• Title/Summary/Keyword: annealing conditions

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A Study on Non-propagating Crack in Fatigue Behavior of Pure Titanium (공업용 순 티타늄의 피로거동에서 정류균열에 관한 연구)

  • Kim, Dong-Yeol;Kim, Jin-Hak;Kim, Min-Geon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.4 s.175
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    • pp.1001-1006
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    • 2000
  • To verify the existing theory, non-propagating crack(NPC) does not exist in Ti which fulfills the good conditions for being of NPC, NPC detection in Ti was tried out. Also, the conception of fatigue limit in Ti and a main cause for NPC being were inquired. NPC was detected in both sharp notch root ( $\rho$=0.02mm) and micro pit (diameter = 0.25mm) which held fast to the end under stressing of fatigue limit. Therefore, the existing theory was identified as mistake. But, NPC can not be detected in smooth specimen. This fact would be due to the presumption that NPC is very small or crack does not initiate in smooth specimen. Anyway, the fatigue limit of Ti does not correspond to critical stress of crack initiation but correspond to critical stress of NPC growth. Measurement on the COD of NPC in Ti showed that the crack tip was closed even under the peak stress level at fatigue limit. But, after stress relieving annealing crack tip was opened. Consequently, compressive residual stress which is induced around the crack tip is considered to be the factor causing the NPC being.

Change of Mechanical Properties of Clad Steel According to the Welding Process Design (용접 공정 디자인에 따른 클래드강의 기계적 성질 변화)

  • Lee, Jung-Hyun;Park, Jaw-Won
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.3
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    • pp.372-379
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    • 2013
  • In this study, we investigated the traits of the clad metals used in hot-rolled clad steel plates. We examined the sensitization and mechanical properties of STS 316 steel plate and carbon steel (A516) under the specific circumstances of post heat treatment and whether a weld was multilayered and thick or repeated because of repairs. The test conditions were as follows. The clad steel plates were butt-welded using FCAW/SAW, and the heat treatment was conducted at $625^{\circ}C$, for 80, 160, 320, 640, or 1280 min. The change in the corrosion resistance was evaluated in these specimens. In the case of the carbon steel (A516), as the heat treatment time increased, the annealing effect caused the tensile strength to decrease. The micro- hardness gradually increased and then decreased after 640 min. The elongation and contraction of the area increased gradually. An oxalic acid etch test and EPR test on STS316, a clad metal, showed a STEP structure and no sensitization. From the test results for the multi-layered and repair welds, it could be concluded that there is no effect on the corrosion resistance of clad metals. In summary, the purpose of this study was to suggest some considerations when developing on-site techniques and evaluate the sensitization of stainless steels.

Fabrication and Characteristics of Tantalum Nitride Thin-Film Strain Gauges (질화탄탈 박막형 스트레인 게이지의 제작과 특성)

  • Chung, Gwiy-Sang;Woo, Hyung-Soon;Kim, Sun-Chul;Hong, Dae-Sun
    • Journal of Sensor Science and Technology
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    • v.13 no.4
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    • pp.303-308
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    • 2004
  • This paper descibes on the characteristics of Ta-N(tantalum nitride) ceramic thin-film strain gauges which were deposited on Si substrates by DC reactive magnetron sputtering in an argon-nitrogen atmosphere (Ar-$(4{\sim}16%)N_{2}$) for high-temperature applications. These films were annealed in $2{\times}10^{-6}$ Torr vacuum furnace at the range of $500{\sim}1000^{\circ}C$. Optimum deposition atmosphere and annealing temperature were determined at $900^{\circ}C$ for 1 hr. in 8% $N_{2}$ gas flow ratio. Under optimum formation conditions, the Ta-N thin-film for strain gauges was obtained a high-resistivity of $768.93{\mu}{\Omega}{\cdot}cm$, a low temperature coefficient of resistance (TCR) of -84 ppm/$^{\circ}C$ and a good longitudinal gauge factor (GF) of 4.12.

