• Title/Summary/Keyword: bond

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The Effects of Various Metal Surface Treatments on the Shear Bond Strength between Titanium Denture Base and Relined Resins (타이타니움 의치상에 대한 다양한 금속표면처리제의 적용이 첨상레진과의 결합강도에 미치는 영향)

  • Eun, Jun-Young;Cho, In-ho;Lee, Jong-Hyuk
    • Journal of Dental Rehabilitation and Applied Science
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    • v.22 no.2
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    • pp.137-148
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    • 2006
  • The purpose of this study was to evaluate the effect of various metal surface treatments on the shear bond strength between titanium denture base and relined resins. The surfaces of commercially pure(cp) titanium were sandblasted with $50{\mu}m$ $Al_2O_3$ for 20 seconds and each group was treated with MR $Bond^{(R)}$, Alloy $Primer^{(R)}$, and Super-Bond $C&B^{(R)}$ accordingly. The specimens were completed by application of relining resins. The specimens were stored in room temperature. And the shear bond strength of the specimens were measured with the MTS universal testing $machine^{(R)}$. The results were as follows: 1. In comparison with the relining materials, $Kooliner^{(R)}$ groups showed statistically higher shear bond strength than Tokuyama Rebase $II^{(R)}$ groups(p<0.05). 2. Comparing shear bond strength, according to surface treatment, Super-bond $C&B^{(R)}$ groups showed the highest bond strength and were significantly higher than the other three groups(p<0.05). Alloy $Primer^{(R)}$ groups showed no significant difference with the MR $Bond^{(R)}$ groups, but was significantly higher than the sandblasting-only groups(p<0.05). 3. Comparing surface treatment in each groups, for two types of relining resin, the group which applies $Kooliner^{(R)}$ and Super-bond $C&B^{(R)}$ showed the highest bond strength and showed significant difference compared to the other groups(p<0.05). When using Tokuyama Rebase $II^{(R)}$, Super-bond C&B group showed the highest bond strength, but there were no significant difference compared to the Alloy $Primer^{(R)}$ group. In this limited study, applying $Kooliner^{(R)}$ and Super-Bond $C&B^{(R)}$ after sandblasting is considered to be advantageous for relining of titanium base dentures.

SHEAR BOND STRENGTH OF COMPOSITE RESIN CORE USED IN COMBINATION WITH VARIOUS RESIN CEMENTS AND DENTIN BONDING AGENTS (레진 시멘트와 상아질접착제를 사용한 콤포지트 레진 코아의 전단결합강도에 관한 연구)

  • Kim Hyun-O;Vang Mong-Sook
    • The Journal of Korean Academy of Prosthodontics
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    • v.42 no.1
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    • pp.30-40
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    • 2004
  • Purpose : The purpose of this study was aimed to compare the shear bond strength on dentin of three dentin bonding agents and two resin cements used in conjunction with self-cured composite resin core material. Material and method : Control group and six experimental groups were divided for this study. Control group was designated as specimens bonded with Tenure$ A&B^{(R)}$. Experimental groups were as follows : PB-BL group : specimens bonded with Prime&Bond $NT^{(R)}$, $BondLink^{(R)}$ SB-BL group : specimens bonded with $^{(R)}$, BondLink$SingleBond^{(R)}$ PB group : specimens bonded with Prime&Bond $NT^{(R)}$ SB group : specimens bonded with $SingleBond^{(R)}$ PF group : specimens bonded with $Panavia-F^{(R)}$ BI group specimens bonded with Bistite $II^{(R)}$ All specimens were stored in $37^{\circ}C$ distilled water for 24 hours, followed by the shear bond strength was tested by universal testing machine. The data was analysed statistically by Mann-Whitney test. Results : 1. For Prime&Bond $NT^{(R)}$ and $SingleBonde^{(R)}$, the shear bond strength was 0.24 MPa and 7.19 MPa each by each, while Tenure $A&B^{(R)}$ group control was measured at 13.93 MPa (p<0.05). Especially for Prime&Bond $NT^{(R)}$ it did not get conjunction with dentin. 2. For Prime&Bond $NT^{(R)}$ and $SingleBond^{(R)}$ using $BondLink^{(R)}$, there was no significant difference as a result of 11.73 MPa and 14.00 MPa each by each (p<0.05). 3. For $Panavia-F^{(R)}$ and Bistite $II^{(R)}$, they showed the highest shear bond strength as measured by 18.24 MPa and 16.09 MPa each (p<0.05).

Generation of Si-O-C Bond without Si-$CH_3$ Bond in Hybrid Type SiOC Film

  • Oh, Teresa
    • Journal of the Semiconductor & Display Technology
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    • v.7 no.3
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    • pp.1-4
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    • 2008
  • The chemical shift of SiOC film was observed according to the flow rate ratio. SiOC film had the broad main band of $880\sim1190cm^{-1}$ and the sharp Si-$CH_3$ bond at $1252cm^{-1}$, and the peak position of the main bond in the infrared spectra moved to high frequency according to the increasing of an BTMSM flow rate. So the increment of the alkyl group induced the C-H bond condensation in the film, and shows the blueshift in the infrared spectra. In the case of P5000 system of Applied Materials Corporation, the strong bond of Si-CH3 bond in precursor does not enough to dissociated and ionized, because low plasma energy due to the capactive coupled CVD. Therefore, there was the sharp peak of Si-$CH_3$ bond at $1252cm^{-1}$.

