• Title/Summary/Keyword: alumna

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Effect of Metal Fluoride on the Formation of α-Alumina Particles (금속 불화물 첨가제가 α-알루미나 입자생성에 미치는 영향)

  • Seo, Geum-Suk;Lee, Sang-Geun;Ahn, Byung-Hyun;Ju, Chang-Sik;Hong, Seong-Soo;Park, Seong-Soo;Lee, Gun Dae
    • Korean Chemical Engineering Research
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    • v.48 no.5
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    • pp.627-631
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    • 2010
  • $\alpha$-Alumna particles were prepared by a precipitation method with metal fluoride additive. Aluminum nitrate and ammonia solution were used as starting materials. $AlF_3$, $CaF_2$, and $MnF_2$ were utilized as additives. The effects of precipitation solvent and metal fluoride on the phase transformation temperature, size and morphology of $\alpha$-alumna particles were investigated. The solvent for precipitation did not affect the phase transformation temperature, while it influenced the size of $\alpha$-alumna particles. The phase transformation temperature to $\alpha$-alumna was reduced by addition of metal fluoride and was different with metal cation in metal fluoride ($AlF_3(800^{\circ}C)$ < $MnF_2(900^{\circ}C)$ < $CaF_2(950^{\circ}C)$). The addition of each of three metal fluorides led to the formation of platelike particles and, among the three additives, $MnF_2$ additive resulted in the formation of relatively small particle.

A Study on Wettability of Silicate Glasses on the Different Impurities in Alumina Substrates (알루미나의 순도에 따른 알루미나와 실리케이트계 유리와의 젖음성에 관한 연구)

  • 안병국
    • Journal of Welding and Joining
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    • v.16 no.2
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    • pp.122-128
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    • 1998
  • This investigation was performed to collect fundamental informations concerning the behavior of glass solders on ceramic joining process. The wettability of glasses on two types of alumina was evaluated by sessile drop method. SiO$_2$-CaO-Al$_2$O$_3$system glasses were selected as solder glasses, and alumina that have different purities were used for substrate materials. It is indicated that contact angles of glasses on 99% purity of alumina substrate do not change as increasing time at elevated temperature, however the contact angles on the 92% purity of alumina substrate exhibit the strong time dependency. The time-dependent property on 92% alumina was due to the interlayer reactions occurred between the glass solder and impurities on the substrate.

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Effect of Electrical Properties on the EPDM- $Al(OH)_3$ Composite by UV Accelerated weathering (Al(OH)3가 EPDM의 자외선 촉진열화에 미치는 전기적 특성평가)

  • Shim, Dae-Sup
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.243-247
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    • 2003
  • The effect of accelerated weathering(UV) on three type of ethylene propylene diene monomer(EPDM) composite used for higher voltage insulator were investigated by weather-emoter. For weatherability of EPDM composite, surface resistance, dielectric breakdown strength, change of contact angle, surface composition were measured according to UV accelerated weathering time. From the resort of the measurement of surface resistivity, contact angle of EPDM composite decreased and showed chalking and cracking phenomenon when UV weathweing time was for 1500 h and 2000 h. The analysis of surface atomic composition indicated that surface aluminiu(Al) content was detected due to chalking phenomenon after 1500 h of UV weathering, Oxygen content of all composite increased due to the oxidation.

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Basic Experimental Investigations to UV Laser Micro-Machining of Nano-Porous Alumina Ceramic Material (나노 다공 구조를 가진 알루미나 재료의 UV 레이저 미세가공에 관한 실험적 기초 연구)

  • Shin, Bo-Sung;Lee, Jung-Han
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.11 no.1
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    • pp.62-67
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    • 2012
  • Recently UV laser is widely used to process micro parts using various materials such as polymers, metals and ceramics because it has a very high intensity at the focused spot area. It is generally known that there are still some difficulties for alumina($Al_2O_3$) ceramics to directly make micro patterns like holes and lines on the surface of working material using 355nm UV laser because the alumina has a very low absorption coefficient at that wavelength. But nowadays new alumna with nano-porous holes is developed and applied to advanced micro functional parts of IT, BT and BT industries. In this paper, we are going to show the mechanism of photo-thermal ablation for nano-porous ceramics. Inside hole there is a lot of multiple reflections along the depth of hole. Experimentally we can find the micro hole drilling and micro grooving on the surface of nano-porous alumina.

