• 제목/요약/키워드: chemical composition analysis

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피삭제와 공구재종의 상관관계에 근거한 절삭조건의 최적화(II) (Optmization of Cutting Condition based on the Relationship between Tool Grade and Workpiece Material (2nd. Report))

  • 한동원;고성림
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1995년도 추계학술대회 논문집
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    • pp.169-172
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    • 1995
  • In optmizing cutting condition for face milling operation, tool wear is an important maching factor. For the purpose of establishing the relationship between various maching factor and tool wear, cutting tests have been performed. As a result, hardness and chemical composition of workpiece material, chemical compositition and grain size of cutting tool and cutting speed have been selected as machining factor. In addition, relationship between feed rate and workpiece hardness has been observed. Prior to utilizing cutting condition recommended by 'Machining Data Hardbook(MDH)' as a Knowledge base, an analysis for the validity has been provided. Based on this analysis, tool life criteria applied by MDH has been modifiied. Finaly, using MDH recommended data for neural network trainning, we can compensate the result form the trained neural network for optimizing cutting condition for some given workpice and cutting tool.

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단벌기 순환림 후보 호랑버들 7 클론의 화학적 조성과 에너지 함량 (Chemical composition and Energy contents analysis of Seven Clones of Salix hultenii as short-rotation forestry candidate)

  • 신수정;김용상;연익준;한심희
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2009년도 춘계학술대회 논문집
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    • pp.436-438
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    • 2009
  • To evaluate short rotation forestry candidates, seven clones of Salix hultenii were investigated as focused on chemical compositions and energy contents. There were significant variations in chemical compositions and energy contents among different clones. Variations in hot-water extractives content were 6.6-16.0% and 19.6-25.4% variation in lignin content. In carbohydrate compositional analysis, xylan contents were 7.5-13.1% with variation among different clones. Higher heating values were 17.69-20.02 MJ/kg.

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Critical evaluation of a Nigerian sub-bituminous coal potential for energy derivation

  • Odeh, Andrew O.
    • Advances in Energy Research
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    • 제4권3호
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    • pp.203-211
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    • 2016
  • A good understanding of the chemical composition and structural characteristics of a carbonaceous material is essential in conversion processes. Understanding how the composition and structural changes influence the burning behaviour of coal is important when assessing a coal's potential for utilization. To explore the potentials of a typical Nigerian coal, both conventional and advanced analytical techniques such as proximate analysis, ultimate analysis, calorific value, surface area analyser, SEM, FTIR, XRD and SAXS were employed. The results obtained from these characterizations agree favourable well with a typical South African coal that is of enormous contribution to the gross domestic product (GDP) of the nation economy.

Taxonomical Study of Chrysosplenium L. (Saxifragaceae) in Korea Based on Chemical Composition

  • Kim, Hyun-Jun;Jeong, Hea-Seok;Kang, Shin-Ho
    • 한국자원식물학회지
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    • 제26권6호
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    • pp.718-725
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    • 2013
  • Components extracted from 7 species and 18 populations of Chrysosplenium in Korea were compared and analyzed using GC-MS analysis. 57 components (${\geq}80%$ quality) were identified, of which neophytadiene, palmitic acid and phytol were found at all the taxa. Percentage composition of isolated extracts showed a clear difference in components type and GC-MS profile. On the basis of that result, data matrix was made and cluster analysis using UPGMA was conducted. From the result of cluster analysis, two groups were recombined; one with alternate leaves comprised C. japonicum in Ser. Alternifolia and C. flagelliferum in Ser. Flagellifera and the other with opposite leaves gradationally comprised C. psuedofauriei in Ser. Sinica, C. ramosum in Ser. Oppositifolia and C. sphaerospermum, C. valdepilosum, C. flaviflorum in Ser. Pilosa. These chemotaxonomic results agreed in general with those of existing studies on external morphology and molecular. In conclusion, chemical composition can be an useful characters in understanding the relation analysis among interspecific and intraspecific complex with the help of cluster analysis of 7 species and 18 populations of Chrysosplenium in Korea.

