• The Journal of Advanced Prosthodontics
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• 제6권6호
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• pp.451-455
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• 2014

PURPOSE. The most common failure seen in restorations with a zirconia core is total or layered delamination of the ceramic veneer. In the present study, the shear bond strengths between veneering ceramics and colored zirconia oxide core materials were evaluated. MATERIALS AND METHODS. Zirconia discs ($15{\times}12{\times}1.6mm$) were divided into 11 groups of 12 discs each. Groups were colored according to the Vita Classic scale: A3, B1, C4, D2, and D4. Each group was treated with the recommended shading time for 3 s, or with prolonged shading for 60 s, except for the control group. Samples were veneered with 3 mm thick and 3.5 mm in diameter translucent ceramic and subjected to shear test in a universal testing machine with a crosshead speed of 1 mm/min. One-way analysis of variance (ANOVA) and Tukey's HSD tests were used for comparisons of the groups having the same shading times. A paired t-test was used for groups of the same color (3 s/60 s). RESULTS. Among the 11 groups investigated C4 (3 s) had the highest bond strength with a value of 36.40 MPa, while A3 (3 s) showed the lowest bond strength with a value of 29.47 MPa. CONCLUSION. Coloring procedures can affect zirconia/ceramic bond strength. However, the results also showed that bond strengths of all the investigated groups were clinically acceptable.

• 대한기계학회논문집A
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• 제32권7호
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• pp.569-575
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• 2008

In this study, disk type of thermal barrier coating system for gas turbine blade was isothermally aged in the furnace changing exposure time and temperature. For each aging condition, bond tests for three samples were conducted for evaluating degradation of adhesive or cohesive strength of thermal barrier coating system. For as-sprayed condition, the location of fracture in the bond test was in the middle of epoxy which have bond strength of 57 MPa. As specimens are degraded by thermal aging, bond strength gradually decreased and the location of failure was also changed from within top coat at the earlier stage of thermal aging to the interface between top coat and TGO at the later stage due to the delamination in the coating.

• 한국강구조학회 논문집
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• 제27권4호
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• pp.359-370
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• 2015

본 연구에서는 AFRP 스트립과 강재사이의 부착거동에 관한 실험적 연구를 수행하였다. 실험적 연구를 통해 AFRP 판과 강판사이의 계면부착거동을 관찰하고, 계면부착응력을 산정하는 것이 본 연구의 목표이다. 실험변수로는 부착길이와 AFRP의 두께를 선택하였으며, 18개의 일면전단시편 제작하여 실험을 수행하였다. 실험결과 부착길이와 AFRP 두께가 증가함에 따라 하중값을 증가하였으며, 부착길이와 AFRP 두께가 증가함에 따라 각각 63%, 86%의 하중값이 증가하였다. 끝으로 강재와 AFRP 사이의 부착응력-슬립관계를 산정하였다. 부착응력-슬립관계는 탄성선형거동을 보이고 있으며, 부착길이와 AFRP 두께는 부착응력과 파괴에너지에 영향을 덜 미치는 것으로 나타났다.

• Journal of Welding and Joining
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• 제19권2호
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• pp.221-227
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• 2001

Based on the principle of complementary energy, an analytical method is developed which focuses on the end effects for determining thermal stress distributions in a three-layered beam. This method gives the stress distributions which completely satisfy the stress-free boundary conditions. A numerical example is given in order to verify this method. The results show that the present analytical solutions have the values of stress in excellent agreement with the solutions derived by other investigators. Using this method, the effects of the thickness of bond coat on the thermal stresses of a typical sprayed thermal barrier coating, which consists of IN738LC substrate, MCrAIY bond coat and ZrO$_2$-8wt%Y$_2$O$_3$top coat, were investigated.

