• Title/Summary/Keyword: aging treatment

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The Effect of Heat Treatment on the Microstructural Evolution and Mechanical Properties of Co-base Materials (CO-기 합금의 열처리에 의한 미세조직 및 기계적 특성변화에 관한 연구)

  • Kim, Gi-Yeob;Jung, Byong-Ho;Ahn, Yong-Sik
    • Journal of Power System Engineering
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    • v.5 no.2
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    • pp.63-70
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    • 2001
  • To obtain the optimal condition of heat treatment of wear-resistant alloy, hardness and Charpy V-notch test have been performed with Co-based Stellite No.4, No.6 and Tribaloy 800 alloys, following by heat treatment at the various conditions. Heat treatment at $1250^{\circ}C$ for 1 hours caused the as-casted Tribaloy 800 with FCC crystal structure to transform to HCP structure and lamellar eutectic structure was disappeared, which did not influence on the hardness. Aging at $800^{\circ}C$ for 20 hours, following by $1250^{\circ}C$ for 2 hours heat treatment has enhanced hardness significantly, which is due to the precipitation of large amounts of Laves-phase. The hardness of Stellite alloys was increased by the aging at $800^{\circ}C$ to 5 hours, and was nearly constant by the aging over 5 hours. The toughness of Stellite alloys was a few influenced by the aging treatment.

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Treatment of Presbyphonia (Aging Voice) (노인성 음성의 치료)

  • Kwon, Tack-Kyun
    • Journal of the Korean Society of Laryngology, Phoniatrics and Logopedics
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    • v.25 no.1
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    • pp.13-15
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    • 2014
  • Presbyphonia is defined as voice change caused by aging. Since presbyphonia is one of the natural aging processes, the treatment should be considered for the patients complaining communication difficulties. The treatment should not only target on presbylaryngis, but also on underlying systemic conditions such as lung function, neurological diseases and medications. Therefore, the treatment for the patients with presbyphonia should be multidisciplinary including underlying disease control, voice therapy and surgical treatment. Although various experiments on treatment of presbylaryngis are currently being tried, repeated injection laryngoplasty is still playing an important role because presbyphonia is destined to get worse over time.

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Dependence of Hardness Change on Microstructure during Isothermal Aging in Mg-Al Alloy (Mg-Al 합금에서 등온 시효 중 경도 변화의 미세조직 의존성)

  • Han, Jin-Gu;Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.6
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    • pp.249-255
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    • 2019
  • This study is intended to clarify the main microstructural factors that contribute to an increase of hardness during isothermal aging in Mg-Al alloy. For this work, Mg-9.3%Al alloy specimens were solution-treated at 688 K for 24 h followed by water quenching, and then aged at 473 K for up to 24 h. The aging at 473 K yielded nodular discontinuous precipitates (DPs) with (${\alpha}+{\beta}$) lamellar morphology at the grain boundaries, and the volume fraction of DPs increased from 0% to ~30% with increasing aging time up to 12 h. For the aging times longer than 12 h, further formation of DPs was substantially inhibited owing to the occurrence of significant continuous precipitation within the ${\alpha}-(Mg)$ matrix, and the density of continuous precipitates (CPs) becomes greater with increasing aging time. Hardness of the specimen was steadily increased with aging time up to 24 h. Microstructural examination on the aged specimens revealed that the increased overall hardness at the early stage of aging is associated with the increased volume fraction of DPs, but at the later stage of aging, where the amount of DPs was hardly changed, the increased hardness of the ${\alpha}-(Mg)$ matrix in response to the higher density of CPs within the matrix, plays a key role in increasing the overall hardness value.

Influence of Rainfall During the Ripening Stage on Pre-Harvest Sprouting, Seed Quality, and Longevity of Rice (Oryza sativa L.)

  • Baek, Jung-Sun;Chung, Nam-Jin
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.59 no.4
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    • pp.406-412
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    • 2014
  • The influence of rainfall during the ripening stage on pre-harvest sprouting, seed viability, and seed quality was investigated in two Korean rice cultivars, Shindongjin and Hopum. When the rainfall was artificially treated in a greenhouse, HP started to pre-harvest sprouting at three days of rainfall treatment (DRT), but Shindongjin did not show pre-harvest sprouting at 40 DAH treatment and just 0.3~0.8% at 50 DAH, which was much lower than 15.3~25.8% of Hopum in the same treatment. After harvest, the seed germination of Hopum decreased about 10~25% compared to non-treated seeds, but that of Shindongjin decreased much little rate than that of Hopum. The seed longevity tested by accelerated aging decreased with prolonged rainfall period in both cultivars, but the varietal difference was clear; Shindongjin could withstand longer accelerated aging than Hopum. Shindongjin maintained its germination (>50%) ability after 15 days of accelerated aging regardless of the rainfall treatment period and time, but Hopum dropped below 50% germination ability after only 5 days of accelerated aging. In conclusion, rainfall during the ripening stage induced not only pre-harvest sprouting, but also reduced seed quality and longevity during storage, which varied between two cultivars.

