• Title/Summary/Keyword: close adhesion

Search Result 52, Processing Time 0.024 seconds

Microstructures and Solderability of Multi-composition Sn-Cu Lead-free Solders (Sn-CU계 다원 무연솔더의 미세구조와 납땜특성)

  • Kim Ju-Youn;Bae Kyoo-Sik
    • Korean Journal of Materials Research
    • /
    • v.15 no.9
    • /
    • pp.598-603
    • /
    • 2005
  • To develope new lead-free solders with the melting temperature close to that of Sn-37Pb$(183^{\circ}C)$, Sn-0.7Cu-5Pb-1Ga, Sn-0.7Cu-5Pb-1Ag, Sn-0.7Cu-5Pb-5Bi-1Ag, and Sn-0.7Cu-SBi-1Ag alloys were composed by adding low-netting elements such as Ga, Bi, Pb, and Ag to Sn-0.7Cu. Then the melting temperatures, microstructures, wettability, and adhesion properties of these alloys were evaluated. DSC analysis showed that the melting temperature of Sn-0.7Cu-SPb-1Ga was $211^{\circ}C$, and those of other alloys was in the range of $192\~200^{\circ}C$. Microstructures of these alloys after heat-treatment at $150^{\circ}C$ for 24 hrs were basically composed of coarsely- grown $\beta-Sn$ grains, and $Cu_6Sn_5$ and $Ag_3Sn$ intermetallic precipitates. Sn-0.7Cu-5Pb-1Ga and Sn-0.7Cu-5Pb-5Bi-1Ag showed excellent wettability, while Sn-0.7Cu-5Bi-1Ag and Sn-0.7Cu-5Pb-5Bi-1Ag revealed good adhesion strength with the Cu substrates. Among 4 alloys, Sn-0.7Cu-5Pb-5Bi-1Ag with the lowest melting temperature $(192^{\circ}C)$ and relatively excellent wettability and adhesion strength was suggested to be the best candidate solder to replace Sn-37Pb.

Adhesion Amount of Acetamipride on Plant and the Pest Control Effect According to the Reduced Application Amount (살포량 감소에 의한 살충제 Acetamipride의 작물 부착량과 나방류 방제효과)

  • Kim, Young-Shin;Jang, Ji-Woong;Jin, Na-Young;Yu, Yong-Man;Youn, Young-Nam;Lim, Chi-Hwan
    • The Korean Journal of Pesticide Science
    • /
    • v.19 no.3
    • /
    • pp.317-322
    • /
    • 2015
  • This study was conducted to obtain basic data for deriving the appropriate application amount of insecticide for effective pest control. We have investigated the correlation among the application amount of insecticide, the adhesion amount of active ingredient and the pest control effect. The linear standard curve of acetamiprid was $R^2=0.9994$, and the scope of the recovery factor was between 71% and 93% with less than 6% of the coefficient of variation. During the test conducted in 2015, the application amount was reduced to 302 L/10a which was 70 L less than the previous year and the spraying pressure was reduced as well. After analyzing the adhesion amount of active ingredient, it was found that a correlation coefficient of adhesion amount of the active ingredients became lower from 82% to 69%, that indicated insecticide liquid was evenly distributed compared to 2014. Also more than 95% of control effect was displayed, thereby indicating that there is a close relation with the correlation coefficient of the adhesion amount of active ingredient. It also presented that the adhesion amount of active ingredient on the ground was 2.2 times more than that on the leaves of apple trees.

Influence of plant surface spray adhesion of dinotefuran and thiodicarb on control of apple leafminer

  • Kim, Young-Shin;Kim, Kwang-Soo;Jin, Na-Young;Yu, Yong-Man;Youn, Young-Nam;Lim, Chi-Hwan
    • Korean Journal of Agricultural Science
    • /
    • v.43 no.3
    • /
    • pp.346-352
    • /
    • 2016
  • This study was conducted to obtain the correlation between the plant surface spray adhesion amount of pesticides and the pest control effect. The linearity of the standard curves of dinotefuran and thiodicarb was $R^2=0.9999$, and recovery was between 70% to 120% which was satisfactory for insecticide residue analyses. The pest control effect was evaluated by assessing the number of apple leafminers (Phyllonorycter ringoniella, Gracillariidae, Lepidoptera) captured by sex pheromone traps from late June to late September in 2015. For the adhesion amount, dinotefuran recovered from trap A and B, respectively were $47{\mu}g/50cm^2$ and $23{\mu}g/50cm^2$, which can be characterized as a very low adhesion amount in comparison to the average adhesion amount of $81{\mu}g/50cm^2$ in the field. In case of thiodicarb, $691{\mu}g/50cm^2$ and $71{\mu}g/50cm^2$ were recovered from trap A and B, respectively, and the average amount in the field is $325{\mu}g/50cm^2$. These results showed close correlation with the insect population captured by trap A and B. The numbers of insects captured by trap A and B between the end of July and late August were similar. After spraying thiodicarb on August 28, the number of apple leafminers captured by trap B is bigger than that of trap A. It appears that pest occurrence tended to be high at low adhesion amounts of the active ingredient. Therefore, in order to obtain an optimal control effect, it is suggested that uniform application of insecticides is critical instead of relying on the amount of insecticide applied in the field.

