• Bulletin of the Korean Chemical Society
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• v.25 no.10
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• pp.1508-1512
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• 2004

A gas chromatography/mass spectrometric (GC/MS) method has been developed for the determination of trace mono-n-butyltin (MBT), di-n-butyltin (DBT), and tri-n-butyltin (TBT) compounds in sediments. Samples were extracted by 10% acetic acid in methanol containing 0.03% tropolone and were then derivatized for GC/MS analysis. Ethylation by sodium tetraethylborate and phenylation by sodium tetraphenylborate were evaluated as a derivatization reaction of the organotins in sample extract. n-Hexane was added into reaction media in the beginning of the reaction for the continuous extraction of derivatized organotins. Ethylation requires less than 2 hours to get proper derivatization yields for MBT, DBT, and TBT altogether and produces relatively low amounts of side reaction products. Compared to ethylation, phenylation requires much longer time but provides relatively lower yield and produces considerable amounts of side reaction products. Therefore, the ethylation reaction was applied for the analysis of organotin compounds in sediment. An isotope dilution mass spectrometric (IDMS) method based on GC/MS has been applied to the accurate determination of DBT compounds in the sediments. The IDMS results from the analyses of sediment samples showed a reasonable repeatability and a good agreement with the values obtained by IDMS based on liquid chromatography/induced coupled plasma/mass spectrometry.

• Journal of Institute of Control, Robotics and Systems
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• v.10 no.9
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• pp.833-839
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• 2004

This paper proposes a method that minimizes the consumed energy by searching the optimal locations of the mass centers of links composing of a biped robot using Real-Coded Genetic Algorithm. Generally, in order to utilize optimization algorithms, the system model and design variables must be defined. Firstly, the proposed model is a 6-DOF biped robot composed of seven links, since many of the essential characteristics of the human walking motion can be captured with a seven-link planar biped walking in the saggital plane. Next, Fourth order polynomials are used for basis functions to approximate the walking gait. The coefficients of the fourth order polynomials are defined as design variables. In order to use the method generating the optimal gait trajectory by searching the locations of mass centers of links, three variables are added to the total number of design variables. Real-Coded GA is used for optimization algorithm by reason of many advantages. Simulations and the comparison of three methods to generate gait trajectories including the GCIPM were performed. They show that the proposed method can decrease the consumed energy remarkably and be applied during the design phase of a robot actually.

• Special Issue of the Society of Naval Architects of Korea
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• 2013.12a
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• pp.85-89
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• 2013

In the engine room and the aft body, there are so many fluid tanks such as fresh water tank and oil tank. The vibration analysis for the fluid tank structures has to consider the added mass effect due to the fluid. However, it is known that the result of the fluid tank has the difference according to the boundary condition of the fluid field such as infinite fluid and finite fluid. In this paper, a numerical case study is carried out for the research about the vibration characteristics of the fluid tank with various fluid field. In addition, an experimental study is carried out to verify the validity of the vibration analysis for the fluid tank structure.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.17 no.1 s.118
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• pp.3-9
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• 2007

In this paper, a numerical case study is carried out on the hydroelastic vibration of rectangular plate with various fluid field. It is assumed that the tank wall is clamped along the plate edges. The VMM(virtual mass method) of Nastran is used for the simulation of fluid domain and calculating natural frequency of fluid-coupled structure. In this paper, natural frequencies are calculated and compared for rectangular plates with various fluid field such as infinite fluid and finite fluid, length change of finite fluid field and various fluid contacting conditions.

• Journal of Forest and Environmental Science
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• v.29 no.2
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• pp.109-115
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• 2013

Fast-grown wood generally contains a high proportion of juvenile wood that results in inferior dimensional stability and durability against biological deteriorations. In the present research, the Acacia mangium wood from plantation forests in Vietnam was treated with high temperature in air. The effects of heat treatment on physical properties of Acacia mangium wood, including mass loss (ML), water absorption (WA), water-repellent effectiveness (WRE) and anti-swelling efficiency (ASE) were examined. The results showed that the dimensional stability and the water-repellent effectiveness are increased by about 15-46% and 8-18%, respectively. However, the mass and dimension of wood are decreased. The results also indicated that both treatment temperature and treatment duration significantly affect the wood properties of Acacia mangium. It is thus concluded that heat treatment demonstrates an interesting potential to improve the wood quality of Acacia mangium for solid timber products. This technology provides an environmentally safe method of protecting sustainable common woods to give a new generation of value-added biomaterials with increased stability without the use of toxic chemicals.

