• 접착 및 계면
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• 제7권4호
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• pp.60-64
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• 2006

In modern vehicle construction the search for means of weight reduction, improving durability, increasing comfort and raising body stiffness are issues of priority to the design engineer. The intelligent usage of many materials such as high strength steel, light-alloys and plastics enables a significant vehicle weight reduction to be achieved. The classical joining techniques used in the automobile industry need to be newly-evaluated since they often do not present workable solutions for such mixed-material connections, for example aluminium/steel. Calculation/simulation methods have made progress as a key factor for broader and more cost-effective implementation of structural bonding. This will lead to reduction of spotwelds and accelerate the car development. A special focus of the paper is the use of high strength steel grades. It will be shown that adhesive bonding is a key tool for yielding the potential of advanced high strength steel for low gauging without compromising the stiffness. The latest status of adhesive development has been described. Improvements with physical strength and glass temperature as well as of process relevant properties are shown. Also the situation regarding occupational hygiene is treated, showing that by further spotweld point reduction the emission around the working area can be even lowered against the current praxis. High performing lightweight design cannot longer do without high performing crash durable adhesives.

• 한국표면공학회지
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• 제29권5호
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• pp.549-555
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• 1996

Diamond Like Carbon film is amorphous film which is considered to consist of three coordinate graphite structure and tetrahedron coordinate diamond structure. Its hardness, thermal conductivity and chemical stability are nearly to one of diamond. It is well known to become semi-conductor by doping of inpurity. In this study Diamond Like Carbon film was synthesized by Microwave Plasma CVD in the gas mixture of hydrogen-methan-nitrogen and doped of nitrogen on the single-crystal silicon or silica glass. The temperature of substrate and nitrogen concentration in the gas mixture had an effect on the bonding state, structural properties and conduction mechanism. The surface morphology was observed by Scanning Electron Microscope. The strucure was analyzed by laser Raman spectrometry. The bonding state was evaluated by electron spectroscopy. Diamond Like Carbon film synthesized was amorphous carbon containing the $sp^2$ and $sp^3$ carbon cluster. The number of $sp^2$ bonding increased as nitrogen concentration increased from 0 to 40 vol% in the feed gas at 1233K substrate temperature and at $7.4\times10^3$ Pa. Increase of nitrogen concentration made Diamond Like Carbon to be amorphous and the doze of nitragen could be controlled by nitrogen concentration of feed gas.

• 한국안전학회지
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• 제38권2호
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• pp.1-7
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• 2023

Fiber-metal laminates (FMLs) and polymer matrix composites (PMCs) are formed in various ways. In particular, FMLs in which aluminum is laminated as a reinforced layer are widely used. Also, glass fiber-reinforced plastics (GFRPs) are generally applied as fiber laminates. The bonding interface layer between the aluminum and fiber laminate exhibits low strength when subjected to hot press fabrication in the event of delamination fracture at the interface. This study presents a simple method for strengthening the interface bonding between the aluminum metal and GFRP layer of FML composites. The surfaces of the aluminum interface layer are engraved with three kinds of patterns by using the laser machine before the hot press works. Furthermore, the effect of the laser patterns on the interfacial toughness is investigated. The interfacial toughness was evaluated by the energy release rate (G) using an asymmetric double cantilever bending specimen (ADCB). From the experimental results, it was shown that the strip type pattern (STP) has the most proper pattern shape in GFRP/Al FML composites. Therefore, this will be considered a useful method for the safety assessment of FML composite structures.

• 한국정밀공학회지
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• 제17권6호
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• pp.103-110
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• 2000

In this study, the angular twist type torque-meter was designed and manufactured with STS 304 and fiber-reinforced composite materials to improve the dynamic properties of the existing torque-meter. From the Experimental and analytical results, it was found that the dynamic characteristics of co-cured bonded torque-meter rotating shaft were better than those of the adhesively and unreinforced torque-meter rotating shaft. For the torque-meter rotating shaft manufactured by co-cured bonded with the glass fiber-epoxy composite and with a stacking sequence of $[$\pm$30$^{\circ}$/STS304]_{2s}$, the natural frequency and the radial spring constant were increased by 64% and 137% compared to those of the unreinforced torque-meter rotating shaft.

• 한국안광학회지
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• 제6권1호
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• pp.87-91
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• 2001

PECVD 방법으로 60 Hz 상용전원을 사용하여 발생한 아세틸렌 플라스마로부터 다이아몬드성 탄소박막을 제작하고 Raman 분광에 의하여 D($sp^3$)와 G($sp^2$) 피크를 관측하여 박막의 다이아몬드성 정도를 확인하였고 $sp^3$와 $sp^2$의 비율과 FTIR 결과로부터 박막내의 수소함량의 측정을 통하여 아세틸렌 분압비와의 연관성을 확인하였다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2000년도 하계학술대회 논문집 C
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• pp.1800-1802
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• 2000

본 연구에서는 냉음극 발광 소자인 FEA를 이용하여 Cold Cathode Lamp 제작과 그 구조에 대해서 연구하였다. Anode plate에는 ZnO:Zn 형광체를 전기영동법으로 증착한 후 tube slabs와 anode plate를 frit glass를 이용하여 접합하였다. FEA와 substrate의 bonding, addressing을 위한 wire bonding, substrate와 집속전극, setter를 stem base의 외부전극에 연결하기 위한 spot welding, tube와 stem base를 glass melting method로 접합 공정을 하였다. 진공배기 시스템에 배기판을 연결하여 ${\sim}10^{-7}$torr까지 배기한 후 heater를 이용하여 배기관을 tip-off하였다. 최종적으로 진공을 유지하기 위해 getter를 RF 고주파로 활성화하였다. 결론적으로 lamp외 특성을 비교분석한 후 휘도 및 발광효율을 향상시키기 위한 구조절 개선과 방안을 고찰하였다.