Formation of Metal Electrode on Si3N4 Substrate by Electrochemical Technique (전기화학 공정을 이용한 질화규소 기판 상의 금속 전극 형성에 관한 연구)

  • Shin, Sung-Chul;Kim, Ji-Won;Kwon, Se-Hun;Lim, Jae-Hong
    • Journal of the Korean institute of surface engineering
    • /
    • v.49 no.6
    • /
    • pp.530-538
    • /
    • 2016
  • There is a close relationship between the performance and the heat generation of the electronic device. Heat generation causes a significant degradation of the durability and/or efficiency of the device. It is necessary to have an effective method to release the generated heat. Based on demands of the printed circuit board (PCB) manufacturing, it is necessary to develop a robust and reliable plating technique for substrates with high thermal conductivity, such as alumina ($Al_2O_3$), aluminium nitride (AlN), and silicon nitride ($Si_3N_4$). In this study, the plating of metal layers on an insulating silicon nitride ($Si_3N_4$) ceramic substrate was developed. We formed a Pd-$TiO_2$ adhesion layer and used APTES(3-Aminopropyltriethoxysilane) to form OH groups on the surface and adhere the metal layer on the insulating $Si_3N_4$ substrate. We used an electroless Ni plating without sensitization/activation process, as Pd particles were nucleated on the $TiO_2$ layer. The electrical resistivity of Ni and Cu layers is $7.27{\times}10^{-5}$ and $1.32{\times}10^{-6}ohm-cm$ by 4 point prober, respectively. The adhesion strength is 2.506 N by scratch test.

EFFECT OF A REWETTING AGENT ON DENTIN ADHESION (재습윤제의 적용이 상아질 접착에 미치는 효과)

  • Cho, Young-Gon;Park, Yil-Yoon;Lee, Young-Gon
    • Restorative Dentistry and Endodontics
    • /
    • v.28 no.1
    • /
    • pp.11-22
    • /
    • 2003
  • This study compared the dentin adhesion to composite resin according to air-dry, blot dry, application of rewetting agent on air-dry or blot dry dentin surface by microleakag test and SEM observation. For microleakage test, class V cavity preparations with dentinal margins were prepared on both buccal and lingual surfaces of 40 extracted human molars. For SEM observation, occlusal dentin of 20 extracted human molars were exposed. After etched the dentin, prepared teeth were randomly divided into four groups; D group: air dry for 10-15 sec., B group: blot dry with moist cotton pellet, D-R group: air dry and rewet with Aqua-Prep F for 20 sec., B-R group: blot dry and rewet with Aqua-Prep F for 20 sec. Treated cavities and surfaces were filled or constructed using One-Step adhesives and Aelitefil composite resins. Specimens were stored in distilled water for 24 hours. For microleakage test, the specimens were thermocycled and soaked into 2% methylene blue. The specimens were sectioned longitudinally and evaluated for microleakage under steromicroscope. The data were statistically analysed by Kuskal-Wallis Test, Mann-Whitney and Wilcoxon signed ranked tests. For SEM observation, the specimens were bisectioned mesiodiatally. After decalcified and deproteinized, specimens were observed under SEM. The results of this study were as follows; 1. The microleakges on dentinal margin were the highest in D group compared with B group, D-R group, and B-R group(p<0.05). But there was no significant difference between B group, D-R group and B-R group. 2. D group showed gap and a few resin tags between dentin and composite resin. 3 B group, D-R group, and B-R groups showed close adaptation between dentin and composite resin. It showed that resin rags in B group were numerous and long, in D-R group were few and short, in B-R group were numerous and short or long. 4. Adhesive layer showed in D-R group ($10{\;}\mu\textrm{m}$) and B-R group ($3{\;}\mu\textrm{m}$) In conclusion, use of rewetting agent to dry dentin was efficient to dentin adhesion, also it did not provide reverse effect on blot dry dentin.

A Study on the Eroticism Expressed on the Female's Contemporary Sportswear (현대 여성 스포츠웨어에 표현된 에로티시즘에 관한 연구)

  • Kim, Sun-Hwa
    • Journal of the Korean Society of Fashion and Beauty
    • /
    • v.5 no.1 s.12
    • /
    • pp.8-13
    • /
    • 2007
  • The purpose of the study was to analyze how to express the eroticism on the female's contemporary sportswear. Six hundred fifty few pictures in the fashion magazines such as Vogue, and Elle etc., and at the collections through the internet from 2000 to 2005, were used for the analysis. Other related books and articles were also used for the study. The eroticism on the female's contemporary sportswear was mainly expressed through two ways such as direct exposure and indirect exposure. The details of the eroticism expressed through these two ways were as follows; 1. The extent of direct exposure in bust area and leg were excessive compared to other body area specially in tennis wear, swimsuit, boxing wear and dance wear etc. 2. See-through and close adhesion were used in order to express eroticism indirectly.