Surface Composition Change of UV/Ozone Modified Polypropylene (UV/오존에 의해 개질된 폴리프로필렌의 표면 조성 변화)

  • Kim, J.I.;Ryu, S.H.
    • Elastomers and Composites
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    • v.37 no.1
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    • pp.49-56
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    • 2002
  • Polypropylene is oxidized with UV/ozone as a function of UV treatment time and ozone flow rate and its surface characteristics are investigated using contart angle measurements and XPS. The aging behavior of oxidized surface is investigated under air, water and ethylene glycol as the aging media. Adhesion strength is also investigated using a lap shear test. Polar surface energy increases with increasing UV/ozone treatment time as well as ozone flow rate. No polar surface energy change is observed under water aging, while under air aging it decreases significantly within 2-3 days and reaches the close value as that of the untreated PP. Adhesion strength increases with increasing UV/ozone treatment time as well as ozone flow rate.

Mechanical Properties of Forged Nimonic 80A Superalloy Fabricated by Vacuum Spray Casting (진공분무주조법에 의해 제조한 Nimonic 80A 초내열합금 단조재의 기계적 특성)

  • Lee, Yun-Soo;Hyun, Soong-Keun;Jung, Dae-Hyun;Byun, Joong-Sig
    • Korean Journal of Metals and Materials
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    • v.50 no.4
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    • pp.263-270
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    • 2012
  • This study investigates the effect of heat treatment on the mechanical properties of a forged Ni-based superalloy called Nimonic 80A. Nimonic 80A ingot samples were fabricated by vacuum spray casting to achieve a fine and homogenized microstructure. The ingot samples were subsequently hot-forged with the diameter of 220 mm at 1373 K. From the center to the surface of the forged Nimonic 80A, its average grain size decreased and its micro-Vickers hardness increased slightly. Solution treatment was carried out at 1353 K with 8 hours of air cooling followed by aging treatment, which was carried out in the range of 873-1073 K with various times from 0.5 to 256 hours. To set the optimum aging conditions, micro-Vickers hardness tests were performed. The maximum hardness value of 388.0 Hv was obtained by aging at 973 K for 32 hours. Also, tensile tests were performed for optimum aging conditions at room temperature and 873 K. The results can be used effectively to perform reasonable heat treatment of Nimonic 80A superalloy.

Changes of Carbide Characteristics and Magnetic Properties in Artificially Aging Heat Treated 2.25CrMo Steel (경년열화 열처리된 2.25CrMo 강에서의 탄화물 특성 및 자기적 성질의 변화)

  • Byeon, Jal Won;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.14 no.6
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    • pp.323-329
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    • 2001
  • Artificial aging was performed to simulate the microstructural degradation in 2.25CrMo steel arising from long time exposure at $540^{\circ}C$. The carbide morphologies were classified as acicular, pipe and globular type, and the number of carbides per unit area was measured for each type of carbides. The fine acicular carbides were found to diminish drastically in the initial stage of aging. An attempt was made to evaluate the microstructural degradation in artificially aging heat treated 2.25CrMo steel by the magnetic property measurements such as saturation magnetization, coercivity and remanence. The saturation magnetization showed no distinct trend with aging time. However, the coercivity and remanence were observed to decrease rapidly in initial 920 hours of aging time and then decrease slowly afterwards.

