• Journal of Welding and Joining
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• 제26권4호
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• pp.73-78
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• 2008

In this paper, research was the variation of microstructure and mechanical properties of clad(A4045/A3003) Al alloy sheet by gas tungsten arc welding. Tensile properties of the gas tungsten arc welding joint decreased because of the softened heat affected zone(HAZ). The hardness of HAZ was lower than that of base metal, because relieved the work hardening effect of the welding heat. Hardness distribution of the weld zone with the base metal appears similarly, but the hardness of HAZ decreased remarkably. The microstructure in the weld zone of A4045 clad layer was formed a coarse columner grains of Si-rich. In the case of large weld heat input, the Si of the A4045 were diffused and until A3003 weld zone they decreased the strength.

• 한국지반공학회:학술대회논문집
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• 한국지반공학회 2009년도 세계 도시지반공학 심포지엄
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• pp.1100-1106
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• 2009

This study intends to develop a pulse discharge device to strengthen the pushing power by expanding the cavity of the anchor settlement to form a spheric root for the purpose of constructing the economical and stable anchor. and, a series of field test were carried out in order to check applicability of machines of pulse powered underreamed anchors. Through the experiments, the electrical characteristics of the pulse power equipment had been identified it and the dynamic pressure generated from the subsequent change had been measured. Here, the measured dynamic pressure is the cavity expansion pressure to impact on the ground around the anchor settlement. Since this pressure has effects of cavity expansion and bored surface hardening with dynamic hardening effects on the anchor settlement, it is expected that it will largely contribute the increase of pushing power with a strong frictional resistance.

• 연구논문집
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• 통권31호
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• pp.113-125
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• 2001

Silicon addition in titanium alloys generally results in solid solution hardening by silicon itself and precipitation hardening by titanium silicides. The morphology and distribution of the titanium silicides depend upon the alloy chemistry or the heat treatment condition, and play an important role in improving the mechanical properties of the alloys. In this study, the morphology and crystallographic characteristics of the titanium silicides in the Ti-Fe-Si alloy system were studied. Three types of silicides were found in the alloys; (1) interconnected chain-like silicides at grain boundary, (2) coarse silicides over im, (3) fine silicides smaller than 0.2m. Ti3Si was dominant in cast + HIP condition while Ti5Si3 was dominant in as-cast state. It is recognized that $Ti_5Si_3$$\rightarrow$$Ti_3Si$ transition occurred by the peritectoid reaction and it may be promoted by the pressure during HIP. However, in the case of the fine silicides, $Ti_3Si$ and $Ti_5Si_3$ were found simultaneously even after HIP. Such a fine silicide was found to have a crystallographic orientation relationship with matrix.

• Metals and materials international
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• 제24권6호
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• pp.1221-1231
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• 2018

The effect of strain aging on tensile behavior and properties of API X60, X70, and X80 pipeline steels was investigated in this study. The API X60, X70, and X80 pipeline steels were fabricated by varying alloying elements and thermomechanical processing conditions. Although all the steels exhibited complex microstructure consisting of polygonal ferrite (PF), acicular ferrite, granular bainite (GB), bainitic ferrite (BF), and secondary phases, they had different fractions of microstructures depending on the alloying elements and thermomechanical processing conditions. The tensile test results revealed that yielding behavior steadily changed from continuous-type to discontinuous-type as aging temperature increases after 1% pre-strain. After pre-strain and thermal aging treatment in all the steels, the yield and tensile strengths, and yield ratio were increased, while the uniform elongation and work hardening exponent were decreased. In the case of the X80 steel, particularly, the decrease in uniform elongation was relatively small due to many mobile dislocations in PF, and the increase in yield ratio was the lowest because a large amount of harder microstructures such as GB, BF, and coarse secondary phases effectively enhanced work hardening.

• 열처리공학회지
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• 제11권4호
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• pp.247-257
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• 1998

In order to evaluate the relation between prior structure and fatigue strength on a induction surface hardened medium carbon steel(SAE1050M) for automotive drive shafts, torsional fatigue test were conducted with various cases of different hardened depths and applied loads. Prior structures of the steel such as pearlite, fine pearlite and spheroidal pearlite were prepared by conventional nomalizing, tempering after quenching and spheroidized annealing, respectively. Maximum torsional fatigue strength can be obtained when the case depth is 18~25% diameter of the bar in each prior structure. The effect of case depth on the torsional fatigue strength was different depending on applied load to specimen, but the most good fatigue life was shown in the case of pearlitic structure when the case depth was 4.0~5.5mm(18~25% of bar diameter). Among three different prior structures, energy consumption, to obtain high strength or to get the same case depth, was the most saved in the case of pearlitic structure.

• 한국재료학회지
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• 제3권6호
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• pp.606-613
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• 1993

자동차용 부품재 및 일반산업용 재료로 사용되고 있는 AC4A Al합금에 $SiC_{w}$ preform을 용탕단조법으로 강화시킨 복합재료의 시효 경화능은 SiC/aub w/30%> 10%> 20%의 순이며, 이는 $100^{\circ}C$-$400^{\circ}C$까지의 등시시효에서도 같은 결과를 나타낸다. 복합재의 T6처리재가 AC4A I/M재 보다도 시효경화능이 크고 절대값이 높았으며 $SiC_{w}$체적분율 증가에 따라 초기경화 현상을 나타내었다. 가압력에 의한 강화효과는 미시효때와 같이 가압력 75MPa일때 가장 좋았으며, $SiC_{w}$는 30%> 10%>20%순이었다. 가압력이 낮을경우 가입과 동시에 휘스커는 파단되지 않고 원래의 형상을 유지하거나 기지금속과 wetting으로 일부 변형된 다음 가압이 진행되면서 이부부의 응력 집중으로 wetting부가 파단하게 되어 가압력을 이기지 못하고 파단하게 되어 휘스커 모양도 다각형이거나 구형에 가깝게 되며 가압이 진행됨에따라 재차 파단되므로써 길이도 짧게 된다. 한편 가압력 75 MPa일 경우 휘스커의 형상은 일부 변형된 것과 잘게 파손된 것이 고르게 공존하고 있어 강화효과가 가장 우수한 것으로 사료된다.