• Journal of the Korean Wood Science and Technology
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• 제37권4호
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• pp.357-363
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• 2009

본 연구에서는 작업성과 경제성을 고려하여 집성재 제작용 접착제를 목재와 유리섬유강화플라스틱(GFRP: Glass fiber reinforced plastic) 접착에 적용할 수 있는지를 검토하였다. 복합집성재는 접착제 종류와 혼합비에 따라 6가지 타입으로 제작하여 블록전단강도시험과 침지박리, 삶음박리 시험을 실시하였다. 레조시놀수지 접착제와 초산비닐 수지접착제, 에폭시수지 접착제를 사용한 복합집성재 3가지 타입과 레조시놀수지 접착제와 초산비닐수지 접착제를 혼합한 3가지 타입으로 총 6가지 타입으로 제작하였다. 블록전단시험 결과 모든 타입의 복합집성재가 KS F 3021 기준 $7.1N/mm^2$ 보다 높아 전단강도는 양호하였지만, 목파율에서는 초산비닐수지접착제가 65.9%로 가장 우수한 접착 성능을 나타내었다. 박리시험에서는 초산비닐수지 접착제를 사용한 경우 GFRP 접착층까지 포함된 경우 침지 박리는 1.08%, 삶음박리는 4.16%로 KS F 3021 합격기준인 5% 이하를 만족하였다. 레조시놀수지 접착제만을 사용 한 경우 목재 접착층은 침지박리 1.26%, 삶음박리 0%로 합격기준을 만족하였으나 GFRP 접착층을 포함시킬 경우 침지박리는 21.85%로 합격기준을 만족하지 못하였고 삶음박리의 경우만 1.45%로 만족하였다.

• The Journal of Advanced Prosthodontics
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• 제1권3호
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• pp.129-135
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• 2009

STATEMENT OF PROBLEM. Zirconia-based restorations have the common technical complication of delamination, or porcelain chipping, from the zirconia core. Thus the shear bond strength between the zirconia core and the veneering porcelain requires investigation in order to facilitate the material's clinical use. PURPOSE. The purpose of this study was to evaluate the bonding strength of the porcelain veneer to the zirconia core and to other various metal alloys (high noble metal alloy and base metal alloy). MATERIAL AND METHODS. 15 rectangular ($4\times4\times9mm$) specimens each of zirconia (Cercon), base metal alloy (Tillite), high noble metal alloy (Degudent H) were fabricated for the shear bond strength test. The veneering porcelain recommended by the manufacturer for each type of material was fired to the core in thickness of 3mm. After firing, the specimens were embedded in the PTFE mold, placed on a mounting jig, and subjected to shear force in a universal testing machine. Load was applied at a crosshead speed of 0.5mm/min until fracture. The average shear strength (MPa) was analyzed with the oneway ANOVA and the Tukey's test ($\alpha$= .05). The fractured specimens were examined using SEM and EDX to determine the failure pattern. RESULTS. The mean shear strength ($\pm\;SD$) in MPa was 25.43 ($\pm\;3.12$) in the zirconia group, 35.87 ($\pm\;4.23$) in the base metal group, 38.00 ($\pm\;5.23$) in the high noble metal group. The ANOVA showed a significant difference among groups, and the Tukey' s test presented a significant difference between the zirconia group and the metal group. Microscopic examination showed that the failure primarily occurred near the interface with the residual veneering porcelain remaining on the core. CONCLUSION. There was a significant difference between the metal ceramic and zirconia ceramic group in shear bond strength. There was no significant difference between the base metal alloy and the high noble metal alloy.

