• 제목/요약/키워드: calibration equation

검색결과 311건 처리시간 0.032초

Measurement of lipid content of compost fermentation using near-infrared spectroscopy

  • Daisuke Masui;Suehara, Ken-ichiro;Yasuhisa Nakano;Takuo Yano
    • Near Infrared Analysis
    • /
    • 제2권1호
    • /
    • pp.37-42
    • /
    • 2001
  • Near infrared spectroscopy (NIRS) was applied to determination of the lipid content of the compost during the compost fermentation of tofu (soybean0curd) refuse. The absorption of lipid observed at 5 wavelengths, 1208, 1712, 1772, 2312 and 2352 nm on the second derivative spectra. To formulated a calibration equation, a multiple linear regression analysis was carried out between the near-infrared spectral data and on the lipid content in the calibration sample set (sample number, n=60) obtained using Soxhlet extraction method. The value of the multiple correlation coefficient (R) was 0.975 when using the wavelengths of 1208 and 1712 nm were used in the calibration equation. To validate the calibration equation obtained, the lipid content in the validation sample set (n=35) not used for formulating the calibration equation was calculated using the calibration equation, and compared with the value obtained using the Soxhlet extraction method. Good agreement was observed between the results of the Soxhlet extraction method and those values of the NIRS method. The simple correlation coefficient (r) and standard error of prediction (SEP) were 0.964 and 0.815 %, respectively. suitability of the lipid content as an indicator of the compost fermentation of tofu refuse was also studied. The decrease of the lipid content in the compost corresponded to the decrease of the total dry weight of the compost in the composter. The lipid content was a significant indicator of the compost fermentation. The NIRS method was applied to measure the time course of the lipid content in the compost fermentation and good results were obtained. The study indicates that NIRS is a useful method for process management of the compost fermentation of tofu refuse.

벼 생체엽신 질소함량 측정을 위한 근적외선분광분석의 검량식 작성 (Determination of Calibration Curve for Total Nitrogen Contents Analysis in Fresh Rice Leaves Using Visible and Near Infrared Spectroscopy)

  • 권영립;백미화;최동칠;최정식;최영근
    • 한국작물학회지
    • /
    • 제50권6호
    • /
    • pp.394-399
    • /
    • 2005
  • 벼 영양진단에서 중요한 성분인 생체잎의 질소함량을 NIRS를 이용하여 신속하고 정확하게 분석하기 위해 최적의 검량식 작성에 관한 일련의 시험을 실시한 결과는 다음과 같다. 벼 생체엽 질소함량 검량식의 결정계수는 익산, 정읍, 부안지역이 각각 0.879, 0.858, 0.819였다. Outlier를 제거한 후 검량식을 다시 작성한 결과 0.896, 0.878, $0.88\%$로 각각 0.017, 0.02, 0.061씩 향상되었다. Merge 기능을 이용하여 검량식을 합병한 후 검량식을 다시 작성한 결과 0.971로 정확도가 더욱 향상되었다. 벼 생체엽의 질소함량 검량식에 의한 분석값과 습식분석 평균값의 차이는 $0.001\%$를 나타냈다. 이와 같은 결과로서 건조와 분쇄과정을 생략하기 때문에 시료의 변질을 막을 수 있고 시간과 비용을 줄일 수 있는 벼 생잎의 질소농도 측정이 근적외분석기술에 의해 가능할 것으로 판단되었다.

3차원 시각 센서를 탑재한로봇의 Hand/Eye 캘리브레이션 (Hand/Eye calibration of Robot arms with a 3D visual sensing system)

  • 김민영;노영준;조형석;김재훈
    • 제어로봇시스템학회:학술대회논문집
    • /
    • 제어로봇시스템학회 2000년도 제15차 학술회의논문집
    • /
    • pp.76-76
    • /
    • 2000
  • The calibration of the robot system with a visual sensor consists of robot, hand-to-eye, and sensor calibration. This paper describe a new technique for computing 3D position and orientation of a 3D sensor system relative to the end effect of a robot manipulator in an eye-on-hand robot configuration. When the 3D coordinates of the feature points at each robot movement and the relative robot motion between two robot movements are known, a homogeneous equation of the form AX : XB is derived. To solve for X uniquely, it is necessary to make two robot arm movements and form a system of two equation of the form: A$_1$X : XB$_1$ and A$_2$X = XB$_2$. A closed-form solution to this system of equations is developed and the constraints for solution existence are described in detail. Test results through a series of simulation show that this technique is simple, efficient, and accurate fur hand/eye calibration.

