• 대한기계학회논문집A
• /
• 제26권4호
• /
• pp.617-624
• /
• 2002

An equation of J-integral for a penny-shaped crack at the end of the fiber embedded in rubber matrix is proposed. The values of J-integral for the specimens with various crack and specimen radius are obtained by FEA(Finite Element Analysis). The dimensional analysis is applied to derive an equation of J-integral as a nonlinear elastic energy release rate. The geometry and deformation calibration function in an equation of J can be expressed in a separated form. The geometry calibration function characterizing the effects of cord and specimen size is expressed in a polynomial form of fourth order. The deformation calibration function characterizes the effect of the overall level of strain. As approaching the infinitesimal strain, the value of the deformation calibration function approaches the results of LEFM(Linear Elastic Fracture Mechanics).

• 한국방사선학회논문지
• /
• 제7권1호
• /
• pp.93-98
• /
• 2013

이 연구의 목적은 6 MV 광자 빔에 대한 광자극형광나노닷선량계(OSLnD)의 교정을 조사하는 데 있다. OSLnD의 선량반응 분석으로부터 선형 및 비선형 교정의 선량범위들은 결정을 하였다. 교정 및 교정식의 정확성을 평가하기 위하여 교정 및 품질관리선량계의 세트들은 만들어서 사용하였다. 교정들은 각각 0~300 cGy 및 20~1300 cGy 선량범위에서 선형 및 비선형적으로 수행하였다. 교정의 오차들은 선형 및 비선형 교정에 대하여 품질관리선량계들의 측정으로부터 각각 0.1% 이하로 얻었다. 이 연구는 6 MV 광자 빔에 대한 OSLnD의 교정식을 제공한다.

• 한국연초학회지
• /
• 제35권1호
• /
• pp.1-6
• /
• 2013

Near InfraRed Spectroscopy(NIRS) is a quick and accurate analytical method to measure multiple components in tobacco manufacturing process. This study was carried out to develop calibration equation of near infrared spectroscopy for the prediction of the amount of chemical components and hot water solubles(HWS) of reconstituted tobacco leaf. Calibration samples of reconstituted tobacco leaf were collected from every lot produced during one year. The calibration equation was formulated as modified partial least square regression method (MPLS) by analyzing laboratory actual values and mathematically pre-treated spectra. The accuracy of the acquired equation was confirmed with the standard error of prediction(SEP) of chemical components in reconstituted tobacco leaf samples, indicated as coefficient of determination($R^2$) and prediction error of sample unacquainted, followed by the verification of model equation of laboratory actual values and these predicted results. As a result of monitoring, the standard error of prediction(SEP) were 0.25 % for total sugar, 0.03 % for nicotine, 0.03 % for chlorine, 0.16 % for nitrate, and 0.38 % for hot water solubles. The coefficient of determination($R^2$) were 0.98 for total sugar, 0.97 for nicotine, 0.96 for chlorine, 0.98 for nitrate and 0.92 for hot water solubles. Therefore, the NIRS calibration equation can be applicable and reliable for determination of chemical components of reconstituted tobacco leaf, and NIRS analytical method could be used as a rapid and accurate quality control method.

• 약학회지
• /
• 제40권6호
• /
• pp.625-631
• /
• 1996

The $H^+$-selective membrane consists of tridodecylamine, 2-nitrophenyl octyl ether and a little amount of additive in carboxylated PVC matrix, where penicillinase(Pcase ) and glutaraldehyde may be covalently attached to the matrix. When the $H^+$-selective electrode was used as a detector of biosensor, calibration curve calculated from Nernst equation was not linear. So we investigated the characteristic responses of the $H^+$-selective electrode to the product H+ from hydrolysis of penicillin-G(Pc-G) and plotted calibration curve correlating potential to concentration of Pc-G linearly. The optimal concentration of buffer solution was theoretically calculated and was also experimented. We tried to explain the linear curve of potential to concentration of Pc-G by using Henderson-Hasselbach equation. This method is more effective in calibration curve plotting than any other previous methods. The results obtained may help in further developing pH electrodes with improved analytical preformance.

• 한국자원식물학회:학술대회논문집
• /
• 한국자원식물학회 2020년도 춘계학술대회
• /
• pp.100-100
• /
• 2020

Wheat is mainly composed of carbohydrate but it contains a moderate amount of protein, which gives a very useful characteristics to flour food such as the unique elasticity and stickiness of the dough. We developed a calibration equation for analyzing crude protein content using Near Infrared Spectroscopy to quick analyze the crude protein content of wheat germplasm stored in the National Agrobiodiversity Center, RDA, Korea. The 1,798 wheat germplasms were used to draw up the calibration formula. The crude protein's interval distribution of 1,798 wheat germplasms used for the calibration was 7.04-20.84%, the average content was 13.2%, and standard deviation was 2.6%. The germplasms distribution was composed of a suitable group for the preparation of the calibration formula because the content distribution was a normal, excluding the 13.0-15.5% content section. In order to verify the applicability of the NIRS prediction model, we measured the crude protein content of the 300 wheat germplasms that were not used for the calibration using both Kjeldahl analysis and NIR spectrum. The analysis value calculated using each method were statistically processed, and the test results and statistical indicators of the predictive model were compared. As a result, The R² value of the optimized NIRS prediction model was 0.997, and the Standard error of Calibration value(SEC) was 0.132, and slope value was 1.000. With prediction model selection, compared to Kjeldahl method, R² values were 0.994(Kjeldahl), 0.998(NIRS), and the SEC value were 0.191 and 0.132, respectively, comparing the statistical indices of the forecast model. And slope value were 1.013, 1.000, respectively. The analysis of crude protein content by the NIRS predictive model developed by each statistical index showing similar figures is judged to show a high degree of correlation with the Kjeldahl analysis. The proven calibration equation will be used to measure the crude protein content of wheat germplasms held by the National Agrobiodiversity Center, and by dividing the wheat germplasms by their use according to the crude protein content, it will provide useful information to relevant researchers.