A Study on the Crystallization Behavior of Al85Ce5Ni10 Amorphous Ribbon (Al85Ce5Ni10 비정질 리본의 결정화 거동에 관한 연구)

  • Moon, J.T.;Jo, W.M.;Shin, B.M.;Lee, Y.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.3
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    • pp.236-243
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    • 1995
  • Since amorphous alloys have been known to have better mechanical and chemical properties than crystalline alloys of the same composition, a great number of studies on the formation of Al-based amorphous alloys have been carried out actively. However, little has been obtained about the effect of Rare-Earth metal and Transition metal addition on amorphous phase formed by melt spinning method. This study included fabrication of amorphous alloy $Al_{85}Ce_5Ni_{10}$ by melt spinning methods and DTA, XRD, TEM analysis to determine crystalization behavoir. Annealing treatments were carried out in Ar atmosphere under isothermal and nonisothermal conditions. The diffraction pattern of non-heated ribbons showed broad form characteristic of glass metallic alloy. The crystallization of amorphous $Al_{85}Ce_5Ni_{10}$ takes place eutedtoidly by homogeneous formation of Al and MS-1, followed by precipitation of the $Al_{11}Ce_3$ and later $MS-1{\rightarrow}Al_3Ni$ transformation.

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The Changes of the Microstructure and the Physical Properties of Heat Set PET Partially Oriented Yarns (PET부분배향사(POY)의 열처리에 따른 내부구조 및 물성변화)

  • Choi Jong Myoung;Cho Gil Soo
    • Journal of the Korean Society of Clothing and Textiles
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    • v.12 no.3 s.28
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    • pp.343-350
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    • 1988
  • This study was carried out to investigate the microstructure and physical property of PET POY which was taut-annealed under various conditions. The DSC melting curves of annealed PET POY showed double melting peaks in most cases. As temperature and time increased, form II crystal became sharp and increased in size, and form I crystal decreased in size. The slower the heating rate, the higher the programmed heating effect during DSC analysis. Crystallinity and briefringence of annealed specimens increased as the treatment temperature and time increased. Breaking tenacity of specimens treated for 3 minutes increased as the treatment temperature increased, but others decreased. Elongation at break decreased as the annealing temperature and time increased. Dye uptake of annealed specimens decreased as the temperature increased up to $190^{\circ}C\~210^{\circ}C$. then the uptakes increased at higher temperatures. At the same temperature, dye uptake of the specimen decreased as time increased.

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The Electrical Resistivity of a SiCw/Al Alloy Composite with Temperature

  • Kim Byung-Geol;Dong Shang-Li;Park Su-Dong;Lee Hee-Woong
    • Korean Journal of Materials Research
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    • v.14 no.7
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    • pp.489-493
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    • 2004
  • The electrical property of MMC is essentially important to some applications such as power transmission lines and cables, electronic and electrical components as well as electromagnetic shielding equipments. The behavior of electrical resistivity of $SiC_{w}/Al$ alloy composites under as-extruded and annealed conditions has been investigated within the temperature range from room temperature to $450^{\circ}C$. It can be seen that within entire temperature range, the electrical resistivity of composites was higher than that of an unreinforced matrix alloy under the same condition of either as-extrusion or annealing. The temperature dependence of both exhibited positive incline like a typical metal. The variation of electrical resistivity of an unreinforced matrix alloy with temperature from ambient temperature to $450^{\circ}C$ was nearly monotonous, while those of composites increased monotonously at low temperature and rose to a high level after about $250^{\circ}C or 275^{\circ}C$. The difference of these temperature dependences on electrical resistivity can be interpreted as qualitatively the interfaces of $SiC_{w}$ fibers and matrix, where act as nucleation sites.

Optimization of Ohmic Contact Metallization Process for AlGaN/GaN High Electron Mobility Transistor

