• Title/Summary/Keyword: analytical testing

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Sample Development for Quality Control of Formaldehyde and Proficiency Analytical Testing (정도관리용 포름알데히드 시료개발 및 분석능력평가)

  • Park, Hae Dong;Jang, Miyeon;Park, Seunghyun
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.30 no.1
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    • pp.58-66
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    • 2020
  • Objectives: The objective of this study was to develop formaldehyde samples for quality control (QC) and to test the applicability of proficiency analytical testing in Korea. Methods: We made formaldehyde samples with certified standard solutions (formaldehyde in water or acetonitrile) and 2,4-dinitrophenylhydrazine (2,4-DNPH)-coated silicagel tubes. Four levels of formaldehyde concentration were tested for storage stability at room temperature and at 4℃ over three months. Analytical proficiency testing was performed with four or 36 institutes. Results: Formaldehyde sample tubes were easily made through the injection of standard solutions and the average efficiencies of recovery were 95-101%. The coefficients of variation (CV) of the formaldehyde samples were 1.39-2.55%. The recovery efficiencies fell between 90% and 110% at the concentration range of 1-10 ㎍/sample over three months storage at refrigerated and room temperature. The CVs were less than 5% in the proficiency analytical testing. By adjusted proficient ranges, 64% of the results of the second proficiency analytical testing were acceptable. Conclusions: The formaldehyde samples made by injection on 2,4-DNPH-coated silicagel tubes were stable and applicable for quality control.

Analytical testing and evaluation of truss typed structures for tunnel maintenance

  • Lee, Dongkyu;Kim, Dohwan;Lee, Jaehong;Noh, Pilsung;Park, Sungsoo
    • Smart Structures and Systems
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    • v.15 no.4
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    • pp.949-961
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    • 2015
  • The goal of this study is to present numerical modeling and analytical testing in order to evaluate an innovative space truss typed temporary structure, which is used to maintenance and repair of road tunnels. The present space truss structure has merits to use UL-700 high strength steel tube as members and to carry out maintenance and repair works of road tunnels without blocking cars and transportations. Numerical modeling and analytical testing of the space truss are investigated by using commercial engineering software, i.e., ABAQUS 6.5-1, and then it is verified that the truss structure has both structural safety and effective function for maintenances and repairs of road tunnels.

A study on the development of analytical method for zinc pyrithione in cosmetics (화장품 중 zinc pyrithione 분석방법 개발에 대한 연구)

  • Jung, Jung-sul;Bae, Kyeong-mi;Son, Seung-hwan;Park, Jung-woo;Kim, Ji-hyun;Hong, Sung-taeg;Sun, Yle-shik
    • Analytical Science and Technology
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    • v.28 no.3
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    • pp.160-167
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    • 2015
  • This study aims to develop a new analytical method to detect zinc pyrithione, the ingredient of cosmetics appointed as restricted ingredients and used as preservatives.. The analytical method was based on data gathered from the relevant literature. Information about the amounts of these ingredients was researched in order to select the base-matrix materials used to validate the analytical method. After selecting and preparing the base-matrix materials, the analytical method was validated by method validation procedures. The analytical method was verified first by inter-laboratory validation and then through analyzing the cosmetics sold in the market. Based on the results of this study, guidelines are proposed for the analysis of restricted ingredients in cosmetics, which will provide a method to test the cosmetics circulating in the Korean market. The use of the proposed guidelines will increase the quality of the cosmetics as well as the safety of human health, which will enhance the competitiveness of the Korean cosmetics industry and lead to an increase in the exportation of cosmetics.

Analytical Beam Field Modeling Applied to Transducer Optimization and Inspection Simulation in Ultrasonic Nondestructive Testing

  • Spies, Martin
    • Journal of the Korean Society for Nondestructive Testing
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    • v.23 no.6
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    • pp.635-644
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    • 2003
  • To ensure the reliability of ultrasonic nondestructive testing techniques for modern structural materials, the effects of anisotropy and inhomogeneity and the influence of non-planar component geometries on ultrasonic wave propagation have to be taken into account. In this article, fundamentals and applications of two analytical approaches to three-dimensional elastic beam field calculation are presented. Results for both isotropic materials including curved interfaces and for anisotropic media like composites are presented, covering field profiles for various types of transducers and the modeling of time-dependent rf-signals.

Model-Based Prediction of Pulsed Eddy Current Testing Signals from Stratified Conductive Structures

  • Zhang, Jian-Hai;Song, Sung-Jin;Kim, Woong-Ji;Kim, Hak-Joon;Chung, Jong-Duk
    • Journal of the Korean Society for Nondestructive Testing
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    • v.31 no.6
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    • pp.609-615
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    • 2011
  • Excitation and propagation of electromagnetic field of a cylindrical coil above an arbitrary number of conductive plates for pulsed eddy current testing(PECT) are very complex problems due to their complicated physical properties. In this paper, analytical modeling of PECT is established by Fourier series based on truncated region eigenfunction expansion(TREE) method for a single air-cored coil above stratified conductive structures(SCS) to investigate their integrity. From the presented expression of PECT, the coil impedance due to SCS is calculated based on analytical approach using the generalized reflection coefficient in series form. Then the multilayered structures manufactured by non-ferromagnetic (STS301L) and ferromagnetic materials (SS400) are investigated by the developed PECT model. Good prediction of analytical model of PECT not only contributes to the development of an efficient solver but also can be applied to optimize the conditions of experimental setup in PECT.