에폭시 아스팔트 혼합물의 에폭시 화학 조성에 따른 양생수준 예측 (A Study on Curing Level Prediction Model for Varying Chemical Composition of Epoxy Asphalt Mixture)

  • 조신행;김낙석
    • 대한토목학회논문집
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    • 제35권2호
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    • pp.465-470
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    • 2015
  • 에폭시 아스팔트 혼합물은 에폭시 수지와 경화제의 화학반응이 진행되어 양생시간을 거쳐 성능 발현이 이루어진다. 에폭시 아스팔트의 양생수준은 후속공정의 진행과 교통개방 및 공정계획의 수립에 절대적인 영향을 미치므로 정확한 예측모델의 개발이 중요하다. 본 연구에서는 기존 예측식에 사용되는 인자들의 화학적 의미 분석을 통하여 에폭시 수지의 농도와 경화특성을 반영하여 기존식보다 확대된 적용 범위를 갖는 양생수준 예측식을 제시하였다. 실외양생 실험과 비교 결과 상관계수가 0.971 이상으로 나타나 조성이 다른 에폭시 아스팔트 혼합물의 온도와 시간에 따른 양생수준을 예측할 수 있는 것으로 나타났다.

Changes in microbial population and chemical composition of corn stover during field exposure and effects on silage fermentation and in vitro digestibility

  • Sun, Lin;Wang, Zhijun;Gentu, Ge;Jia, Yushan;Hou, Meiling;Cai, Yimin
    • Asian-Australasian Journal of Animal Sciences
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    • 제32권6호
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    • pp.815-825
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    • 2019
  • Objective: To effectively use corn stover resources as animal feed, the changes in microbial population and chemical composition of corn stover during field exposure, and their silage fermentation and in vitro digestibility were studied. Methods: Corn cultivars (Jintian, Jinnuo, and Xianyu) stovers from 4 random sections of the field were harvested at the preliminary dough stage of maturity on September 2, 2015. The corn stover exposed in the field for 0, 7, 15, 30, 60, 90, and 180 d, and their silages at 60 d of ensiling were used for the analysis of microbial population, chemical composition, fermentation quality, and in vitro digestibility. Data were analyzed with a completely randomized $3{\times}6$ [corn stover cultivar $(C){\times}exposure$ d (D)] factorial treatment design. Analysis of variance was performed using SAS ver. 9.0 software (SAS Institute Inc., Cary, NC, USA). Results: Aerobic bacteria were dominant population in fresh corn stover. After ensiling, the lactic acid bacteria (LAB) became the dominant bacteria, while other microbes decreased or dropped below the detection level. The crude protein (CP) and water-soluble carbohydrate (WSC) for fresh stover were 6.74% to 9.51% and 11.75% to 13.21% on a dry matter basis, respectively. After exposure, the CP and WSC contents decreased greatly. Fresh stover had a relatively low dry matter while high WSC content and LAB counts, producing silage of good quality, but the dry stover did not. Silage fermentation inhibited nutrient loss and improved the fermentation quality and in vitro digestibility. Conclusion: The results confirm that fresh corn stover has good ensiling characteristics and that it can produce silage of good quality.

도.토기의 화학조성-경주 황남대총 출토 도.토기를 중심으로 (The scientific analysis of potteries excavated from Kyong-ju relics-In terms of potsherds excavated from Wangkyong, Walsung, Hwangnam great tomb)

  • 홍종욱;문환석;황진주;조남철
    • 보존과학연구
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    • 통권20호
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    • pp.91-120
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    • 1999
  • This paper presents the results of investigation on crystal, firing temperature and trace elements analysis of fragments 4~8 centriesexcavated from Kyong ju historical sites such as Wang kyong,Walsung, Hwangnam great tomb by application of optical microscope, neutron activation analysis and X-ray diffraction. Temper analysis of clay for identification of local or foreign production; Trace elements is not presented a unique chemical composition. That’s data have to be treated a statistical process in order to normalize. The results followed ;(1) Firing temperature could be estimated $700^{\circ}C$ on some softness pottery at Walsung and most of hardness others are $1,000^{\circ}C$ to $1,200^{\circ}C$.(2) Crystal structures are divided into three kinds of mineralogical composition(Quartz, Mullite, Feldspar).(3) Considering of the results of statistical data, chemical composition of Walsung is more similarly Wang kyong than Hwangnam great tomb.