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A Study on the Bond Properties of Carbon Fiber Sheets used for Strengthening Structures (구조물 보강용 탄소섬유쉬트의 부착특성에 관한 연구)

  • 황진석;김지영;백명종;박형철;박칠림
    • Proceedings of the Korea Concrete Institute Conference
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    • 1997.10a
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    • pp.653-658
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    • 1997
  • Recently, carbon Fiber sheet (CFS) is frequently used for strengthening deteriorated concrete structures. To strengthening damaged structures, the property and characteristic of the bond between CFS and the concrete surface must be understood. The tensile test of single lap shear specimen was performed to study bond strength, bond stress distribution and stress transfer between CFS and concrete surface according to the bond length. Based on the test results, there were ultimate influence length (UIL) in which bond stress was distributed, and ultimate strain reduction ratio (USRR) by which strain was reduced linearly. Bond resisting force (BRF) was estimated by UIL and USRR, and which was compared with ultimate loads. According to the results of comparison, it was shown that ultimate bond strength could be estimated reasonablely by BRF.

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Evaluation of Bond Strength Properties with Changing the Aspect Ratio and Temperature of Concrete (콘크리트의 형상비 및 온도변화에 따른 부착강도 특성평가)

  • Kim, Hyun Seok;Jung, Won Kyong;Oh, Han Jin;Park, Jun Young;Kim, Hyung Bae
    • International Journal of Highway Engineering
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    • v.20 no.3
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    • pp.19-26
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    • 2018
  • PURPOSES : The main purpose of this study is suggest of field bond strength evaluation method for more objective evaluation method through Evaluation of Bond Strength Properties with changing aspect ratio and temperature. METHODS : The evaluation is laboratory bond strength test. Using the core machine, the pull-off test method ; the bond strength test of interface layer the universal testing machine. RESULTS : As a result of the laboratory bond strength evaluation, it was verified that the bond strength by aspect ratio decreases linearly with increasing aspect ratio and the bond strength properties by temperature change existed at high and low temperature condition relative to odinary temperature condition. CONCLUSIONS : According to the results of laboratory bond strength evaluation, the field bond strength evaluation results suggest applying the proposed correction factor (0.8, 1.0, 1.4, 1.9) according to aspect ratio(0.5, 0.1, 1.5, 2.0), For more objective evaluation of the bond strength, it is analyzed that the evaluation value is within $6{\sim}32^{\circ}C$ and the result can be obtained within 5% of the coefficient of variation.

IEEE 1500 Wrapper Design Technique for Pre/Post Bond Testing of TSV based 3D IC (TSV 기반 3D IC Pre/Post Bond 테스트를 위한 IEEE 1500 래퍼 설계기술)

  • Oh, Jungsub;Jung, Jihun;Park, Sungju
    • Journal of the Institute of Electronics and Information Engineers
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    • v.50 no.1
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    • pp.131-136
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    • 2013
  • TSV based 3D ICs have been widely developed with new problems at die and IC levels. It is imperative to test at post-bond as well as pre-bond to achieve high reliability and yield. This paper introduces a new testable design technique which not only test microscopic defects at TSV input/output contact at a die but also test interconnect defects at a stacked IC. IEEE 1500 wrapper cells are augmented and through at-speed tests for pre-bond die and post-bond IC, known-good-die and defect free 3D IC can be massively manufactured+.

A STUDY ON THE SHEAR BOND STRENGTH AND SCANNING ELECTRON MICROSCOPIC INVESTIGATION OF DENTIN BONDING AGENTS (상아질 접착제의 전단결합강도 및 주사전자현미경적 연구)

  • Lee, Gi-Hwan;Im, Mi-Kyung
    • Restorative Dentistry and Endodontics
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    • v.20 no.1
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    • pp.289-302
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    • 1995
  • The purpose of this study was to estimate the shear bond strength and observe the fractured and interfacial surfaces of various dentin bonding agents used conjunction with a visible light cured composite. The senentytwo human premolars and molars extracted due to periodontal or orthodontic reasons were used and randomely divided into six groups. All the prepared dentin surfaces were treated with Superbond D-liner, Scotchbond Multi-Purpose, All-Bond 2 and Prisma Universal Bond 3 accroding to the manufacturer's instructions. Six specimens were then demineralized in 10 % HCl for 24 hours and the other six specimens were not demineralized in order to observe the interfacial surfaces with Hitachi X-450 SEM at 25Kv. Also shear bond strength were obtained using an Instron Testing Machine with a crosshead speed of 1mm/min. The following results were obtained : 1. Although shear bond strength of Superbond D-Liner(17.35 MPa) and Scotch-bond Multi-Purpose group(17.29 MPa) were higher than the All-Bond 2(12.80 MPa) and Prisma Universial Bond 3 (13.43 MPa), there were no significant statistic differences in the shear bond strength between 4 groups.(P<0.05) As a result of etching to dentin in Prism a Universial BOND 3 experimentally, the resin tag was formed, but shear bond strength was decreased. 2. The resin tag into the opened dentinal tubule was formed in Superbond D-Liner, Scotchbond Multi-Purpose, All-Bond 2(etching) and Prisma Universial Bond 3(etching), but not in the All-Bone 2 and Prism a Universial Bond 3(non-etching). 3. Strong, durable bonds between dentin and dentinal bonding agents are essential, not only resin tag into the dentinal tubules, but also hybrid layer.

