• Title/Summary/Keyword: analysis and synthesis

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Synthesis and surface characterization of mesoporous carbon for the adsorption of methane gas (메탄가스 흡착을 위한 메조포러스 카본 합성과 표면 특성 연구)

  • Park, Sang-Won;Lee, Kamp-Du;Noh, Min-Soo
    • Journal of Environmental Science International
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    • v.22 no.7
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    • pp.837-845
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    • 2013
  • This study was designed to synthesize mesoporous carbon, porous carbonic material and to characterize its surface in an attempt to adsorption methane gas($CH_4$). Synthesis of mesoporous carbon was carried out under two steps ; 1. forming a RF-silica complex with a mold using CTMABr, a surfactant, and TEOS, raw material of silica, and 2. eliminating silica through carbonization and HF treatment. The mesoporous carbon was synthesized under various conditions of synthesis time and calcination. Eight different types of mesoporous carbon, which were designated as MC1, MC2, MC3, MC4, MCT1, MCT2, MCT3, and MCT4, were prepared depending upon preparation conditions. The analysis of mesoporous carbon characteristics showed that the calcination of silica stabilized the mixed structure of silica and carbonic complex, and made the particle uniform. The results also showed that hydrothermal synthesis time did not have a strong influence on the size of pore. The bigger specific surface area was obtained as the hydrothermal synthesis time was extended. However, the specific surface area was getting smaller again after a certain period of time. In adsorption experiments, $CH_4$ was used as adsorbate. For the case of $CH_4$, MCT3 showed the highest adsorption efficiency.

Synthesis of Japanese Encephalitis Virus in Porcine Kidney Stable Cells Observed by Fluorescent Antibody Technique and Autoradiography

  • Lee, Chong-Hoon;Fukai, Konosuke
    • The Journal of the Korean Society for Microbiology
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    • v.3 no.1
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    • pp.51-65
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    • 1968
  • The site of the synthesis of Japanese encephalitis virus(JEV) in the actinomycin-treated and infecter PS Y15 cells(a porcine kidney stable cell line) was observed by the immunofluorescent antibody technique, acridine orange staining, and the autoradiographic analysis. In the parallel studies by immunofluorescent technique and acridine orange staining it the infected cells, Viral protein(as an antigen) and viral RNA were detected at the same site of cytoplasm. In the autoradiographic analysis, the cytoplasmic labeling of $^3H$-uridine was due to the synthesis of JEV-RNA, while the nucleolus and nucleus were not involved. In the autoradiographic studies on the secton of infected cells, the $^3H$-uridine was frequently incorporated around the cytoplasmic vacuoles. This localization of labeling agreed with the site of acridine orange positive granules. The results suggest that the syntheses of the viral RNA and viral protein occurred in the similar site of cytoplasm of the infected cells, and also the virus particles seem to be assembled in the sites of the viral RNA and protein syntheses.

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Synthesis and Implementation of a Multi-Port DC/DC Converter for Hybrid Electric Vehicles

  • Santhosh, T. K.;Natarajan, K.;Govindaraju, C.
    • Journal of Power Electronics
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    • v.15 no.5
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    • pp.1178-1189
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    • 2015
  • A non-isolated Multiple Input Converter (MIC) with an input port, two storage ports and a load port is proposed. The synthesis of the proposed four port converter with its switch realization is presented. A steady state analysis of each operating mode with a small-signal model is derived, and a stability analysis is done. A mode selection controller is proposed to automatically choose a specific operating mode based on the voltage levels of the different source and storage units. In addition, a voltage control loop is used to regulate the output voltage. A 200W prototype is built with a TMS320F28027 DSP controller to test the feasibility of the operating modes. Simulation and experimental results show the ability of the proposed converter to handle multiple inputs either individually or simultaneously.

Study on the synthesis and characterization of soybean based transformer oils (대두유 에스테르계 절연유의 합성과 분석)

  • Han, Dong-Hee;Cho, Han-Goo;Han, Se-Won;Ahn, Myeong-Sang;Oho, Dae-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.244-245
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    • 2005
  • Electrical insulation is one of the most important parts in a high voltage apparatus. Traditionally mineral oils and synthetic esters have been widely used as dielectric coolants for power transformers. Recently, researchers are interested in the environmental friendly vegetable oil from environmental viewpoint. This paper reports on the synthesis and characterization of soybean based ester oils. Two different types of soybean based transformer oils, named as methyl ester and isopropyl ester were synthesized. The synthesis of these esters was achieved by transesterification reactions of soybean oil and alcohol in the presence of catalyst. The GC and NMR spectroscopic analysis of the esters have been performed. The thermal stability of the esters was determined by thermal gravimetric analysis(TGA).

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Synthesis and spectroscopic characterization of zinc ferrite nanoparticles

  • Arora, Shefali;Nandy, Subhajit;Latwal, Mamta;Pandey, Ganesh;Singh, Jitendra P.;Chae, Keun H.
    • Advances in nano research
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    • v.13 no.5
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    • pp.437-451
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    • 2022
  • Synthesis approaches usually affect the physical and chemical properties of ferrites. This helps ferrite materials to design them for desired applications. Some of these methods are mechanical milling, ultrasonic method, micro-emulsion, co-precipitation, thermal decomposition, hydrothermal, microwave-assisted, sol-gel, etc. These methods are extensively reviewed by taking example of ZnFe2O4. These methods also affect the microstructure and local structure of ferrite which ultimately affect the physical and chemical properties of ferrites. Various spectroscopic techniques such as Raman spectroscopy, Fourier Transform Infrared spectroscopy, Ultra Violet-Visible spectroscopy, Mossbauer spectroscopy, extended x-ray absorption fine structure, and electron paramagnetic resonance are found helpful to reveal this information. Hence, the basic principle and the usefulness of these techniques to find out appropriate information in ZnFe2O4 nanoparticles is elaborated in this review.