  • Wang, Cong;Cho, Sung-Jin;Kim, Nam-Young
    • Transactions on Electrical and Electronic Materials
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    • v.14 no.1
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    • pp.32-35
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    • 2013
  • In this paper, a manufacturing process was developed for fabricating high-quality AlGaN/GaN high electron mobility transistors (HEMTs) on silicon carbide (SiC) substrates. Various conditions and processing methods regarding the ohmic contact and pre-metal-deposition $BCl_3$ etching processes were evaluated in terms of the device performance. In order to obtain a good ohmic contact performance, we tested a Ti/Al/Ta/Au ohmic contact metallization scheme under different rapid thermal annealing (RTA) temperature and time. A $BCl_3$-based reactive-ion etching (RIE) method was performed before the ohmic metallization, since this approach was shown to produce a better ohmic contact compared to the as-fabricated HEMTs. A HEMT with a 0.5 ${\mu}m$ gate length was fabricated using this novel manufacturing process, which exhibits a maximum drain current density of 720 mA/mm and a peak transconductance of 235 mS/mm. The X-band output power density was 6.4 W/mm with a 53% power added efficiency (PAE).

Evaluation of Acceptor Binding Energy of Nitrogen-Doped Zinc Oxide Thin Films Grown by Dielectric Barrier Discharge in Pulsed Laser Deposition

  • Lee, Deuk-Hee;Chun, Yoon-Soo;Lee, Sang-Yeol;Kim, Sang-Sig
    • Transactions on Electrical and Electronic Materials
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    • v.12 no.5
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    • pp.200-203
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    • 2011
  • In this research, nitrogen (N)-doped zinc oxide (ZnO) thin films have been grown on a sapphire substrate by dielectric barrier discharge (DBD) in pulsed laser deposition (PLD). DBD has been used as an effective way for massive in-situ generation of N-plasma under conventional PLD process conditions. Low-temperature photoluminescence spectra of N-doped ZnO thin films provided near-band-edge emission after a thermal annealing process. The emission peak was resolved by Gaussian fitting and showed a dominant acceptor-bound excitation peak ($A^{\circ}X$) that indicated acceptor doping of ZnO with N. The acceptor binding energy of the N acceptor was estimated to be approximately 145 MeV based on the results of temperature-dependent photoluminescence (PL) measurements.

A Study on the Fatigue Crack Growth Behavior and Fracture Toughness of Martensitic Stainless Steel(12%Cr) (마르텐사이트계 스테인리스강 (12%Cr) 의 피로균열 진전거동 및 파괴인성연구)

  • 윤병주
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.9 no.4
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    • pp.154-160
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    • 2000
  • Martensitic stainless steels containing 12%Cr are commonly used in quenched and tempered conditions. The quenching heat treatment involves annealing to obtain austenite and to dissolve the carbides , followed by cooling to transform the austenite into martensite and often to cause carbide predipitation. In this study, we used three different tempered specimens which were temperated at 30$0^{\circ}C$, 67$0^{\circ}C$ and 75$0^{\circ}C$ . The crack propagation and fracture toughness tests were performed on this three different specimens. The experimental results showed that the highest value of crack growth rate and the lowest value of fracture toughness were observed in the specimen which were temperated at $600^{\circ}C$, however, when the specimen were temperated at 75$0^{\circ}C$, the vale of crack growth rate was significantly decreased and the value of fracture toughness was significantly increased as compared to which were temperated at $600^{\circ}C$.

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Structural health monitoring through meta-heuristics - comparative performance study

  • Pholdee, Nantiwat;Bureerat, Sujin
    • Advances in Computational Design
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    • v.1 no.4
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    • pp.315-327
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    • 2016
  • Damage detection and localisation in structures is essential since it can be a means for preventive maintenance of those structures under service conditions. The use of structural modal data for detecting the damage is one of the most efficient methods. This paper presents comparative performance of various state-of-the-art meta-heuristics for use in structural damage detection based on changes in modal data. The metaheuristics include differential evolution (DE), artificial bee colony algorithm (ABC), real-code ant colony optimisation (ACOR), charged system search (ChSS), league championship algorithm (LCA), simulated annealing (SA), particle swarm optimisation (PSO), evolution strategies (ES), teaching-learning-based optimisation (TLBO), adaptive differential evolution (JADE), evolution strategy with covariance matrix adaptation (CMAES), success-history based adaptive differential evolution (SHADE) and SHADE with linear population size reduction (L-SHADE). Three truss structures are used to pose several test problems for structural damage detection. The meta-heuristics are then used to solve the test problems treated as optimisation problems. Comparative performance is carried out where the statistically best algorithms are identified.