• Journal of Technologic Dentistry
• /
• v.33 no.1
• /
• pp.47-54
• /
• 2011

Purpose: To investigate shear bonding strength between dental zirconia ceramics with different surface treatment and metal bracket. Methods: Zirconia ceramics(LAVA, 3M ESPE, USA) were divided to 4 groups according to their surface treatment; no surface treatment(G1), sand blasting(G2), silane coating(G3), and sand blasting+silane coating(G4). Specimens were bonded to metal bracket using resin bond($Transbond^{TM}XT$, 3M Unitek, USA). Shear bond strength was measured using universal test machine(3366 INSTRON. U.S.A) with cross head speed of 1 mm/min. Microstructural investigation for fracture surface was performed after shear test. Results: Shear bonding strengths of single surface treatment groups (G2 and G3) were higher than no treatment group(G1). Combined Treatment Group (G4) showed the highest shear bond strength of 9.15MPa. Microstructural observation shows that higher shear bonding strength was obtained when debonding was occurred at metal bracket/resin interface rather than zirconia ceramic/resin interface. Conclusion: Surface treatment of zirconia is necessary to obtain higher bonding strength. Combined treatment can be more effective when surface the surfaces are kept clean and homogeneous.

• Journal of the Korean Ceramic Society
• /
• v.37 no.3
• /
• pp.211-218
• /
• 2000

The attrition-milled powder mixtures of Al and Al2O3 were oxidized below 140$0^{\circ}C$ for 1 hr and post-sintered at 150$0^{\circ}C$ and 1$600^{\circ}C$ for 2 hr. During attrition milling, ZrO2 was added to the system by grinding effect of ZrO2 balls. The average particle size of the powder mixtures was decreased by the attrition milling as the aluminum content decrease. Above 120$0^{\circ}C$, sintering behaviro was observed on the fine Al2O3 particles resulted from the oxidation of Al. The specimens heat-treated at 140$0^{\circ}C$ for 1 hr showed the bending strength of 166 MPa and hardness of 220 MPa. The specimens post-sintered at 1$600^{\circ}C$ for 2hr had a linear shrinkage of 9~12% and a relative density of about 95%. After the post-sintering, the specimens having 55 vol% Al content revealed the bending strength of 513 MPa and hardness of 718 MPa. The Weibull modulus to the bending strength was about 16.

• Proceedings of the KIPE Conference
• /
• 2018.07a
• /
• pp.536-538
• /
• 2018

This paper introduces an enhanced interleaved (IL) PFC (Power Factor Correction) boost converter typed 650V Intelligent Power Module (IPM), which is fully optimized hybrid IGBT converter modules; Silicon (Si) IGBT and Silicon Carbide (SiC) diode, for up to 10kW HVAC (Heating, Ventilation, and Air Conditioning) systems. It utilizes newly developed $4^{th}$ Generation Field Stop (FS) trench IGBTs, $EXTREMEFAST^{TM}$ anti-paralleled diodes, SiC Junction Barrier Schottky (JBS) diodes, Bridge rectifiers, Multi-function LVIC, and Built-in thermistor provide good reliable characteristics for the entire system. This module also takes technical advantage of DBC (Direct Bonded Copper) substrate for the better thermal performance. It is shown that the Si IGBT/SiC diode hybrid IL PFC module can achieve excellent EMI performance and greatly enhance the power handling capability or switching frequency of various applications compared to the Si IGBT/Diode. This paper provides an overall description of the newly developed 650V/50A Hybrid SiC IL PFC IPM product.

• Bulletin of the Korean Chemical Society
• /
• v.28 no.1
• /
• pp.89-94
• /
• 2007

The new pinane derivative containing unique multifused ring system was synthesized. The crystal, molecular and electronic structure of the title compound has been determined. Both pinane ring systems have the same conformation. The five-membered oxazolidine ring exists in twisted chair conformation. The structure is expanded through O-H…O hydrogen bond to semiinfinite hydrogen-bonded chain. The bond lengths and angles in the optimised structure are similar to the experimental ones. The CH3 and CH2 groups (except this of oxazolidine ring) are negatively charged whereas the CH groups are positively charged. The largest negative potential is on the oxygen atoms. The C-N natural bond orbitals are polarised towards the nitrogen atom (ca. 61% at N) whereas the C-O bond orbitals are polarised towards the oxygen atom (ca. 67% at O). It is consistent with the charges on the nitrogen and oxygen atom of oxazolidine ring and the direction of the dipole moment vector (3.08 Debye).

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.20 no.4
• /
• pp.1275-1289
• /
• 1996

The plane elasticity problem of collinear cracks in a layered medium is investigated. The medium is modeled as bonded structure constituted from a surface layer and a semi-infinite substrate. Along the bond line between the two dissimilar homegeneous constituents, it is assumed that as interfacial zone having the functionally graded, nonhomogeneous elastic modulus exists. The layered medium contains three collinear cracks, one in each constituent material oriented perpendicular to the nominal interfaces. The stiffness matrix formulation is utilized and a set of homogeneous conditions relevant to the given problem is readily satisfied. The proposed mixed boundary value problem is then represented in the form of a system of integral equations with Cauchy-type singular kernels. The stress intensity factors are defined from the crack-tip stress fields possessing the standard square-root singular behavior. The resulting values of stress intensity factors mainly address the interactions among the cracks for various crack sizes and material combinations.