• 한국세라믹학회지
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• 제27권6호
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• pp.755-762
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• 1990

The tungsten paste was printed on the surface of 92% alumina sheet which was made by type casting process. The printed tungsten was bonded on the Al2O3 by co-firing in reducing atmosphere. During the co-firing, the binder burn-out was easier in wet H2 atmosphere than in dry H2, which affected sintered density. In practically, the use of wet H2 above 100$0^{\circ}C$ was beneficial for density of alumina and bond strength. This phenomena occured more distinctly when atmosphere varied from dry H2 to wet H2 than varied dew point in wet H2. In wet H2, the improvement in bonding strength can be attributed to good glass migration into the metal layer due to inhibition of the tungsten particle growth, with increase of alumina density, at the temperatrue higher than 100$0^{\circ}C$.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2000년도 하계학술대회 논문집
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• pp.561-564
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• 2000

Silicon capacitive pressure sensor has been fabricated by using electrochemical etching stop and silicon-to-glass electrostatic bonding technique. A diaphragm structure is designed to compensate the nonlinear response. A cavity is etched into the silicon to the depth of 2$\mu\textrm{m}$ by anisotropic etching in 20wt.% TMAH solution at 80$^{\circ}C$. A fabricated sensor showed 3.3 pF zero-pressure capacitance, 297 pp.m/mmHg sensitivity, and a 7.4 7%F.S. nonlinear response in a 0-1 kgf/cm$^2$pressure range.

• 한국결정성장학회지
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• 제17권2호
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• pp.82-89
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• 2007

붕규산염계 유리에 EAF Dust를 $40{\sim}80wt%$ 첨가하고 후 용융하여 유리를 제조한 후 $700^{\circ}C$/10hr으로 열처리하여 결정화유리 시편을 합성하였다. FT-IR, SEM, 그리고 EDS 분석을 통하여 조성 및 열처리 조건에 따른 시편내 결정상 및 결합상태 변화를 관찰하고, 이를 TCLP(Toxic Characterization Leaching Procedure) 실험에서 얻은 결과와 연계시켜 시편의 화학적 내구성을 연구하였다. 유리에 더스트 첨가량이 증가함에 따라 FT-IR 스펙트럼 상의 가교산소 진동피크($1050{\sim}1060cm^{-1}$)와 비가교산소 진동피크($960cm^{-1}$)가 합쳐진 넓은 피크($1000cm^{-1}$ 부근)가 저파수쪽으로 이동하였다. 동시에 boroxol ring의 $B_2O_3$ 구조가 tetrhedral-, trigonal- 그리고 di-borate로 변화되는 것을 확인하였다. 결정화유리 시편에서 Fe-O 피크가 확인되었으며 이는 spinel이 생성되었다는 XRD 결과와 일치하였다. TCLP를 행한 유리시편의 표면은 균열이 심하였으나 결정화유리는 큰 변화가 없어, 결정상 생성이 화학적 내구성을 향상시킴을 확인하였다. Fe의 용출량은 더스트가 80wt% 첨가된 결정화유리의 경우, 유리시편에 비하여 1/15로 감소하였다. Zn은 더스트 첨가량이 70wt% 이하인 결정화유리에서 용출량이 유리에 비해 높았으나 80wt% 이상 시편에서는 유리보다 감소하였고 이는 willemite 생성과 연관이 있는 것으로 사료된다.

• 대한치과교정학회지
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• 제30권1호
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• pp.83-89
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• 2000

레진 강화형 글래스 아이오노머 시멘트의 접착 강도를 알아보고, 타액 오염이 접착제의 종류에 따라 접착 강도에 어떠한 영향을 미치는지 관찰하여 봄으로써 임상적 효용성을 알아보기 위하여 본 연구를 시행하였다. 교정 치료를 목적으로 발거된 소구치에 교정용 복합 레진 접착제로 Ortho-One, 레진 강화형 글래스 아이오노머 시멘트로는 Fuji Ortho LC, Vitremer, Advance를 사용하여 통상적인 과정의 브라켓 접착을 하였으며, 타액 오염군은 타액 오염후에 건조 한 뒤 브라켓을 접착한 후 증류수에 침적하고 $37^{\circ}C$ 항온조에 24시간 보관하였다. 만능시험기로 인장 접착 강도를 측정하여 다음과 같은 결과를 얻었다. 1. 통상의 방법으로 브라켓을 부착한 경우 인장 접착 강도는 Ortho-One군에서는 $7.68\pm1.76$ 이었으며, Advance군에 서는 $7.87\pm2.80$, Fuji Ortho LC군에서는 $4.99\pm2.53$, Vitremer군에서 는 $2.80\pm0.88$ MPa 나타났다. 타액 오염시킨 경우 인장 접착 강도는 Ortho-One군에서 는 $4.12\pm1.67$, Advance군에서는 $5.37\pm0.68$, Fuji Ortho LC군에서는 $4.41\pm1.61$, Vitremer군에서는 $2.60\pm1.10$ MPa 로 나타났다. 2. 타액 오염시킨 경우 Fuji Ortho LC와 Vitremer는 거의 영향이 없었고 (p>0.05), Ortho-One과 Advance는 큰 폭의 접착 강도 저하 현상을 나타냈다 (p<0.05). 3. Advance와 Ortho-One, Fuji Ortho LC는 만족할 만한 인장 접착 강도를 나타내어 브라켓 접착시 임상적 유용성이 있으리라 생각된다.