• Title/Summary/Keyword: and characterization

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Hot stage microscopy and its applications in pharmaceutical characterization

  • Arun Kumar;Pritam Singh;Arun Nanda
    • Applied Microscopy
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    • v.50
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    • pp.12.1-12.11
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    • 2020
  • Hot stage microscopy (HSM) is a thermal analysis technique that combines the best properties of thermal analysis and microscopy. HSM is rapidly gaining interest in pharmaceuticals as well as in other fields as a regular characterization technique. In pharmaceuticals HSM is used to support differential scanning calorimetry (DSC) and thermo-gravimetric analysis (TGA) observations and to detect small changes in the sample that may be missed by DSC and TGA during a thermal experiment. Study of various physical and chemical properties such sample morphology, crystalline nature, polymorphism, desolvation, miscibility, melting, solid state transitions and incompatibility between various pharmaceutical compounds can be carried out using HSM. HSM is also widely used to screen cocrystals, excipients and polymers for solid dispersions. With the advancements in research methodologies, it is now possible to use HSM in conjunction with other characterization techniques such as Fourier transform infrared spectroscopy (FTIR), DSC, Raman spectroscopy, scanning electron microscopy (SEM) which may have additional benefits over traditional characterization techniques for rapid and comprehensive solid state characterization.

Extraction of Electrical Parameters for Single and Differential Vias on PCB (PCB상 Single 및 Differential Via의 전기적 파라미터 추출)

  • Chae Ji Eun;Lee Hyun Bae;Park Hon June
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.42 no.4 s.334
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    • pp.45-52
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    • 2005
  • This paper presents the characterization of through hole vias on printed circuit board (PCB) through the time domain and frequency domain measurements. The time domain measurement was performed on a single via using the TDR, and the model parameters were extracted by the fitting simulation using HSPICE. The frequency domain measurement was also performed by using 2 port VNA, and the model parameters were extracted by fitting simulation with ADS. Using the ABCD matrices, the do-embedding equations were derived probing in the same plane in the VNA measurement. Based on the single via characterization, the differential via characterization was also performed by using TDR measurements. The time domain measurements were performed by using the odd mode and even mode sources in TDR module, and the Parameter values were extracted by fitting with HSPICE. Comparing measurements with simulations, the maximum calculated differences were $14\%$ for single vias and $17\%$ for differential vias.

Recurrence Relation and Characterization of The Rayleigh Distribution Using Order Statistics

  • Lee, In-Suk;Kim, Sang-Moon
    • Journal of the Korean Data and Information Science Society
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    • v.10 no.2
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    • pp.299-311
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    • 1999
  • In this paper the single and product moments of order statistics of the doubly truncated Rayleigh distribution are studied. Some recurrence relations of order statistics are derived. Using order statistics, also characterization of the Rayleigh distribution are derived.

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Nondestructive Characterization and In-situ Monitoring of Corrosion Degradation by Backward Radiated Ultrasound

  • Song, Sung-Jin;Kim, Young H.;Bae, Dong-Ho;Kwon, Sung D.
    • Corrosion Science and Technology
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    • v.4 no.3
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    • pp.114-119
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    • 2005
  • Since the degradation caused by corrosion is restricted to the surface of materials, conventional ultrasonic nondestructive evaluation methods based on ultrasonic bulk waves are not applicable to characterization of the corrosion degradation. To take care of this difficulty, a new nondestructive evaluation method that uses ultrasonic backward radiation has been proposed recently. This paper explores the potential of this newly developed method for nondestructive characterization and in-situ monitoring of corrosion degradation. Specifically, backward radiated ultrasounds from aged thermo-mechanically controlled process (TMCP) steel specimens by corrosion fatigue were measured and their characteristics were correlated to those of the aged specimens. The excellent correlation observed in the present study demonstrates the high potential of the backward radiated ultrasound as an effective tool for nondestructive characterization of corrosion degradation. In addition, the potential of the backward radiated ultrasound to in-situ monitoring of corrosion degradation is under current investigation.

