating system. The viscosity of EMC was measured by using a rheometer for the curing cycle of the CNT Heater. In the EMC/Cu Bi-layer Package manufactured through the two process methods by mentioned above, the voids inside the EMC was analyzed using an optical microscope. In addition, the interfacial void and warpage of the EMC/Cu Bi-layer Package were analyzed through C-Scanning Acoustic Microscope and 3D-Digital Image Correlation. According to these experimental results, it was confirmed that there was neither void in the EMC interior nor difference in the warpage at room temperature, the zero-warpage temperature and the change in warpage.

• Steel and Composite Structures
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• v.38 no.5
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• pp.533-545
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• 2021

What is desirable in engineering is to bring the engineering model as close to reality as possible while the simplicity of model is also considered. In recent years, several studies have been performed on nanocomposites but some of these studies are somewhat far from reality. For example, in many of these studies, the carbon nanotubes (CNTs) are assumed completely straight, flawless and uniformly distributed throughout the matrix but by studying nanocomposites, we find that this is not the case. In this paper, three steps have been taken to bring the presented models for nanocomposites closer to reality. One is that assuming the straightness of nanotubes is removed and the waviness is considered. Also, the nanotubes are not considered to be pristine and the influence of defect is included in accordance with reality. In addition, the approximation of uniform distribution of nanotubes is ignored and according to experimental observations, the effect of nanotube aggregation is considered. As far as we know, this is the first study on these three topics together in an article. Moreover, we also include the size effects in our models for nanocomposites. To show the accuracy of our models, our results are calibrated with experimental results and compared with theoretical model. For numerical examples, we present the buckling behaviors of nanocomposites including the size effects using nonlocal theory and compare the results of our models with the results of models with above-mentioned approximations.

• Particle and aerosol research
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• v.6 no.2
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• pp.61-67
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• 2010

In this paper, we describe a new method to form polymer thin films, in which carbon nanotubes (CNTs) are homogeneously distributed so that they can strengthen the mechanical property of resulting polymer film. To do so, we first homogeneously mixed CNTs with polymer in a DMF solvent. With the assistance of ultrasonic nebulizer, the polymer/CNT solution was then aerosolized into micro-sized droplets and finally turned into solidified polymer/CNT composite particles by gas-phase drying process. As the results of SEM and TEM analysis, CNTs were found to be homogeneously immobilized in the polymer matrix particles due to rapid drying process in the gas phase. For comparison purpose, (i) the polymer/CNTs composite particles prepared by aerosol processing method and (ii) polymer/CNTs sheets prepared by simple solution-evaporation method were employed to form polymer/CNTs composite thin films using a hot press. As the result, the aerosol processing of composite particles was found to be a much more effective method to form homogeneously distributed-CNTs in the polymer matrix thin film.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.56 no.4
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• pp.739-744
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• 2007

In this paper, we have investigated mechanical and chemical properties by changing the content of carbon nanotube, which is component part of semiconductive shield in underground power transmission cable. Specimens were made of sheet with the eight of those for measurement. The condition of specimens was a solid sheet. Chemical properties of specimens was measured by FT-ATR (Fourier Transform Attenuated Total Reflectance). Stress-strain of specimens was measured by TENSOMETER 2000. A speed of measurement was 200[mm/min], ranges of stress and strain were 400[Kgf/Cm] and 600[%]. We could observe (unctional group (C=O, carbonyl group) of specimens through FT-ATR. From these experimental result, the concentration of functional group [C=O] was high accor야ng to increasing the content of carbon nanotube. We could know CNT/EEA was excellent more than other specimens from above experimental results. In Addition, the elongation ratio was decreased, and yield strength was increased according to increasing the content of carbon nanotube. Also, from these experimental result, we could know that a small amount of CNT/EEA has a excellent mechanical and chemical properties.

• Advances in aircraft and spacecraft science
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• v.5 no.6
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• pp.633-652
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• 2018

The present paper focuses on the development of a model for simulating the thermoelectric behavior of CNTs/CFRP Organic Matrix Composite (OMC) laminates for aeronautical applications. The model is developed within the framework of the thermodynamics of irreversible processes and implemented into commercial ABAQUS Finite Element software and validated by comparison with experimental thermoelectric tests on two types of composites materials, namely Type A with Carbon Nanotubes (CNT) and Type B without CNT. A simplified model, neglecting heat conduction, is also developed for simplifying the identification process. The model is then applied for FEM numerical simulation of the thermoelectric response of aircraft panel structures subjected to electrical loads, in order to discuss the potential danger coming from electrical solicitations. The structural simulations are performed on quasi-isotropic stacking sequences (QI) $[45/-45/90/0]_s$ using composite materials of type A and type B and compared with those obtained on plates made of metallic material (aluminum). For both tested cases-transit of electric current of intermediate intensity (9A) and electrical loading on panels made of composite material-higher heating intensity is observed in composites materials with respect to the corresponding metallic ones.