• Bulletin of the Korean Chemical Society
• /
• v.34 no.5
• /
• pp.1401-1406
• /
• 2013

This study tested the feasibility of observing H/D exchange of intact protein by top-down electron capture dissociation (ECD) mass spectrometry for the investigation of protein structure. Ubiquitin is selected as a model system. Local structural information was obtained from the deuteration levels of c and $z^{\cdot}$ ions generated from ECD. Our results showed that ${\alpha}$-helix region has the lowest deuteration level and the C-terminal fraction containing a highly mobile tail has the highest deuteration level, which correlates well with previous X-Ray and HDX/NMR analyses. We studied site-specific H/D exchange kinetics by monitoring H/D exchange rate of several structural motives of ubiquitin. Two hydrogen bonded ${\beta}$-strands showed similar HDX rates. However, the outer ${\beta}$-strand always has higher deuteration level than the inner ${\beta}$-strand. The HDX rate of the turn structure (residues 8-11) is lower than that of ${\beta}$-strands (residues 1-7 and residues 12-17) it connects. Although isotopic distribution gets broader after H/D exchange which results in a limited number of backbone cleavage sites detected, our results demonstrate that this method can provide valuable detailed structural information of proteins. This approach should also be suitable for the structural investigation of other unknown proteins, protein conformational changes, as well as protein-protein interactions and dynamics.

• Proceedings of the Korean Society of Propulsion Engineers Conference
• /
• 2017.05a
• /
• pp.517-520
• /
• 2017

In this paper, we represented the structural design parameter effect on the sealing gap behavior of solid rocket motor case and nozzle connection under penetrated pressure through the sealing path between insulation rubber and the ablative FRP bonded on the inside convergent wall of nozzle. It is important to keep the good sealing capacity during all the combustion time of SRM. To achieve the crucial role of sealing system of SRM, designers must consider design factors for stable sealing clearance gap as the nearly unchanged initial design state as possible for sufficient compression rate of O-ring under sealing gap pressure.

• Proceedings of the KIEE Conference
• /
• 2006.07c
• /
• pp.1623-1624
• /
• 2006

It is a paper for design, manufacture and estimation of industry inkjet head. Simulations for Actuator, Ink flow and Ejection are executed for securing design ability. Relations between droplet and properties of ink are explained closely through simulation for nozzle. Actually, two silicon plates are made by dry and wet etching and directly bonded. PZT materials is attached on the bended ink flow part and cut to $540{\mu}m$ interval by dicing saw. Actuator was seen variation within 10% between simulation and actual head. Through the ejection estimation, it is shown that stabilized driving voltages change according to viscosity and surface tension of metal ink. Using the metal ink of viscosity of 4.8 cps and surface tension of 0.025 N/m, it is possible to eject the stable droplets with 5m/s, 20 pl, 5 kHz.

• Computers and Concrete
• /
• v.2 no.5
• /
• pp.389-409
• /
• 2005

The Finite Element Analysis (FEA) is evidently a powerful tool for the analysis of structural concrete having nonlinearity and brittle failure properties. However, the result of FEA of structural concrete is sensitive to two modeling factors: the shear transfer coefficient (STC) for an open concrete crack and force convergence tolerance value (CONVTOL). Very limited work has been done to find the optimal FE Modeling (FEM) methodologies for structural concrete members strengthened with externally bonded FRP sheets. A total of 22 experimental deep beams with or without FRP flexure or/and shear strengthening systems are analyzed by nonlinear FEA using ANAYS program. For each experimental beams, an FE model with a total of 16 cases of modeling factor combinations are developed and analyzed to find the optimal FEM methodology. Two elements the SHELL63 and SOLID46 representing the material properties of FRP laminate are investigated and compared. The results of this research suggest that the optimal combination of modeling factor is STC of 0.25 and CONVTOL of 0.2. A SOLID 46 element representing the FRP strengthening system leads to better results than a SHELL 63 element does.

• Steel and Composite Structures
• /
• v.32 no.1
• /
• pp.127-139
• /
• 2019

Bridges, offshore oil platforms and other infrastructures usually require at some point in their service life rehabilitation for reasons such as aging and corrosion. This study explores the application of adhesively bonded CFRP patches in repair of corroded circular hollow sectional (CHS) steel beams. An experimental program involving three-point bending tests was conducted on intact, corroded, and repaired CHS beams. Meso-scale finite element (FE) models of the tested beams were developed and validated by the experimental results. A parametric study using the validated FE models was performed to examine the effects of different CFRP patch parameters, including patch dimensions, number of plies and stacking sequence, on efficiency of the repair system. Results indicates that the corrosion reduced elastic stiffness and flexural strength of the undamaged beam by 8.9 and 15.1%, respectively, and composite repair recovered 10.7 and 18.9% of those, respectively, compared to undamaged beam. These findings demonstrated the ability of CFRP patch repair to restore full bending capacity of the corroded CHS steel beam. The parametric study revealed that strength and stiffness of the repaired CHS beam can be enhanced by changing the fiber orientations of wet composite patch without increasing the quantity of repair materials.