• Archives of Pharmacal Research
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• v.19 no.6
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• pp.566-569
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• 1996

A sensitivity method has been developed for the detection and determination of niflmic acid(NA) in human urine. Samples were extracted with diethylether. Flunixin (FN) was added to the sample prior to extraction as an internal standard. Niflumic acid was converted to its methyl derivative and analyzed by capillary gas chromatography/negative chemical isonization mass spectrometry. Using selected ion monitoring (SIM), the levels of NA down to 5 pg/ml could be detected in 5 ml spiked urine sample. Calibration curve was linear over the range of 0.5 ppm-50 ppm. The recovery of niflumic acid from urine at 40 pg/ml was to be $91.7{\pm}3.8(n=3)$ and the coefficient of variation was 4.1%.

• Culinary science and hospitality research
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• v.14 no.3
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• pp.210-222
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• 2008

This study showed that the brown stock, which is the base of demi-glace sauce, extracted by using a high pressure heating extractor is more advantageous than that extracted by the traditional extraction method for the mass production. We compared the former with the latter in terms of minerals and free amino acids. The results of this study are summarized as follows. When mineral contents were compared, the brown stock extracted by high.pressure heating extraction showed the tendency of increase in mineral contents in proportion to heating temperature and heating time, but, from extraction temperature of 140$^{\circ}C$, the contents of K, Mg, Na and P decreased with the increase of extraction time. In addition, mineral contents in the brown stock extracted by high-pressure heating extraction were generally lower than those in brown stock extracted by the traditional extraction method. This result was produced probably because materials were added repeatedly in the traditional method. Amino acids contents in brown stock according to the extraction methods were also examined. They increased with the increase in the number of extractions in the brown stock extracted by the traditional method, and those in the brown stock extracted using a high pressure heating extractor increased with the increase in heating temperature and extraction time. The results of this study are expected to be useful as a practical material for the mass production of brown stock products.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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• 2000.10a
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• pp.63-67
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• 2000

Up to this day, Most studies of hydroelasticity are inclined to frequency domain atnlysis. Thos amlysis Q the landing, take-4, and dropping of airaqft on a structure. So, the concern of this prrper is a tra a VLFS subjected to dymmic lazd induced by airplane larndirrg and take-off. To predict added mass, dampr exciting force, the source-dipole distribution method were used The responses are accomplished by Fdoimain analysis method is based on Newmark $\beta$ method to pursuit time step pnzcedure taking advantage function for hvdrodvnumic effects.

• Journal of Ocean Engineering and Technology
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• v.15 no.1
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• pp.26-30
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• 2001

Up to now, Most studies of hydroelasticity are about frequency domain analysis. Those aren't suited for analysis of the landing take-off, and dropping of aircraft on a structure. So, the concern of this paper is the transient behavior of a VLFS subjected to dynamic load, induced by airplane landing and take-off. To predict the added mass, damping coefficient, and wave exciting force, the source-dipole distribution method was used in the frequency domain. The responses are accomplished by using the FEM scheme. A time domain analysis method is based on the Newmark β method to pursue the time step procedure, taking advantage of memory effect function for hydrodynamic effects.

• Korean Journal of Food Science and Technology
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• v.41 no.6
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• pp.609-614
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• 2009

Sesame oil was sometimes replaced by mixed oil due to high price in Korean market. To find out authentic sesame oil, electronic nose (E-nose) based on mass spectrometer system was used. Sesame oil was blended with perilla oil at the ratio of 97:3, 94:6, 91:9, 88:12 and 85:15, respectively. Intensities of each fragment from sesame oil by E-nose based on MS were completely different from those of perilla oil. The obtained data was used for discriminant function analysis. For quantitative analysis, the partial least square algorithm was used. The added concentration of perilla oil to sesame oil was correlated with discriminant function first score (DF1) and second score (DF2). From this relationship it could be found out how much perilla oil added. DFA plot indicated a significant separation of pure sesame oil and pure perilla oil. The different geographical origin of sesame oil was used for blending with perilla oil were closed to that of sesame oil. Korean sesame oil mixture and Indian sesame oil one were well separated. And the correlation between mixing ratios and DF1 values was found at the ratio of 97:3, 91:9, and 85:15 (SE vs PE oil), respectively. But the added concentration of perilla oil to sesame oil was correlated with discriminant function first score (DF1). E-nose based on MS system could be used as an efficient method for purity of oil quality.