• Corrosion Science and Technology
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• v.18 no.1
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• pp.33-38
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• 2019

Alloy 600/182 with excellent mechanical/chemical properties have been utilized for nuclear power plants. Although both alloys are known to have superior corrosion resistance, stress corrosion cracking failure has been an issue in primary water environment of nuclear power plants. Therefore, primary water stress corrosion crack (PWSCC) growth rate tests were conducted to investigate crack growth properties of Alloy 600/182. To investigate PWSCC growth rate, test facilities including water chemistry loop, autoclave, and loading system were constructed. In PWSCC crack growth rate tests, half compact-tension specimens were manufactured. These specimens were then placed inside of the autoclave connected to the loop to provide primary water environment. Tested conditions were set at temperature of $360^{\circ}C$ and pressure of 20MPa. Real time crack growth rates of specimens inside the autoclave were measured by Direct Current potential drop (DCPD) method. To confirm inter-granular (IG) crack as a characteristic of PWSCC, fracture surfaces of tested specimens were observed by SEM. Finally, crack growth rate was derived in a specific stress intensity factor (K) range and similarity with overseas database was identified.

• Corrosion Science and Technology
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• v.5 no.3
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• pp.85-89
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• 2006

KAERI(Korea Atomic Energy Research Institute) has developed a repassivation rate test system which can be operated at $300^{\circ}C$. It consists of an autoclave, three electrodes for an electrochemical test and a diamond scratch tip. All the electrodes are electrically insulated from the autoclave by using high temperature fittings. Reproducible repassivation curves of alloy 600 at 300 C were obtained. Repassivation rate of alloy 600 at pH 13 was slower than that of pH 10. Stress corrosion cracking test was carried as a function of the pH at a high temperature. At pH 10, alloy 600 showed a severe stress corrosion cracking(SCC), whereas it did not show a SCC at pH 7. From the viewpoint of a relationship between the current density and the charge density, a big difference was observed in the two solutions; the slope of pH 13 was steeper than that of pH 10. So the stress corrosion susceptibility at pH 13 seems to be higher than that of pH 10. The system would be a good tool to evaluate the SCC susceptibility of alloy 600 at a high temperature.

• KIEAE Journal
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• v.7 no.4
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• pp.127-133
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• 2007

As a fundamental study on the corrosion resistance of reinforced concrete structures using Natural Inorganic Minerals exposed to carbonation environment, The test specimens were concrete(W/C=60%) with Natural Inorganic Minerals content of 0%, 10%. Accelerated carbonation and autoclave corrosion accelerated curing were then conducted with them. The corrosion resistance of steel in concrete with Natural Inorganic Minerals content of 0%, 10% was examined by corrosion form, half-cell potential, polarization resistance, corrosion area and weight loss after 24 hours of autoclave corrosion accelerated curing.The results of the study showed that as for steel in concrete with Natural Inorganic Minerals content of 10%, the corrosion resistance was more excellent than steel in concrete with Natural Inorganic Minerals content of 0%.

• Journal of the Korean Chemical Society
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• v.11 no.1
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• pp.33-37
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• 1967

The influence of impurities contained in Marmatite ores on leaching of zinc was investigated. The zinc sulfide having the same crystal structure of natural Sphalerite was prepared by heating the zinc sulfide chemically precipitated, at $650^{\circ}C$ in nitrogen atmosphere. The activation energy of the sample was 25.8 kcal per mole in the leach test when oxygen partial pressure was 5 atm. and the value was exceedingly high compared to that obtained in Marmatite ores. Synthetic zinc sulfides added with small amount of each impurities were treated in same procedure. As a result, it was found that the leaching velocity was accelerated sharply when about 1 percent of $Cu^{++}$ was blended to the sample. Larger amount of iron has also same effect but the effect was minor compared to the copper. The other impurities indicated no appreciable catalytic action.

• Proceedings of the Korea Concrete Institute Conference
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• 2006.11a
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• pp.465-468
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• 2006

This paper investigates the effect of curing conditions on the strength improvement of polymer-modified mortars using epoxy resin with various curing methods. The polymer-modified mortars using epoxy resin are prepared with various polymer-cement ratios, and subjected to standard, hot water, heat cure and autoclave cures. The epoxy-modified mortars are tested for flexural and compressive strengths at desired curing methods. From the test results, the flexural and compressive strengths of the epoxy-modified mortars are hardly improved by the autoclave and hot water cures compared to the ideal cure of $20^{\circ}C$. Among the four types of curing methods, the strengths of the heat cured epoxy-modified mortars is largely improved. Especially, it is obtained in the mortars sealed with PVDC film.