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제주화산도의 암석성분에 관한 통계학적인 수치해석 (The Statistical on Numerical Analysis for The Petrology and Bulk Chemical Composition. In Cheju Volcanic Island)

  • 택훈
    • 동굴
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    • 제14권15호
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    • pp.42-90
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    • 1987
  • 제주화산도의 암석학에 대한 암석기재 및 총화학 조성의 63종은 이문원에 의해 보고되고 있다. 총화학조성 데-타는 FORTRAN77의 프로그램에 의해 해석을 하였다. 해석에는 우선 최소자집법에 의해 환산식과 산분도를 검토했다. 다음에 통계적 데-타는 평균치, 최대치, 최소치, 범위, 표준편차, 분산, 표준오차 및 변동계수를 구했다. 표준편차의 큰 단위 물질은 SiO$_2$, MgO 및 FeO이고 작은 단위 물질은 MnO와 P$_2$O$_{5}$이다. 표준오차와 분산은 표준편차와 매우 유사한 조항이 있다. 그렇지만 변동계수는 표준편차와 다르다. 여기에서 큰 단위 변동계수는 $H_2O$$^{-}$$H_2O$$^{+}$이고, 작은 단위 변동계수는 $Al_2$O$_3$ 및 SiO$_2$ 이다. 상관계수의 계산은 정과 부의 상관성을 SiO$_2$, $Al_2$O$_3$ 및 TiO$_2$에 대해서 다른 조성과의 관계를 계산적으로 구할수 있다.

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Macromolecular and Elemental Composition Analyses of Leuconostoc mesenteroides ATCC 8293 Cultured in a Chemostat

  • Bang, Jeongsu;Li, Ling;Seong, Hyunbin;Kwon, Ye Won;Jeong, Eun Ji;Lee, Dong-Yup;Han, Nam Soo
    • Journal of Microbiology and Biotechnology
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    • 제27권5호
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    • pp.939-942
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    • 2017
  • The cellular composition and metabolic compounds of Leuconostoc mesenteroides ATCC 8293 were analyzed after cultivation in an anaerobic chemostat. The macromolecular composition was 24.4% polysaccharide, 29.7% protein, 7.9% lipid, 2.9% DNA, and 7.4% RNA. Its amino acid composition included large amounts of lysine, glutamic acid, alanine, and leucine. Elements were in the order of C > O > N > H > S. The metabolites in chemostat culture were lactic acid (73.34 mM), acetic acid (7.69 mM), and mannitol (9.93 mM). These data provide a first view of the cellular composition of L. mesenteroides for use in metabolic flux analysis.

Preparation and Characterization of Monolithic Poly(methacrylic acid - ethylene glycol dimethacrylate) Columns for High Performance Liquid Chromatography

  • Yan, Hong-yuan;Row, Kyung-Ho
    • Bulletin of the Korean Chemical Society
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    • 제27권1호
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    • pp.71-76
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    • 2006
  • Porous polymer monolithic columns were prepared by the direct free radical copolymerization of methacrylic acid and ethylene glycol dimethacrylate within the confines of a chromatographic column in the presence of toluene-dodecanol as a porogenic solvent. The separation characteristics of the monolithic columns were tested by a homologous series of xanthine derivatives, theophylline and caffeine. The effects of the polymerization mixture composition and polymerization condition, mobile phase composition, flow rate and temperature on the retention times and separation efficiencies were investigated. The results showed that the selection of correct porogenic solvents and appropriate polymerization conditions are crucial for the preparation of the monolithic stationary phases. The separation efficiency was only extremely weakly dependent on flow rate and temperatures. Hydrogen-bonding interaction played an important role in the retention and separation. Compared with conventional particle columns, the monolithic column exhibited good stability, ease of regeneration, high separation efficiency and fast analysis.