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Effect of additional etching and ethanol-wet bonding on the dentin bond strength of one-step self-etch adhesives

  • Ahn, Joonghee;Jung, Kyoung-Hwa;Son, Sung-Ae;Hur, Bock;Kwon, Yong-Hoon;Park, Jeong-Kil
    • Restorative Dentistry and Endodontics
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    • v.40 no.1
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    • pp.68-74
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    • 2015
  • Objectives: This study examined the effects of additional acid etching on the dentin bond strength of one-step self-etch adhesives with different compositions and pH. The effect of ethanol wetting on etched dentin bond strength of self-etch adhesives was also evaluated. Materials and Methods: Forty-two human permanent molars were classified into 21 groups according to the adhesive types (Clearfil SE Bond [SE, control]; G-aenial Bond [GB]; Xeno V [XV]; Beauti Bond [BB]; Adper Easy Bond [AE]; Single Bond Universal [SU]; All Bond Universal [AU]), and the dentin conditioning methods. Composite resins were placed on the dentin surfaces, and the teeth were sectioned. The microtensile bond strength was measured, and the failure mode of the fractured specimens was examined. The data were analyzed statistically using two-way ANOVA and Duncan's post hoc test. Results: In GB, XV and SE ($pH{\leq}2$), the bond strength was decreased significantly when the dentin was etched (p < 0.05). In BB, AE and SU (pH 2.4 - 2.7), additional etching did not affect the bond strength (p > 0.05). In AU (pH = 3.2), additional etching increased the bond strength significantly (p < 0.05). When adhesives were applied to the acid etched dentin with ethanol-wet bonding, the bond strength was significantly higher than that of the no ethanol-wet bonding groups, and the incidence of cohesive failure was increased. Conclusions: The effect of additional acid etching on the dentin bond strength was influenced by the pH of one-step self-etch adhesives. Ethanol wetting on etched dentin could create a stronger bonding performance of one-step self-etch adhesives for acid etched dentin.

Bond Strength of Reinforcing Steel to High Strength, High Flow Belite Concrete (고강도, 고유동 Belite 콘크리트의 부착성능)

  • 김상준;조필규;이세웅;최완철
    • Proceedings of the Korea Concrete Institute Conference
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    • 1998.04b
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    • pp.653-660
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    • 1998
  • Bond strength of reinforcing bar to high-performance concrete using belite cement is explored using beam end test specimen. The key parameters for the bond test are slump of concrete, top bar effect, and strength of concrete in addition to concrete covers. Specimen failed in the typical brittle bond failure splitting the concrete cover as the wedging action. The test results show that the specimens with belire cement concrete show higher bond strength than those with portland cement concrete. Bond strength of the top bar is less than bond strength of bottom bar, but the top bar factor satisfies the modification factor for top reinforcement. The results also show that the bond strength is function of the square root of concrete compressive strength and cover thickness. The recently developed high-strength and high-slump concrete with belite cement performs well in terms of bond strength to reinforcing steel.

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BONDING STRENGTH OF GLASS-IOMOMER CEMENT AND COMPOSITE RESIN COMBINATION (Glass ionomer cement의 상아질 결합력에 관한 연구)

  • Um, Chung-Moon;Oilo, Gudbrand
    • Restorative Dentistry and Endodontics
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    • v.19 no.2
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    • pp.633-640
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    • 1994
  • The tensile bond strength to dentin was measured for three glass-ionomer cement and composite resin combinations: two light-curing glass-ionomer cements(Vitrebond and XR - Ionomer) and one traditional glass - ionomer cement(Ketac - Bond), two adhesive systems(Scotchbond, and XR - Bonding System), and a corresponding composite resin. The bond strength of this "sandwich" was also compared with that of the same cements used in bulk. Vitredbond showed a significantly higher bond strength in bulk than did the other two cements. Of the sandwiches, the XR - Iomomer and XR - Bond combination showed a bond strength significantly higher than that of the Vitrebond and Scotchbond or Ketac- bond and Scotchbond combination. The fracture of the bond was mainly adhesive for Vitrebond, cohesive for XR - Ionomer when used in bulk and adhesive - cohesive when used in a sandwich, and cohesive for Ketac-Bond.

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