  • PDF

Radiometric Calibration Method with Compensation of Nonlinearity of Detector for Hyper-Spectral Camera

  • Yang, Ji-Hyeon;Choi, Byung-In;Park, Hee Duk;Kim, Sohyun;Park, Yong Chan
    • 한국컴퓨터정보학회논문지
    • /
    • 제22권10호
    • /
    • pp.27-34
    • /
    • 2017
  • In this paper, we propose a novel radiometric calibration method which can effectively compensate the nonlinearity of the detector for hyper-spectral camera. In general, the detector of hyper-spectral camera can produce nonlinear output depending on radiance and integral time. The conventional radiometric calibration methods extract the imprecise radiance profile from the spectral profile of the target due to this nonlinearity. In our proposed method, we use a quadratic equation instead of a linear equation to describe the relation between output of detector and radiance. Then, we use a fractional function to compensate variation of integration time. Thus, our proposed method can extract more precise spectral profile of radiance than conventional radiometric calibration method.

Measurement of Lipid Content of Compost in the fermentation Process using Near-Infrared Spectroscopy

  • Suehara, Ken-Ichiro;Masui, Daisuke;Nakano, Yasuhisa;Yano, Takuo
    • 한국근적외분광분석학회:학술대회논문집
    • /
    • 한국근적외분광분석학회 2001년도 NIR-2001
    • /
    • pp.1254-1254
    • /
    • 2001
  • Near infrared spectroscopy (NIRS) was applied to determination of the lipid content of compost during compost fermentation of tofu(soybean-curd) refuse. The reflected rays in the wavelength range between 800 and 2500 nm were measured at 2 nm intervals. The absorption of lipid observed at 4 wavelengths, 1208, 1712, 2312 and 2352 nm on the second derivative spectra. To formulate a calibration equation, a multiple linear regression analysis was carried out between the near-infrared spectral data and on the lipid content in the calibration sample set (sample number, n=60) obtained using a Soxhlet extraction method. The calibration equation for prediction of lipid, the value of the multiple correlation coefficient (R) was 0.975 when using the wavelengths of 1208 and 1712nm. To validate the calibration equation obtained, the lipid content in the validation sample set (n=35) not used for formulating the calibration equation were calculated using the calibration equations, and compared with the values obtained using the Soxhlet extraction method. Good agreement were observed between the results of the Soxhlet extraction method and those values of the NIRS method. The simple correlation coefficient (r) and standard error of prediction (SEP) were 0.964 and 0.815 %, respectively. Then, the NIRS method was applied to a compost fermentation in which the time course the lipid content were measured and good results were obtained. The study indicates that NIRS is a useful method for process management of the compost fermentation of tofu refuse.

  • PDF

Relationship between porcine carcass grades and estimated traits based on conventional and non-destructive inspection methods

  • Lim, Seok-Won;Hwang, Doyon;Kim, Sangwook;Kim, Jun-Mo
    • Journal of Animal Science and Technology
    • /
    • 제64권1호
    • /
    • pp.155-165
    • /
    • 2022
  • As pork consumption increases, rapid and accurate determination of porcine carcass grades at abattoirs has become important. Non-destructive, automated inspection methods have improved slaughter efficiency in abattoirs. Furthermore, the development of a calibration equation suitable for non-destructive inspection of domestic pig breeds may lead to rapid determination of pig carcass and more objective pork grading judgement. In order to increase the efficiency of pig slaughter, the correct estimation of the automated-method that can accommodate the existing pig carcass judgement should be made. In this study, the previously developed calibration equation was verified to confirm whether the estimated traits accord with the actual measured traits of pig carcass. A total of 1,069,019 pigs, to which the developed calibration equation, was applied were used in the study and the optimal estimated regression equation for actual measured two traits (backfat thickness and hot carcass weight) was proposed using the estimated traits. The accuracy of backfat thickness and hot carcass weight traits in the estimated regression models through stepwise regression analysis was 0.840 (R2) and 0.980 (R2), respectively. By comparing the actually measured traits with the estimated traits, we proposed optimal estimated regression equation for the two measured traits, which we expect will be a cornerstone for the Korean porcine carcass grading system.

레이저 섬광법에 의한 열확산계수 측정시 적외검출소자에서 실시간 온도보정이 미치는 영향 (Effects of the in-process calibration from IR detector for thermal diffusivity measurement by laser flash method)

  • 이원식;배신철
    • 설비공학논문집
    • /
    • 제10권6호
    • /
    • pp.795-802
    • /
    • 1998
  • For measuring the thermal diffusivity by laser flash method, raw data have to be calibrated using temperature data. We have developed in-process calibration method and polynomial calibration in which thermal diffusivity can be calibrated during measuring, This method is different from existing temperature pre-process calibration method and exponential calibration having various source of error. Using this new calibration method, measurement accuracy was improved about 1∼2% compare to the value by the existing method. We also studied more accurate fitting curve as in Figure 4 was shown the result of measuring output characteristics of IR radiometer with temperature. As illustrated in data, in-process calibration method and polynomial calibration equation is proper than pre-process calibration method and exponential calibration.