• 한국세라믹학회지
• /
• 제24권1호
• /
• pp.47-55
• /
• 1987

The purpose of this work is to establish the basic calibration data for the efficiency of grinding by investigating the Bond's Work Index employing Korean Kaolin as a reference mateial with the laboratory-scale ball mill. A small ordinary ball mill has a dimension of 133 inside diameter and 144mm long. The analysis of the experimental results in this work sets up a equivalent calibration method with the laboratory-scale ball mill to those with special mill. The theoretical expression, derived from the rate equation proposed by Miwa, is obtained to anticipitate the stable revolution number for the next grinding cycle. The proposed equation is more systematic and acurate than lshihara's empirical equation is more systematic and acurate than lshihara's empirical equation for the measurement of gindability of a ball mill.

• International Journal of Aeronautical and Space Sciences
• /
• 제11권3호
• /
• pp.234-239
• /
• 2010

The utilization of micro-electro-mechanical system (MEMS) gyros and accelerometers in low-level inertial measurement unit (IMU) influences cost effectiveness in a positive way under the condition that device error characteristics are fully calibrated. The conventional calibration process utilizes a rate table; however, this paper proposes a new method for achieving reference calibration data from the natural motion of pendulum to which the IMU undergoing calibration is attached. This concept was validated with experimental data. The pendulum angle measurements correlate extremely well with the solutions acquired from the pendulum equation of motion. The calibration data were computed using the regression method. The whole process was validated by comparing the measurement from the 6 sensor components with the measurements reconstructed using the identified calibration data.

• 산업공학
• /
• 제6권1호
• /
• pp.55-65
• /
• 1993

A nonstandard instrument used in the filed frequently becomes out-of-calibration due to environmental noise, misuse, aging, etc. A substantial amount of loss may result if such nonstandard instrument is used to check product quality and performance. Traditional periodic calibration at the calibration center is not capable of detecting out-of-calibration status while the instrument is in use, and therefore, statistical methods need to be developed to check the status of a nonstandard instrument in the field between calibrations. Developed in this paper is a unified measurement assurance model in which statistical calibration at the calibration center and measurement assurance test in the filed are combined. We developed statistical procedures to detect changes in precision and in the coefficients of the calibration equation. Futher, computational experiments are conducted to evaluate how the power of test varies with respect to the parameters involved. Based upon the computational results we suggest procedures for designing effective measurement assurance tests.

• 한국약용작물학회지
• /
• 제10권5호
• /
• pp.340-343
• /
• 2002

삼지구엽초에 함유되어 있는 icariin 함량을 신속하게 추정하기 위하여 NIRS(근적외선 분광분석기)를 이용한 분석 방법을 검토하였다. HPLC를 이용하여 분석된 삼지구엽초 유전자원 150계통에 대한 이카린 함량치를 NIRS 스펙트럼에 적용시켜 42개의 calibration set 와 26개의 valilion set를 구분하였다. NIRS의 검량식을 몇가지 방법에 의하여 비교분석한 결과 2차미분된 스텍트럼을 MPLS(Modified Partial Least Squares)를 이용한 회귀식에 이용하는 것이 가장 적합하였다. HPLC를 이용한 유전자원들의 이카린 함량은 평균 $0.424%(0.12{\sim}0.67%)$이었으며, NIRS에서 도출된 검량식과의 상관계수는 0.951을 나타내었다. 따라서 삼지구엽초의 이카린 함량은 NIRS를 이용하여 신속 편리하게 분석할 수 있음이 인정되었다.

• 대한공간정보학회지
• /
• 제5권1호
• /
• pp.159-165
• /
• 1997

CCD 사진기는 수치영상을 별도의 처리과정 없이 실시간으로 얻을 수 있기 때문에 그 효용성이 날로 증대되고 있다. 본 연구에서는 CCD 사진기의 검정을 위해서 직접선형변환식과 방사 및 편심 왜곡을 검정하기 위한 검정식을 결합한 모형식을 구성하고 3차원 실험모형을 이용해서 검정계수들을 구하였다. CCD 사진기에 의한 수치영상을 상관계수를 이용하여 정합하고 대상물의 3차원 위치를 구함으로써 근거리 사진측량에서의 CCD 사진기 활용 가능성을 확인하였다.