Ka-Band MMIC VCO Design and its Fabrication (Ka-Band용 MMIC VCO의 설계 및 제작)

  • Kim, Wan-Sik;Kang, Seo;Kang, Dae-Hyun;Jeong, Seong-Il;Lee, Jae-Cheul;Lee, Jong-Arc
    • Journal of IKEEE
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    • v.7 no.2 s.13
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    • pp.230-235
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    • 2003
  • A small and integrated MMIC VCO(Voltage Controlled Oscillator) at Ka-band has been developed. This oscillator was designed as Clapp-Gouriet type scheme, fabricated, and implemented on the carrier. This was connected to an alumna substrate on the carrier providing output port for module, utilizing ribbon and wire bonding technique allowing the loss of 0.2dB. This VCO module showed the excellent performance.

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Humidity Sensitive Properties of Polymer Electrolytes of Quaternary Ammonium methacrylate derivatives (메타크릴레이트계 4차 암모늄 유도체 고분자 전해질의 감습특)

  • Kim, Tae-Mi;Gong, Myeong-Seon;Lee, Im-Yeol;Park, Jeong-Gi
    • Korean Journal of Materials Research
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    • v.3 no.6
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    • pp.598-605
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    • 1993
  • Methacryloxyethyl dimethyl alkyl($C_{1}\sim C_{12}$, benzyl and 2, 2-diethoxy ethyl) ammonium bromide monomers were prepared to investigate the relative humidity characteristics for polymer electrolytes with different chemical structures. They were coated on the alumna substrate printed comblike gold electrode by photopolymerization after micro-syringe injection. As the thickness of rhe humid membrane increased, the impendance decreased, whereas the impedance ~ncreased as the carbon cham of alkyl substituent in the monomer increased. The impendance of the polymeric electrolytes with $C_6\sim C_8$ substituents were varied from 19M$\Omega$ to 5K$\Omega$ for the range of 30-90% Mi. The temperature depedence coefficient in the range of 15-$35^{\circ}C$ was found to be -0.45% $RH/^{\circ}C$and the hysteresis falled within the range of $\pm$2% RH. The response time was 35 second for varying humldity from 33% to 85% RH.

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Relationship of parenting style perceived by middle school students, their peer attachment, relationship with teacher, and self-identity with career identity (중학생이 지각하는 부모양육방식, 또래애착, 교사관계, 자아정체감과 진로정체감과의 관계)

  • Noh, So Young;Yu, Nan Sook
    • Journal of Korean Home Economics Education Association
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    • v.30 no.2
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    • pp.21-37
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    • 2018
  • The purposes of this study were to examine the influence of the self-identity, parenting style, peer attachment, and relationship with teacher on career identity, and to verify if self- identity shows the moderating effect in the relationship among the parenting style, peer attachment, relationship with teacher, and career identity of middle school students. The data of 3rd-year middle school students, from the 1st grade panel of 'Korea Children And Youth Panel Survey(KCYPS)' by National Youth Policy Institute, was used as the analysis data. The program which was used for the analysis was SPSS ver 22.0 for descriptive, Cronbach's α, and multiple regression analysis. The results of this study are as follows. First, it was revealed that the most influential variable for career identity was self identity, followed by peer attachment, while relationship with teacher is least influential. Parenting style did not have a direct effect on career identity. Second, it was revealed that self-identity had a moderating effect when the interaction between parenting style and the self-identity, and the interaction between relationship with teacher and the self-identity were injected. Therefore, if the education related to the self-identity is conducted continuously in the home economics subject, the conflict and anxiety on the career problem of middle school students will be reduced and the career identity will be developed more effectively.