• Korean Journal of Materials Research
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• v.20 no.2
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• pp.104-110
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• 2010

The characteristics of all polymer composites containing carbon materials are determined by four factors: component properties, composition, structure and interfacial interactions. The most important filler characteristics are particle size, size distribution, specific surface area and particle shape. As a consequence, in this paper we discuss the aspects of the mechanical, electrical and thermal properties of composites with different fillers of carbon black, carbon nanotube (CNT), graphene and graphite and focus on the relationship between factors and properties, as mentioned above. Accordingly, we fabricate rubber composites that contain various carbon materials in carbon black-based and silica based-SBR matrixes with dual phase fillers and use scanning electron microscopy, Raman spectroscopy, a rhometer, an Instron tensile machine, and a thermal conductivity analyzer to evaluate composites' mechanical, fatigue, thermal, and electronic properties. In mechanical properties, hardness and 300%-modulus of graphene-composite are sharply increased in all cases due to the larger specific surface. Also, it has been found that the thermal conductivity of the CNT-composite is higher than that of any of the other composites and that the composite with graphene has the best electrical properties.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.55 no.12
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• pp.570-575
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• 2006

In this paper, we have investigated thermal properties by changing the content of carbon nanotube, which is component part of semiconductive shield in underground power transmission cable. Heat capacity (${\Delta}H$), glass transition temperature (Tg) and melting temperature (Tm) were measured with the samples of eight, through DSC (Differential Scanning Calorimetry), and the measurement ranges of temperature selected from $-100[^{\circ}C]\;to\;100[^{\circ}C]$ with heating temperature selected per $4[^{\circ}C/min]$ Also, high temperature, heat degradation initiation temperature, and heat weight loss were measured by TGA (Thermogravimetric Analysis) in the temperature from $0[^{\circ}C]\;to\;700[^{\circ}C]$ with rising temperature of $10[^{\circ}C/min]$. As a result, the Glass transition temperatures of the sample were showed near $-20[^{\circ}C]{\sim}25[^{\circ}C]$, and the heat capacity and melting temperature from the DSC was increased according to increasing the content of carbon nanotube, while, thermal diffusivity was increased according to increasing the content of carbon nanotube. Also, heat degradation initiation temperature from the TGA results was increasing according to increasing the content of carbon nanotube with CNT/EEA. Therefore, heat stabilities of EVA, which contained the we VA (vinyl acetate), showed the lowest.

• Carbon letters
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• v.27
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• pp.90-97
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• 2018

Electromagnetic interference (EMI) shielding is an important issue in modern daily life due to the increasing prevalence of electronic devices and their compact design. This study estimated EMI-shielding effect (EMI-SE) of small ($8-14{\times}17mm$) Hanji (Korean traditional paper) doped with carbon nanotubes (CNTs) and compared to Hanji without CNT using $^2H$ (92.1 MHz) and $^{23}Na$ (158.7 MHz) nuclear magnetic resonance (NMR) peak area data obtained from 1 M NaCl in $D_2O$ samples in capillary tubes that were wrapped in the Hanji samples. The simpler method of using the variation of reflected power and tuning frequency by inserting the sample into an NMR coil was also tested at 242.9, 158.7, and 92.1 MHz. Overall, EMI shielding was relatively more effective at the higher frequencies. Our results validated that NMR methods to be useful to evaluate EMI-SE, particularly for small, flexible shielding materials, and demonstrated that EMI shielding by absorption is dominant in Hanji mixed with CNT.

• Journal of Sensor Science and Technology
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• v.29 no.6
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• pp.394-398
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• 2020

In this paper, we report the sensing performance of H₂ gas sensors composed of Pd/carbon nanotube (CNT) buckypaper at room temperature. The CNT buckypaper was made using a simple filtration process and subsequently deposited with Pd as the sensing material. The sensitivity of the sensor increased with respect to the gas concentration. To investigate the effect of Pd thickness, Pd layers of different thickness were deposited on the buckypaper, and the response of the sensor was evaluated. The proposed sensor exhibits excellent sensing properties with optimized Pd thickness at room temperature (25℃). Pd nanoparticles significantly impact the sensitivity and selectivity of the sensor because of the spillover effect. In addition, the sensor is highly suitable for bendable and wearable devices owing to its structural flexibility.

• Steel and Composite Structures
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• v.25 no.6
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• pp.649-661
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• 2017

This paper is motivated by the lack of studies in the technical literature concerning to the influence of carbon nanotubes (CNTs) waviness and aspect ratio on the vibrational behavior of functionally graded nanocomposite annular sector plates resting on two-parameter elastic foundations. The carbon nanotube-reinforced (CNTR) plate has smooth variation of CNT fraction based on the power-law distribution in the thickness direction, and the material properties are also estimated by the extended rule of mixture. In this study, the classical theory concerning the mechanical efficiency of a matrix embedding finite length fibers has been modified by introducing the tube-to-tube random contact, which explicitly accounts for the progressive reduction of the tubes' effective aspect ratio as the filler content increases. Parametric studies are carried out to highlight the influence of CNTs volume fraction, waviness and aspect ratio, boundary conditions and elastic foundation on vibrational behavior of FG-CNT thick sectorial plates. The study is carried out based on three-dimensional theory of elasticity and in contrary to two-dimensional theories, such as classical, the first- and the higher-order shear deformation plate theories, this approach does not neglect transverse normal deformations. The annular sector plate is assumed to be simply supported in the radial edges while any arbitrary boundary conditions are applied to the other two circular edges including simply supported, clamped and free. For an overall comprehension on 3-D vibration of annular sector plates, some mode shape contour plots are reported in this research work.