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Effect of Aging Treatment on the Microstructure and Mechanical Properties of Mg-6Al-xZn (x : 1.5, 2.5) Alloys Fabricated by Squeeze Casting (용탕단조된 Mg-6Al-xZn (x=1.5, 2.5) 합금(合金)의 미세조직 및 기계적 성질에 미치는 시효의 영향)

  • Kim, Soon Ho
    • Journal of the Korean Society for Heat Treatment
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    • v.12 no.1
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    • pp.1-8
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    • 1999
  • This study has investigated the effect of aging treatment on the microstructure and mechanical properties of Mg-6Al-xZn(x = 1.5, 2.5) alloys fabricated by the squeeze casting process. The microstructures of as-squeeze cast were composed of pro-eutectic ${\alpha}$, super saturated ${\alpha}$ and ${\beta}(Mg_{17}Al_{12})$ compound. Aged at both $200^{\circ}C$ and $240^{\circ}C$, Mg-6Al-xZn alloys showed the peak hardness due to the formation of ${\beta}(Mg_{17}Al_{12})$ precipitates. The discontinuous precipitates of the lamella type are predominant at $200^{\circ}C$ aging treatment, while the finely dispersed continuous precipitates were dominant at $240^{\circ}C$ aging treatment. Mg-6Al-xZn alloys fabricated by the squeeze casting process had the better combination of tensile strength and elongation compared to the conventionally cast alloys. As zinc contents increased, the tensile strength was increased by the solid solution strengthening effect of zinc.

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Effect of Aging Heat Treatment on the Mechanical Properties in Inconel 718 Alloy (Inconel 718 합금의 시효열처리가 기계적 성질에 미치는 영향)

  • Kang, Hee Jae;Kim, Jung Min;Jee, Sung Hwan;Sung, Jie Hyun;Kim, Young Hee;Sung, Jang Hyun;Jeon, Eon Chan
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.3
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    • pp.271-277
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    • 2013
  • Inconel 718 super alloy was aging heat treated at the temperature range from $675^{\circ}C$ to $785^{\circ}C$ for 5~40 hours after solution annealing at $1025^{\circ}C$ for 1 hour. The aging treated specimens were investigated microstructure, mechanical properties and thermal expansion/contraction. Precipitates appeared for a long time aging treatment were niobium carbide and also ${\gamma}^{\prime}$ phase. For the aging treatment time of 10 hours, the changes in strength and hardness with increasing aging treatment temperature showed the maximum value at the temperature of $725^{\circ}C$. This maximum value is to be related with the precipitation of ${\gamma}^{\prime}$ and ${\gamma}^{{\prime}{\prime}}$ phases. The decrease in strength, elongation and hardness during long time aging at $725^{\circ}C$ were thought to be induced from the coarsening of the grain size and the transformation of ${\gamma}^{{\prime}{\prime}}$ phase to ${\gamma}^{\prime}$ phase. For the specimens treated for 10 hours, impact energy showed constant value of ~105 J with increasing the aging temperature, however this value continuously decreased with elapsing time at the aging temperature of $725^{\circ}C$. It was found that the decrease in impact value was induced from the coarsening of grain size and the carbide coarsening. The coefficient of thermal expansion of aging treated Inconel 718 alloy increased with raising test temperature, and the coefficient was appeared $11.57{\sim}12.09{\mu}m/m{\cdot}^{\circ}C$ and $14.28{\sim}14.39{\mu}m/m{\cdot}^{\circ}C$, respectively, after heating to $150^{\circ}C$ and $450^{\circ}C$.

A Characteristic of microstructural evolution, microhardness and tensile properties in CrMoV rotor steel weldment experienced by the cyclic thermal aging heat treatment (CrMoV강 용접부의 주기적 열시효처리에 따른 미세조직, 미세경도 및 인장강도 특성)

  • Kim, G.S.;Koh, J.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.12 no.4
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    • pp.303-312
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    • 1999
  • An investigation of the CrMoV rotor steel weldment which experienced by cyclic thermal aging heat treatment and as-received condition was performed. This evaluation was carried out to confirm whether this type of weldment is appropriate for the service environment in terms of microstructural examinations, microhardness measurements and tensile tests. The cyclic thermal aging heat treatment, containing continuous heating and cooling thermal cycle was programmed to simulate the real rotor service condition. The heat treatment was performed for 40 cycles(5920hrs). The results indicated that the weldment was composed of 4 different regions such as heat affected zone of the base metal, butter weld(initial weld), full thickness weld(final weld) and the base metal. The double welding process was applied to eliminate the susceptibility of reheat cracking at heat affected zone of base metal. The grain refinement at the HAZ due to the welding process could reduce the possibility of cracking susceptibility, but its tensile properties was appeared to be low due to the weld metal in as-received condition. The benefit effect, grain refinement was extended with carbides coarsening during the cyclic thermal aging heat treatment. However the poor mechanical properties of the weldment was more degraded as undergoing the heat treatment.

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