Synthesis of Low-Priced Catalyst from Coal Fly Ash for Pyrolysis of Waste Low Density Polyethylene (석탄비산재(石炭飛散災)로부터 저밀도(低密度) 폴리에틸렌 폐기물(廢棄物) 열분해용(熱分解用) 저가(低價) 촉매(觸媒) 합성(合成))

  • Jeong, Byung-Hwan;Na, Jeong-Geol;Kim, Sang-Guk;Mo, Se-Young;Chung, Soo-Hyun
    • Resources Recycling
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    • v.16 no.2 s.76
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    • pp.48-55
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    • 2007
  • A low-priced catalyst for pyrolysis of LDPE has been synthesized. Fly ash, which is waste material generated from coal-fired power plants was used as silica and alumna sources for solid acid catalyst. Amorphous silica-alumina catalysts (FSAs) were pre-pared by dissolution of silica and alumina from fly ash, followed by co-precipitation of the dissoluted ions. A series of LDPE pyrolysis were carried out in a thermogravimetric analyzer to investigate the effects of synthesis conditions such as NaOH/fly ash weight ratio and activation time one catalytic performance of FSAs. The physical properties of FSAs were examined and related to their catalytic performances. FSA(1.2-8) synthesized with NaOH/fly ash weight ratio of 1.2 and the activation time of 8 hours showed the best catalytic performance. The catalytic performance of FSA(1.2-8) was comparable with that of commercial catalysts and it was concluded that the FSA could be a good candidate for catalytic use in the recycling of waste polyolefins.

Back Flushing Behavior of Microfiltration Membrane Fouled by Alumna Colloidal Suspensions (알루미나 현탁액에 의해 오염된 정밀여과막의 역세척 거동)

  • Nam, Suk-Tae;Han, Myeong-Jin
    • Membrane Journal
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    • v.19 no.1
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    • pp.34-46
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    • 2009
  • Effect of backflushing on the membrane fouling for polyethylene capillary membranes was examined by measuring the flux of $Al_2O_3$ colloidal suspensions through the cross flow microfiltration. In the comparison of with and without the application of backflushing, the hydraulic resistance to permeate flow of the suspension was less with backfluslng, but the Increasing rate in permeate resistance was higher. Regardless of backflushing, the cake filtration was dominant at the initial period of filtration with backflushing, being followed by the pore blocking. And at steady state, the fouling mechanism is almost governed by the cake filtration model. On the contrary, the pore blocking preceded the cake filtration in the initial stage of the original membrane before backflushing. And irrespective of backflushing, the ratio of cake filtration to total fouling increased, compared with that fur before backflushing. For the membrane with $0.24{\mu}m$ pore size, the permeate resistance was higher than that of $0.34{\mu}m$ pore size membrane. but the ratio of cake filtration was smaller than that of large pore membrane. In comparing the ratio of each fouling component to the total fouling for the case with backflushing pore blocking was 7.8% and cake filtration was 92.2%. for the case without backflushing, total fouling was composed of 9.6% pore blocking and 90.4% cake filtration.

The Design and Development of Online System to Improve Undergraduate Students' Competency (대학생의 역량개발을 위한 온라인 시스템 설계 및 개발)

  • Moon, Yun-Kyoung;Lee, Kyoung-Jae
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.6
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    • pp.3807-3818
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    • 2015
  • The objective of this study is to develop an on-line system for improving undergraduate students' competency development. After drawing elements necessary for the competency development such as assessment and planning, competency development, analysis of competency assessment, portfolio, analysis of job ability and community, based on the literature research related to competency and the analysis of the existing system, the direction of the system design was set up. The system was developed by using Microsoft Windows operating system in Windows server, ORACLE ver.10 as its database management system, and JSP and JAVA as its programing language. Reviewing errors and improvements of the system, it was modified and complemented. In order to examine the content functional utilization of the final competency development system, the utilization was verified. The competency development system for undergraduate students can be used as on-line space filled with the internalization of knowledge, self-directed competency development, convenience of record management and interactions between students-professors-alumna, owing to its functions such as boosting competency activities, cultivating career-pioneering ability and introspecting. When it is rare to find researches on the competency development system for undergraduate students, it is expected to be helpful to the development of competency education and the career education for undergraduate students as a new alternative for the competency development.