• Journal of the Korean Wood Science and Technology
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• v.32 no.2
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• pp.9-18
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• 2004

This study was carried out to find the efficient methods for preventing resin exudation from spruce board during high temperature environment service.In the dry-air oven test, in-use temperature related to resin exudation of 110℃ could be obtained by the appropriate kiln drying without any special treatment, and the in-use temperature of the radio-frequency/vacuum (RF/V)-dried boards was about 20℃ higher than that of the conventional kiln-dried boards.In the autoclave test, resin exudation was not found from any board dried in the conventional kiln and in the RF/V kiln after the low pressure steam explosion (SE) treating, while for the control resin exudations were more severe in the autoclave test above 130℃ than in the dry-air oven test. It, therefore, would be suggested that resin exudation during high temperature service condition can be prevented more effectively by super-heated steaming green boards than by high-temperature drying boards with low moisture.

• Nuclear Engineering and Technology
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• v.35 no.3
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• pp.206-213
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• 2003

This study focuses on an understanding of the environmental effect on delayed hydride cracking velocity (DHCV) of CANDU Zr-2.5Nb tubes. To simulate DHC susceptibility of the Zr-2.5Nb tubes in reactor operating conditions, DHC tests were successfully carried out in pressurized water at 180 and $250^{\circ}C$ using a self-designed autoclave for the first time. Using 17 mm compact tension specimens electorlytically charged to 34 and 60 ppm H, 3 to 7 DHCV data were determined in water at both temperatures and compared to those determined in air that were already confirmed to be valid through a round robin test on DHCV of Zr-2.5Nb tubes sponsored by a IAEA coordinated research program. The pressurized water environment has little effect on DHCV of Zr-2.5Nb tube in water at both temperatures even though DHCV is slightly lower in water than that in air. The lower DHCV of the Zr-2.5Nb tube during short-term tests is discussed in viewpoint of the cooling rate from the peak temperature to the test temperature.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.7 no.2
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• pp.23-28
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• 1998

In this paper, the experimental and numerical results of buckling loads for laminated composite plates are compared. Using boundary conditions of buckling test are all fixed supports. Experiments were conducted for plates with fiber angles $ heta$=30$^{\circ}$, 45$^{\circ}$,60$^{\circ}$ and aspect ratio a/b=0.8. Experimental results were obtained from load-deflection curves of buckling test. Numerical methods were presented to evaluate buckling loads, using structural analysis results from ANSYS.

• Journal of the korean Society of Automotive Engineers
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• v.13 no.5
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• pp.65-72
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• 1991

This paper presents the results of static crushing test that was conducted to characterize the energy absorption and collapse characteristics of composite box tubes. Fifteen specimens were fabricated with woven fabric prepreg using [0/90] glass/epoxy and were autoclave cured. Quasistatic compression test was performed on them. Collapse mode and energy absorption capacity vary significantly as a function of the thickness and length of a square side of composite box tube.

• Composites Research
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• v.34 no.2
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• pp.88-95
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• 2021

VARTM (Vacuum-assisted resin transfer molding) process is a low-cost process technology and affiliated with OoA (Out of Autoclave). Besides, it has been widely used in various fields. However, because of its lower quality than the autoclave process, it isn't easy to apply the VARTM process to the aerospace industry, which requires high reliability. The main problem of the VARTM process is the loss of mechanical properties due to the low fiber volume fraction and high void content in comparison to the autoclave. Therefore, many researchers have studied to reduce void and increase fiber volume fraction. This study examines whether the method of controlling atmospheric pressure could increase the fiber volume fraction and reduce void during the resin impregnation process. Reliability evaluation was confirmed by compressive strength test, fiber volume fraction analysis, and optical microscopy. As a result, it was confirmed that increasing the atmospheric pressure step by step in the VARTM process of impregnating the preform with resin effectively increases the fiber volume fraction and reduces void.