Ambient vibration testing and seismic performance of precast I beam bridges on a high-speed railway line

  • Toydemir, Burak;Kocak, Ali;Sevim, Baris;Zengin, Basak
    • Steel and Composite Structures
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    • v.23 no.5
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    • pp.557-570
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    • 2017
  • In this study, the seismic performance levels of four bridges are determined using finite element modeling based on ambient vibration testing. The study includes finite element modeling, analytical modal analyses, ambient vibration testing and earthquake analyses of the bridges. For the purpose, four prestressed precast I beam bridges that were constructed for the Ankara-Sivas high speed railway line are selected for analytical and experimental studies. In the study, firstly a literature review related to the dynamic behavior of bridges especially precast beam bridges is given and then the formulation part related to ambient vibration testing and structural performance according to Turkish Seismic Code (2007) is presented. Next, 3D finite element models of the bridge are described and modeled using LARSA 4D software, and analytical dynamic characteristics are obtained. Then ambient vibration testing conducted on the bridges under natural excitations and experimental natural frequencies are estimated. Lastly, time history analyses of the bridges under the 1999 Kocaeli, 1992 Erzincan, and 1999 Duzce Earthquakes are performed and seismic performance levels according to TSC2007 are determined. The results show that the damage on the bridges is all under the minimum damage limit which is in the minimum damage region under all three earthquakes.

An Analytical Model of Eddy Current Signal using Integral Method (적분법을 이용한 와전류신호의 해석적 모델)

  • Cheong, Y.M.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.11 no.2
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    • pp.7-14
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    • 1991
  • The integral model for the eddy current phenomena has been suggested. The model could lift the limitations of the previously well-known analytical model of eddy current theory. The model could be applied to two-dimentional, arbitary shaped defects. The computer programs have been developed in order to calculate the eddy current signal with the suggested integral method. The eddy current signals by the model calculations have been shown similar patterns to the actual experimental data from the real defects in the calibration standard tubes.

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Guided Wave Calculation and Its Applications to NDE

  • Hayashi, Takahiro
    • Journal of the Korean Society for Nondestructive Testing
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    • v.24 no.2
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    • pp.125-135
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    • 2004
  • This paper describes the calculation technique for guided wave propagation with a semi-analytical finite element method (SAFEM) and shows some results of numerical calculation and guided wave simulation for plates, pipes and railway rails. The SAFEM calculation gives dispersion curves and wave structures for bar-like structures. Dispersion curve software for a pipe is introduced, and also dispersion corves for a rail are given and experimentally verified. The mode conversions in a plate with a defect and in a pipe with an elbow or a defect are shown as examples of our guided wave simulations.

The Study on Analytical Method of Lead, Cadmium and Chromium in Copper Metal by Matrix Matching Method of Inductively Coupled Plasma Atomic Emission Spectrometer (유도결합 플라즈마 발광분광기의 매트릭스 보정법에 의한 구리 중납, 카드뮴 및 크롬 분석에 관한 연구)

  • Joo, Sung-Kyun;Kim, Joon;cheong, Nam-Yong;Lim, Kyu-Chual;Choi, Young-Hwan;Kim, Sang-Kyung
    • Journal of the Korean Chemical Society
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    • v.53 no.3
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    • pp.293-301
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    • 2009
  • Analytical results of a fixed concentration of Pb, Cd and Cr in the synthetic copper standard solution (RMs) for using the matrix no matched standard calibration curve at various wavelength by ICP showed that accuracy (140 $\sim$ 1,070% in case of Pb) is very poor at all wavelengths because of the Cu matrix effect. Analytical results of a fixed concentration of Pb, Cd and Cr in the different concentration solutions of Cu showed that found values were on the increase or decrease as the rate of a regular equation as the concentration of Cu was increased. Accuracies by the Cu matching method in the analysis of Pb, Cd and Cr in the synthetic copper standard solution (RMs) were higher than 99.9%.

Modal testing and finite element model calibration of an arch type steel footbridge

  • Bayraktar, Alemdar;Altunisk, Ahmet Can;Sevim, Baris;Turker, Temel
    • Steel and Composite Structures
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    • v.7 no.6
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    • pp.487-502
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    • 2007
  • In recent decades there has been a trend towards improved mechanical characteristics of materials used in footbridge construction. It has enabled engineers to design lighter, slender and more aesthetic structures. As a result of these construction trends, many footbridges have become more susceptible to vibrations when subjected to dynamic loads. In addition to this, some inherit modelling uncertainties related to a lack of information on the as-built structure, such as boundary conditions, material properties, and the effects of non-structural elements make difficult to evaluate modal properties of footbridges, analytically. For these purposes, modal testing of footbridges is used to rectify these problems after construction. This paper describes an arch type steel footbridge, its analytical modelling, modal testing and finite element model calibration. A modern steel footbridge which has arch type structural system and located on the Karadeniz coast road in Trabzon, Turkey is selected as an application. An analytical modal analysis is performed on the developed 3D finite element model of footbridge to provide the analytical frequencies and mode shapes. The field ambient vibration tests on the footbridge deck under natural excitation such as human walking and traffic loads are conducted. The output-only modal parameter identification is carried out by using the peak picking of the average normalized power spectral densities in the frequency domain and stochastic subspace identification in the time domain, and dynamic characteristics such as natural frequencies mode shapes and damping ratios are determined. The finite element model of footbridge is calibrated to minimize the differences between analytically and experimentally estimated modal properties by changing some uncertain modelling parameters such as material properties. At the end of the study, maximum differences in the natural frequencies are reduced from 22% to only %5 and good agreement is found between analytical and experimental dynamic characteristics such as natural frequencies, mode shapes by model calibration.