Analysis of Vibration Characteristics of a Full Vehicle Model Using Substructure Synthesis Method (부분구조합성법을 이용한 전차량 모델의 진동 특성 분석)

  • Kim, Bum-Suk;Kim, Bong-Soo;Yoo, Hong-Hee
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.5
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    • pp.519-525
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    • 2010
  • The finite element (FE) method is generally used to model and simulate the physical behavior of large structures, such as passenger vehicles or aircraft. However, FE analysis involves a very large computation time and cost for developing the analysis model. Therefore, the vibration characteristics of large structural systems are often analyzed using the component mode synthesis (CMS) method, which is one of the substructure synthesis methods. In this study, the vibration characteristics of passenger vehicles are analyzed by using the substructure synthesis method. A passenger vehicle model, which includes a vehicle body, suspension systems, and a sub-frame, is presented. The physical components of the vehicle system are modeled as equivalent substructures using the Craig-Bampton method of CMS. The vibration characteristics, such as the natural frequencies and mode shapes and frequency response, of the vehicle system are determined. The effects of variations in some design parameters on the vibration characteristics of the full vehicle model are also investigated.

Comparative Study on DAE Solution Methods for Effective Multi-Body Dynamics Analysis of Unmanned Military Robot Based on Subsystem Synthesis Method (무인 국방 로봇의 효과적인 다물체 동역학 해석을 위한 부분시스템 합성방법 기반 DAE 해석 기법 비교 연구)

  • Kim, Myoung Ho;Kim, Sung-Soo;Yun, Hong-Seon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.9
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    • pp.1069-1075
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    • 2013
  • An effective method is necessary for the real-time analysis of an unmanned military robot. To achieve highly efficient simulations, a subsystem synthesis method has been developed. The subsystem synthesis method separately generates equations of motion for the base body and for the subsystem. The equations of motion are expressed by DAE, which consist of differential equations and algebraic equations. To increase the accuracy and efficiency of solutions, DAE solvers such as the Direct, CS (Constraint Stabilization), and GCP (Generalized Coordinate Partitioning) method are employed. In this study, the subsystem synthesis method is applied for effective multi-body dynamics analysis of an unmanned military robot, and a comparative study of three different DAE solvers is carried out.

Analysis of the Timing of Spoken Korean Using a Classification and Regression Tree (CART) Model

  • Chung, Hyun-Song;Huckvale, Mark
    • Speech Sciences
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    • v.8 no.1
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    • pp.77-91
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    • 2001
  • This paper investigates the timing of Korean spoken in a news-reading speech style in order to improve the naturalness of durations used in Korean speech synthesis. Each segment in a corpus of 671 read sentences was annotated with 69 segmental and prosodic features so that the measured duration could be correlated with the context in which it occurred. A CART model based on the features showed a correlation coefficient of 0.79 with an RMSE (root mean squared prediction error) of 23 ms between actual and predicted durations in reserved test data. These results are comparable with recent published results in Korean and similar to results found in other languages. An analysis of the classification tree shows that phrasal structure has the greatest effect on the segment duration, followed by syllable structure and the manner features of surrounding segments. The place features of surrounding segments only have small effects. The model has application in Korean speech synthesis systems.

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A Channel Flood Routing by the Implicit Dynamic Wave Model

  • Yoon, Yong-Nam;Chung, Jong-Ho
    • Korean Journal of Hydrosciences
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    • v.2
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    • pp.69-84
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    • 1991
  • US NWS/NETWORK is applied for the analysis of the flood of July 11-15, 1981 through the Goan-Indogyo reach of the Han River. For the flood hydrography synthesis of the lateral inflows from the major tributaries into the main reach the Cleak method is employed. NETWORK coupled with the Clark method of hydrography synthesis simulated with a fair accuracy the oberved flood hydrograph at the downstream boundary of the routing reach. The dffect of SCS runoff curve number for fributary flood synthesis is evaluated. The characteristics of the station variations and time variations of the flood discharges in the reach is also analyzed.

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Optimal synthesis and design of heat transfer enhancement on heat exchanger networks and its application

  • Huang, Zhao-qing
    • 제어로봇시스템학회:학술대회논문집
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    • 1996.10a
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    • pp.376-379
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    • 1996
  • Synthesis for qualitative analysis in connection with quantitative analysis from the pinch design method, EVOP and Operations Research is proposed for the optimal synthesis of heat exchanger networks, that is through of the transportation model of the linear programming for synthesizing chemical processing systems, to determine the location of pinch points, the stream matches and the corresponding heat flowrate exchanged at each match. In the second place, according to the optimization, the optimal design of heat transfer enhancement is carried on a fixed optimum heat exchanger network structure, in which this design determines optimal operational parameters and the chosen type of heat exchangers as well. Finally, the method of this paper is applied to the study of the optimal synthetic design of heat exchanger network of constant-decompress distillation plants.

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