Indoor RSSI Characterization using Statistical Methods in Wireless Sensor Network (무선 센서네트워크에서의 통계적 방법에 의한 실내 RSSI 측정)

  • Pu, Chuan-Chin;Chung, Wan-Young
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2007.10a
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    • pp.457-461
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    • 2007
  • In many applications, received signal strength indicator is used for location tracking and sensor nodes localization. For location finding, the distances between sensor nodes can be estimated by converting received signal's power into distance using path loss prediction model. Many researches have done the analysis of power-distance relationship for radio channel characterization. In indoor environment, the general conclusion is the non-linear variation of RSSI values as distance varied linearly. This has been one of the difficulties for indoor localization. This paper presents works on indoor RSSI characterization based on statistical methods to find the overall trend of RSSI variation at different places and times within the same room From experiments, it has been shown that the variation of RSSI values can be determined by both spatial and temporal factors. This two factors are directly indicated by the two main parameters of path loss prediction model. The results show that all sensor nodes which are located at different places share the same characterization value for the temporal parameter whereas different values for the spatial parameters. Using this relationship, the characterization for location estimation can be more efficient and accurate.

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Characterization of Associating Polymers in Solution

  • Sato, Takahiro
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.118-119
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    • 2006
  • The characterization method for associating polymer solutions was briefly reviewed. The method has not yet established in comparison with the characterization method for molecularly dispersed polymers in solution. However, two examples of associating polymer systems, living polybutadiene anions and amphiphilic statistical copolymers, were successfully characterized on the basis of suitable model and theory.

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AREA PROPERTIES ASSOCIATED WITH STRICTLY CONVEX CURVES

  • Bang, Shin-Ok;Kim, Dong-Soo;Kim, Incheon
    • Bulletin of the Korean Mathematical Society
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    • v.59 no.2
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    • pp.407-417
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    • 2022
  • Archimedes proved that for a point P on a parabola X and a chord AB of X parallel to the tangent of X at P, the area of the region bounded by the parabola X and the chord AB is four thirds of the area of the triangle ∆ABP. This property was proved to be a characteristic of parabolas, so called the Archimedean characterization of parabolas. In this article, we study strictly convex curves in the plane ℝ2. As a result, first using a functional equation we establish a characterization theorem for quadrics. With the help of this characterization we give another proof of the Archimedean characterization of parabolas. Finally, we present two related conditions which are necessary and sufficient for a strictly convex curve in the plane to be an open arc of a parabola.

Characterization of Coagulation on Synthetic Polymerization Al(III) Inorganic Coagulants for Water Treatment (상수처리용 합성 무기고분자 Al(III)계 응집제의 응집특성)

  • Han Seung-Woo;Jung Chul-Woo;Kang Lim-Seok
    • Journal of Environmental Science International
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    • v.8 no.6
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    • pp.717-724
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    • 1999
  • This experiment was performed on three parts with prepared coagulants. (1) The characterization of coagulation for PACI coagulants. (2) Comparison of the characterization of coagulation with PAS and PACI coagulants. And (3) Comparison of the characterization of coagulation for the addition of calcium with PACI. Coagulation experiments were conducted with several dosages and pH for each coagulants. For the characterization of coagulation with PACI coagulants, coagulation of Nakdong river waters with three PACls (r=2.0, 2.2, 2.35) showed that the effectiveness of the three coagulants can be considered as r=2.2 > 2.0 > 2.35 which are also the order of higher polymeric aluminum contents. For the comparison of the characterization of coagulation for PAS and PACI coagulants, PAS (r=0.75) coagulants was more effective than other coagulant for the removal of organic matters by sweep floc mechanism with $A;(OH)_{3(S)}$. For comparison of the characterization of coagulation for the addition of calcium with PACI, the presence of divalent cation like $Ca^{2+}$ was supposed to influence the complex formation of organic anions. From the result of test on coagulation at various pH ranges, the PACI was least affected by the coagulation pH, and the addition of calcium to PACI was very effective for the removal of turbidity and organic materials over broader pH range (pH 4-9).

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Issues with the electrical characterization of graphene devices

  • Lee, Byoung-Hun;Lee, Young-Gon;Jung, Uk-Jin;Kim, Yong-Hun;Hwang, Hyeon-Jun;Kim, Jin-Ju;Kang, Chang-Goo
    • Carbon letters
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    • v.13 no.1
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    • pp.23-28
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    • 2012
  • Graphene is an attractive material for device applications, but device characteristics are very unstable because the graphene is very sensitive to environmental factors such as charges nearby the graphene, metal contacts, defects, contaminants and other adsorbates. Since the interactions between graphene and environmental factors affect the electrical characteristics of graphene devices, the interpretation of electrical characteristics as simple as current-voltage curves is non-trivial, despite the common practice of using well known electrical characterization methods that have been used in silicon MOSFET. This paper addresses major obstacles in the electrical characterization of graphene devices and offers countermeasures to improve the accuracy of electrical characterization methods.