  • PDF

근적외선분광분석기를 이용한 미강의 Tocopherol과 Tocotrienol 함량 분석 (Quantification of Tocopherol and Tocotrienol Content in Rice Bran by Near Infrated Reflectance Spectroscopy)

  • 김용호;강창성;이영상
    • 한국작물학회지
    • /
    • 제49권3호
    • /
    • pp.211-215
    • /
    • 2004
  • 미강에 함유되어 있는 토코페롤 및 토코트리에놀의 함량을 비파괴적으로 신속하게 추정하기 위하여 NIRS(근적외선 분광분석기)를 이용한 분석 방법을 검토하였다. 벼 유전자원 80계통의 미장을 사용하여 HPLC에서 분석된 토코페롤 및 토코트리에놀의 함량치를 NIRS 스펙트럼에 적용시킨 후 검량식을 작성하였다. NIRS의 검량식을 몇가지 방법에 의하여 비교 분석한 결과 2차 미분된 스펙트럼을 MPLS(Modified Partial Least Squares)를 이용한 회귀식에 이용하는 것이 가장 적합하였다. HPLC를 이용한 유전자원들의 성분 함량과 NIRS에서 도출된 검량식과의 상관계수는 토코페롤과 토코트리에놀이 각각 0.992, 0.953을 나타내었다. 이들 검량식은 validation file 에서도 0.846 및 0.956의 높은 상관을 보여 미강 상태에서 토코페롤 및 토코트리에놀의 함량을 NIRS를 이용하여 신속하게 분석할 수 있을 것으로 판단되었다.

근적외선분광광도계(NIRS)를 이용한 국내산 콩과 수입콩의 판별분석 (Discrimination of Korean Domestic and Foreign Soybeans using Near Infrared Reflectance Spectroscopy)

  • 안형균;김용호
    • 한국작물학회지
    • /
    • 제57권3호
    • /
    • pp.296-300
    • /
    • 2012
  • 국내산 콩과 수입콩의 판별에 NIRS를 도입함으로써 보다 빠르고 정확한 식별분석을 하고자 실험을 수행하였다. NIRS를 사용하여 400~2,500 nm 범위에서 콩 분말의 파장을 측정하였으며, 측정된 spectrum은 WINISI II program 을 이용하여 수처리와 회귀분석을 하였다. 검량식 작성을 위한 수처리는 spectrum을 1차미분 및 4 nm gap으로 조정한 것이 가장 적합하였으며, 회귀식은 변형부분최소자승회귀법(Modified partial least squares regression)이 우수하였다. MPLS 회귀분석시 원산지 판별을 위해 loading value를 국내산 콩은 '100', 수입콩은 '1'로 처리하여 검량식을 작성하고 그 적합성을 검증한 결과 factor가 10일 때 도출된 calibration equation의 상관값이 0.98, 교차검증의 상관값이 0.94를 나타내어 상관도가 높음을 알 수 있었다. 따라서 NIRS를 이용한 국내산 콩과 수입콩의 판별분석이 가능할 것으로 판단되었다.

Studies on pharmaceutical assay method using Near Infrared Spectroscopy (NIRS) (II)

  • Kang, Shin-Jung;Yun, Mi-Ok;Lee, Su-Jung;Choi, Hyun-Chul;Kim, Ho-Jeong;Kim, Ji-Yeon
    • 한국근적외분광분석학회:학술대회논문집
    • /
    • 한국근적외분광분석학회 2001년도 NIR-2001
    • /
    • pp.4113-4113
    • /
    • 2001
  • This study developed effective assay method of pharmaceutical quality control was developed by near-infrared spectroscopy (NIRS). The calibration equation model of assay was developed by 2nd deriviative PLS(Partial Least Squares) regression method with NIRS over the wavelength range from 1100 to 1400nm using diazepam tablets (2mg, 5mg). Although diazepam tablets are made by 5-different manufacture, they have similar formulation. When the correlation was compared with values by NIRS and HPLC, the R-2s and standard error of calibration (SEC) for 2mg were 0.9300 and 0.98%, the R-2s and SEC for 5mg were 0.9165 and 0.63%. The validation of the calibration equation model yield that the R-2s and standard error of prediction (SEP) for 2mg were 0.9611 and 0.995%, the R-2s and SEP for 5mg were 0.9114 and 0.842%. The method was validated on assay method for diazepam tablets by the calibration equation.

  • PDF