  • PDF

A Study on the Forming Process Optimization of a Small Tube (소구경 관단 성형공정 최적화)

  • Lee, Jung-Hwan;Lee, Seung-Hoon;Oh, Hyun-Ok
    • Journal of Korean Society of Industrial and Systems Engineering
    • /
    • v.33 no.3
    • /
    • pp.71-78
    • /
    • 2010
  • The end shape of tube for automobile power steering system has influence on the ability of performance. In this case study, we attempted to optimize the forming process of a small tube using Taguchi experimental design methodology. A preliminary experiment was conducted and four main control factors were selected. The experiment was set up as an $L_9(3^4)$ orthogonal array, and determined the optimal levels of the four factors through the analysis of the experimental results. As a result, the performance characteristic(close adhesion power) of the product was improved about 36%. In addition, the process capability index $C_{pk}$ is enhanced from 0.94 to 6.85.

Repairing of a Defective Metallic Line using Laser CVD Deposited Tungsten Film in TFT LCD (레이저 CVD 텅스텐막 증착을 통한 TFT LCD 불량배선 수리)

  • Kim, Sukoon-Koon;Son, Jeong-Seok;Lee, Gi-Sun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.17 no.10
    • /
    • pp.1114-1119
    • /
    • 2004
  • The photodepositioned tungsten film by laser CVD has been carried out the taping test with scotch tape over 10 times. As a result, it exhibited strong adhesion to the under-film such as ITO and SiNx patterned on the LCD substrate. However, it was seriously attacked by alkaline solution used for removing polyimide. And a thickness of laser CVD tungsten film had a close relation to a speed of laser scanning. Also we have improved the success rate of a laser CVD repair with making two pairs of contact hole structure and decreasing laser scanning speed.

A study on the vibration restraint of sports-brassiere (Sports-brassiere의 컵소재에 따른 방진효과에 관한 연구)

  • 손부현
    • Journal of the Korean Home Economics Association
    • /
    • v.34 no.3
    • /
    • pp.123-136
    • /
    • 1996
  • This report deals with the relations between the vibration restraint and the stress-strain properties of the stretch fabrics. For this purpose, a survey was carried out about the preferences in sports-brassiere. Six experimental sports-brassieres of an equal design, but of different materials were tested for vibration using an accelerometer and a motion analyzer while the subject is jogging. 1. The results of the survey on sports-brassiere preferences are as follows; Preferable factors are simple design, shield and close adhesion of sports brassiere. Dissatisfied factors on the sports-brassiere are drooping, vibrating of the breast, itching and wetting. The B-cup-size group perceive the bigger vibration and drooping than A-cup-size. 2. The results of the wearing tests are as follow; This experiment shows the vibration restraint effects on different stretch fabrics, such as hard, medium and soft nature. There was a linear relationship between the vibration restraint and combination of different types of stretch fabrics. Among different brassiere types, the 2-layered brassiere (inner layer of high tension fabric and outer layer of lower stretch fabric) showed the least vibration. In the case of 2-lay brassiere, the wearing comfort rate was highest.

  • PDF

Mechanical Properties of Polypropylene/Talc Composites Prepared via Solid-State Extrusion (고상 압출된 폴리프로필렌/탈크 복합재료의 기계적 물성)

  • Lee, Jaechoon;Ha, Chang-Sik
    • Journal of Adhesion and Interface
    • /
    • v.17 no.4
    • /
    • pp.131-135
    • /
    • 2016
  • We investigated the specific gravity and mechanical property changes of solid-state extruded polypropylene (PP)/talc composites before and after orientation. The specific gravity of the composites increases with increasing the filler contents. The specific gravity of the oriented specimen containing filler in PP matrix is found to be much smaller than that of pre-specimen due to the formation of more micro-voids. It was found that the tensile properties of the composites are increased up to the talc content of 10 wt%, but after the contents exceeding 10 wt%, the tensile properties are decreased. For oriented specimens, the tensile strength of the composites showed monotonously decrease with increasing talc contents. When the contents of talc is 10 wt%, the theoretical values according to Halpin-Tsai equation are close to the experimental values but over 20 wt% of talc contents, the deviation of the experimental values from the theoretical prediction becomes higher. The maximum flexural strength and modulus were observed for PP/talc composites when the talc contents was 10 wt% for both pre-specimen and oriented specimen.