• Journal of Pharmaceutical Investigation
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• 제4권1_2호
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• pp.39-45
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• 1974

According to previous paper, the hardness of semi-solid as ointments and suppositories causes the tough or skin, the pain and connected with absorption, the state of spread or the efficiency of drug. When the hardening agent or the softening agent is added to ointment whid, is registered on the pharmacopeia of the republic of Korea, the experimertal data by apparent logarithmic hardness are shown is Table 1. The results are as the folloring. 1) In case of the softening agent which is added to ointment base, each has shown two different equation with differnented slope as $K_1$ and $K_2$ value determined (Fig. 1,2). 2) When the hardening agent is added to same ointment base, these studies indicated that there is a direct correlation between $K_1$ and $K_2$. However, in case of softening agent $K_1$ and $K_1$ are not correlated as indicated in Fig. $3{\sim}8$. 3) On condition of same ointment base, the critical poit is proportional to $K_1$ 4) The second effect is at least $3{\sim}17$ times more. sensitive than the first effect or in average 8.3 times more sensitive, Therefore, the results presented in this paper. Suggest that, when the drug is added to a certain ointment base, it should be added within this first effect before the critical point is reached.

• 한국식품과학회지
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• 제16권2호
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• pp.153-158
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• 1984

치즈의 융해정도(融解程度)(meltability)를 측정하는 전통적인 방법중 대표적인 2가지 방법, 즉 Schreiber방법과 Arnott방법을 비교 검토하였다. 같은 시료에 대해 두가지방법이 서로 다른 융해정도(融解程度)를 나타내었다. Schreiber 방법에서는 sharp Cheddar가 가장 높은 값을 나타내었으며, 그 다음으로 process American, mild Cheddar, Mozzarella의 순(順)이었고. Arhott 방법에서는 그 순서가 바뀌어서 Mozzarella, mild Cheddar, sharp Cheddar. process American의 순(順)이었다. Process cheese product는 분산(分散)된 값들을 보여 일정한 경향을 나타내지 못하었다. 두가지 방법 모두 일정시간(一定時間) 가열시(加熱時)에는 일정(一定)한 융해정도(融解程度)를 보여주었으며 이것은 scorching이나 case hardening에 의해 더 이상의 흐름을 방지(防止)하였기 때문으로 생각된다. DSC-Thermogram은 14도와 30도 근처에서 endothermal peak를 보여주었다. 이들은 가열시(加熱時) 유지방(乳脂肪)의 융해(融解)에 의한 것으로 설명된다.

• 열처리공학회지
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• 제14권1호
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• pp.8-16
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• 2001

The effects of gas composition, pressure, temperature and time on the case thickness, hardness and nitride formation in the surface of tool steels(STD11 and STD61) have been studied by micro-pulse plasma nitriding. External compound layer and internal diffusion layer and the diffusion layer were observed in the nitrided case of tool steels. The relative amounts and kind of phases formed in the nitrided case changed with the change of nitriding conditions. Generally, only nitride phases such as ${\gamma}(Fe_4N)$, ${\varepsilon}(Fe_{2-3}N)$, or $Cr_{1.75}V_{0.25}N_2$ phases were detected in the compound layer, while nitride and carbide phases such as ${\varepsilon}-nitride(Fe_{2-3}N)$, $(Cr,Fe)_{\gamma}C_3$ or $Fe_3C$ were detected in the diffusion layer by XRD analysis. The thickness of compound layer increased with the increase of nitrogen content in the gas composition. Maximum case depth was obtained at gas pressure of 200Pa.

• 열처리공학회지
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• 제13권5호
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• pp.337-345
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• 2000

As a case hardening process for stainless steels, nitriding is more preferred and widely used than carburizing which deterioates corrosion resistance severely. In order to add the nitrogen into the stainless steels, passive film on the surface must be removed effectively before nitriding. Conventional gas nitriding process is performed in the temperature range of 500 to $600^{\circ}C$ with $NH_3$ gas, which often leads to sensitization of stainless steels. In this study, we tried to activate passive film of austenitic stainless steels by heating at low pressure. ($900^{\circ}C$, $5{\times}10^{-2}$ Torr.) Nitriding was performed at the solution treatment temperature of $1100^{\circ}C$ with nitrogen molecules instead of $NH_3$ gas. An attainable nitrogen content in a case depends on the nitrogen gas pressure at constant nitriding temperature. A case depth is proportional to the square root of solution time, which suggests that inward diffusion of nitrogen follows the Fick's 2nd law. Surface nitrogen atoms are dissolved as interstitial solutes, or precipitated in the form of MN, $M_2N$ nitrides, which increase the case hardeness. Dissolved nitrogen in the case enhances the cavitation resistance of austenitic stainless steels dramatically.