• 제목/요약/키워드: advanced characterization

검색결과 1,013건 처리시간 0.029초

Advancing Mathematical Activity: A Practice-Oriented View of Advanced Mathematical Thinking

  • Rasmussen, Chris;Zandieh, Michelle;King, Karen;Teppo, Anne
    • 한국수학교육학회지시리즈E:수학교육논문집
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    • 제18권2호
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    • pp.9-33
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    • 2004
  • The purpose of this paper is to contribute to the dialogue about the notion of advanced mathematical thinking by offering an alternative characterization for this idea, namely advancing mathematical activity. We use the term advancing (versus advanced) because we emphasize the progression and evolution of students' reasoning in relation to their previous activity. We also use the term activity, rather than thinking. This shift in language reflects our characterization of progression in mathematical thinking as acts of participation in a variety of different socially or culturally situated mathematical practices. We emphasize for these practices the changing nature of student' mathematical activity and frame the process of progression in terms of multiple layers of horizontal and vertical mathematizing.

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Facile Synthesis, Characterization and Photocatalytic Activity of MWCNT-Supported Metal Sulfide Composites under Visible Light Irradiation

  • Zhu, Lei;Meng, Ze-Da;Oh, Won-Chun
    • 한국세라믹학회지
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    • 제49권2호
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    • pp.155-160
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    • 2012
  • This paper reported a simple deposition-precipitation method, introducing the metal (Ni, Ag and Sn) and $Na_2S{\cdot}5H_2O$ to preparedispersion metal sulfide nanoparticles on the surface of the Multi-walled carbon nanotube for synthesis of CNT-$M_xS_y$ ($NiS_2$, $Ag_2S$, SnS) composite photocatalysts. The characterization of the prepared CNT-$M_xS_y$ ($NiS_2$, $Ag_2S$, SnS) composites was performed by X-ray diffraction, scanning electron microscopy with energy dispersive X-ray analysis and BET analysis. Furthermore, the MB degradation rate constant for CNT-SnS composite was $5.68{\times}10^{-3}$ under visible light irradiation, which was much higher than the corresponding values for other samples. The detailed formation and photocatalytic mechanism are also provided here.

Effects of Post Annealing on the Electrical Properties of ZnO Thin Films Transistors

  • Moon, Mi Ran;An, Chee-Hong;Na, Sekwon;Jeon, Haseok;Jung, Donggeun;Kim, Hyoungsub;Lee, Hoo-Jeong
    • Applied Microscopy
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    • 제42권4호
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    • pp.212-217
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    • 2012
  • This paper reports the effects of post-annealing of ZnO thin films on their microstructure and the device performance of the transistors fabricated from the films. From X-ray diffraction and transmission electron microscopy characterization, we uncovered that the grain size increased with the annealing temperature escalating and that the film stress shifted from compressive to tensile due to the grain size increment. Electrical characterization revealed that the grain size increase damaged the device performance by drastically lifting the off-current level. By annealing the devices in an $O_2$ ambient (instead of air), we were able to suppress the off-current while improving the electron mobility.

Alternative Sample Preparation Method for Large-Area Cross-Section View Observation of Lithium Ion Battery

  • Kim, Ji-Young;Jeong, Young Woo;Cho, Hye Young;Chang, Hye Jung
    • Applied Microscopy
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    • 제47권2호
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    • pp.77-83
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    • 2017
  • Drastic development of ubiquitous devices requires more advanced batteries with high specific capacitance and high rate capability. Large-area microstructure characterization across the stacks of cathode, electrolyte and anode might reveal the origin of the instability or degradation of batteries upon cycling charge. In this study, sample preparation methods to observe the cross-section view of the electrodes for battery in SEM and several imaging tips are reviewed. For an accurate evaluation of the microstructure, ion milling which flats the surface uniformly is recommended. Pros and cons of cross-section polishing (CP) with Ar ion and focused ion beam (FIB) with Ga ion were compared. Additionally, a modified but new cross-section milling technique utilizing precision ion polishing system (PIPS) which can be an alternative method of CP is developed. This simple approach will make the researchers have more chances to prepare decent large-area cross-section electrode for batteries.

Synthesis and Characterization of Novel Fused Aromatic Semiconductors

  • Zhao, Qinghua;Park, Jong-Won;Kim, Yun-Hi;Kwon, Soon-Ki
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2006년도 6th International Meeting on Information Display
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    • pp.1193-1197
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    • 2006
  • The novel oligomers were synthesized by Grignard reaction, the suzuki coupling reaction, etc. The oligomers were characterized by Infrared (IR), Mass spectrometer (MS). Their thermal properties were investigated by differential scanning calorimetry (DSC) and Thermogravimetric analysis (TGA). The new oligomers showed high thermal stability above $300^{\circ}C$.

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