• Journal of the Korean Wood Science and Technology
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• 제20권2호
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• pp.9-22
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• 1992

The aim of this research was to investigate physical and mechanical properties of various composition panels, each fabricated with a ratio of fiber to particle of 2 to 10. Type A consisted of fiber-faces and particle-core in layered-mat system. Type B consisted of fiberboard-faces on particleboard-core. Type C consisted of fibers and particles in mixed-mat system. The results obtained from tests of bending strength, internal bond, screw holding strength and stability were as follows: 1. The bending strength and internal bonding of both the Type A panel and the Type B panel were higher than those of the Type C panel and three-layered particle board. 2. The mechanical properties of the Type C panel showed the lowest values of all composition methods. It seems that the different compression ratios of the particle and fiber interrupted the densification of the fibers when hot pressed. 3. The dimensional stability of layered-mat system panels consising of fiber-faces and particle-core was better the than control particleboard. 4. In composition methods of particle and fiber, layered-composition method was more resonable than mixed-composition. The Type B panel had the highest mechanical properties of all the composition types. 5. The Type A panel was considered the ideal composition method because of its resistance to delamination between the particle-layer and the fiber-layer and because of its lower adhesive content and more effective manufa cturing process.

• KCI Concrete Journal
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• 제14권1호
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• pp.15-22
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• 2002

Stresses that develop due to differential shrinkage between polymer modified cement mortar (PM) and Portland cement concrete (PCC) in a repaired concrete beam at early ages were investigated. Interface delamination or debonding of the newly cast repair material from the base is often observed in the field when the drying shrinkage of the repair material is relatively large. This study presents results of both experimental and analytical works. In the experimental part of the study, development of the material properties such as compressive strength, elastic modulus, interface bond strength, creep constant, and drying shrinkage was investigated by testing cylinders and beams for a three-week period in a constant-temperature chamber. Development of shrinkage-induced strains in a PM-PCC composite beam was determined. In the analytical part of the study, two analytical solutions were used to compare the experimental results with the analytically predicted values. One analysis method was of an exact type but could not consider the effect of creep. The other analysis method was rather approximate in nature but the creep effect was included. Comparison between the analytical and the experimental results showed that both analytical procedures resulted in stresses that were in fair agreement with the experimentally determined values. It may be important to consider the creep effect to estimate shrinkage-induced stresses at early ages.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 1999년도 추계학술발표대회 논문집
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• pp.160-163
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• 1999

The mechanical properties and failure behaviour of carbon/phenolic composites were inverstigated by tension and compression. Carbon/phenolic composites were fabricated by infiltration of matrix into 8 harness satin woven fabric of PAN-based carbon fibers. The tensile and compressive tests were performed at 25℃ under air atmosphere and, at 400℃ and 700℃ under N₂ atmosphere. The tensile strengths of carbon/phenolic composites in with-laminar/0° warp direction were about 10 times higher than those in with-laminar/45° warp direction, which was analyzed due to a change of fracture mode from fiber pull-out by shear to tensile fracture of fibers. The fracture of carbon/phenolic composites in with-laminar/45° direction was analyzed due to delamination by buckling. Tensile and compressive strength of carbon/phenolic composites decreased to about 50% at 400℃, and to about 10% at 700℃ compared to that at room temperature. The main reason for the decrease of tensile or compressive strength with increasing temperature was analyzed due to a reduction of bond strength between fibers and matrix resulting from thermal degradation of phenolic resin.

• 대한금속재료학회지
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• 제47권12호
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• pp.811-818
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• 2009

In order to meet increasingly complex and rigorous technical specifications, extensive effort has been devoted to fabricate clad materials with multi-layered metal plates. In this study, novel stainless steel/aluminum/copper (STS/Al/Cu) three-ply clad materials were fabricated by a hot rolling process for cookware applications. The effect of the testing temperature on the mechanical properties of the clad materials and on each component metal was investigated during the tensile tests. The interface properties of the clad materials were also examined by optical microscopy (OM) and an electron probe micro-analyzer (EPMA). The best mechanical and interfacial properties for a warm working process were found in a sample annealed at a temperature of $300^{\circ}C$. For the sample annealed at $400^{\circ}C$, the results of the tensile test indicated that interface delamination occurred only in the region of the Al/Cu interfaces. This was due to the formation of the thick and brittle intermetallic compound of $Al_2Cu$ in the Al/Cu interface. In contrast, no interface delamination was observed in the STS/Al interface, most likely due to its strong bond strength.