• Title/Summary/Keyword: acid strength

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Effect of temperature on the behavior of self-compacting concretes and their durability

  • Salhi, M.;Li, A.;Ghrici, M.;Bliard, C.
    • Advances in concrete construction
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    • v.7 no.4
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    • pp.277-288
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    • 2019
  • The formulation of self-compacting concretes (SCC) and the study of their properties at the laboratory level were currently well mastered. The aim of this work is to characterize SCC under hot climatic conditions and their effects on the properties of fresh and hardened SCC. Particularly, the effect of the initial wet curing time on the mechanical behavior such as the compressive strength and the durability of the SCCs (acid and sulfate attack) as well as the microstructure of SCCs mixtures. In this study, we used two types of cement, Portland cement and slag cement, three water/binder (W/B) ratio (0.32, 0.38 and 0.44) and five curing modes. The obtained results shows that the compressive strength is strongly influenced by the curing methods, 7-days of curing in the water and then followed by a maturing in a hot climate was the optimal duration for the development of a better compressive strength, regardless of the type of binder and the W/B ratio.

Initial Strength Characteristics of Cement Paste Added with Nitric Acid Neutralized Red Mud (질산 중화 레드머드를 첨가한 시멘트 페이스트의 초기강도 특성)

  • Kang, Hye Ju;Kang, Suk Pyo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2021.05a
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    • pp.70-71
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    • 2021
  • An increasing amount of red mud (RM) is being generated globally with the growth in alumi-num production. To avoid the RM becoming a pollutant, methods for effectively recycling RM at a low cost are being investigated. This study proposes a method for recycling RM as a construc-tion material. The cement paste with neutralized liquefied red mud had higher compressive strength than that of plain cement paste and cement paste with liquefied red mud without neutralization at 1 d of aging; this indicates that nitric acid neu-tralization increases the early-age strength.

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THE EFFECT OF LIGHT CURED GLASS IONOMER CEMENT ON THE SHEAR BOND STRENGTH OF ORTHODONTIC BRACKETS (광중합형 글래스 아이오노머 시멘트 교정용 브라켓의 전단결합강도에 미치는 영향)

  • Kim, Cheol;Yoon, Young-Jooh;Kim, Kwng-Won
    • The korean journal of orthodontics
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    • v.27 no.2
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    • pp.327-334
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    • 1997
  • The purpose of this study was to evaluate clinical applicability of light cured glass ionomer cement as a othodontic adhesive. The metal brackets and plastic brackets were bonded with light cured glass ionomer cement(Fuji Ortho $LS^{(R)}$) after polishing with a slurry of pumice, surface conditioning with 10% polyacrylic acid and chemically cured resin(Mono-$Lok2^{(R)}$) after acid etching with 38% phosphoric acid on the extracted human bicuspids. The shear bond strength was tested with a universal testing machine(HGS-100A, Shimadzu Co., Japan) after storage in normal saline at $37^{\circ}C$ or 24 hours and 48 hours. The results were as follows: 1. The shear bond strength of light cured glass ionomer cement group polished with a slurry of pumice was significantly lower than that of chemically cured resin group(P<0.01). 2. The shear bond strength of light cured glass ionomer cement group conditioned with 10% polyacrylic acid was significantly lower than that of chemically cured resin group(P<0.01). 3. The shear bond strength of light cued glass ionorner cement group conditioned with 10% polyacrylic acid was slightly higher than that of light cured glass ionomer cement group polished with a slurry of pumice, but there was no significant difference(P>0.05). 4. There was no significant difference between metal bracket group and plastic bracket group irrelevant off enamel conditioning(P>005). In summary, although the shear bond strength of light cured glass lionomer cement was lower than that of chemically cured resin, it night be clinically applicable.

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The Washing Finish of Blue Jeans(I) - the comparison of neutral cellulase, acid cellulase, stone, and stone-neutral cellulase washings - (청바지의 세탁가공에 관한 연구(I) -세탁가공의 종류를 중심으로-)

  • 신혜원;유효선
    • Journal of the Korean Society of Clothing and Textiles
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    • v.21 no.2
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    • pp.471-481
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    • 1997
  • Denims were treated with neutral cellulase, acid cellulase, stone, and stone-neutral cellulase respectively at different cellulase concentrations varying treatment times in rotary washer. The effect of washing on denim was estimated by the changes in weight, color, back staining, tear strength, flex stiffness, and surface characteristics. Also the comparison of neutral cellulase, acid cellulase, stone, and stone-neutral cellulase washings was studied. Washing removes surface fibers and provides weight loss, color difference, back staining, and a decrease in tear strength and in flex stiffness. Stone-neutral cellulase washing and acid cellulase washing have a larger washing effect than neutral cellulase washing and stone washing.

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Structure-Activity Relationship Study of Asiatic Acid Derivatives for New Wound Healing Agent

  • Jeong, Byeong-Seon
    • Archives of Pharmacal Research
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    • v.29 no.7
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    • pp.556-562
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    • 2006
  • Ten semi-synthetic derivatives of asiatic acid were prepared and their wound healing effects were evaluated by employing a tensile strength assay and a wound area assay. Among them, ethoxymethyl 2-oxo-3,23-isopropylidene-asiatate (12) showed the strongest and the fastest wound healing activity. Furthermore, it left the smallest scar after healing.

EFFECTS OF ACID TREATMENT OF FLUORIDE APPLIED DENTIN SURFACE ON DENTIN BONDING (불소도포한 상아질면의 산처리가 상아질접착에 미치는 영향)

  • Hwang, Hea-Kyung;Ahn, Sik-Hwan;Kim, Sung-Kyo;Jo, Kwang-Hun;Park, Jin-Hoon
    • Restorative Dentistry and Endodontics
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    • v.21 no.2
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    • pp.602-618
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    • 1996
  • The purpose of this study was to investigate the effect of acid treatment of fluoride applied dentin surface with various concentrations of phosphoric acid for various periods of time on dentin bonding. Dentin specimens prepared from freshly extracted bovine mandibular anterior teeth were divided into fluoridated and nonfluoridated groups. Specimens of nonfluoridated group were pretreated with 10% phosphoric acid for 15 seconds. Those of fluoridated groups were treated with 2% sodium fluoride or 2% stannous fluoride solution for 5 minutes and stored in $37^{\circ}C$ distilled water for 3 days, followed by phosphoric acid treatment. The concentrations of phosphoric acid were 10%, 32% or 50% and the treatment periods of time were 15, 30 or 60 seconds. All the specimens were bonded with All Bond$^{(R)}$ 2 and Bisfil$^{TM}$ composite resin. After bonded specimens were stored in $37^{\circ}C$ distilled water for 24 hours, tensile bond strengths of each specimens were measured and the pretreated dentin and the fractured dentin surfaces were examined under the scanning electron microscope. The results were as follows : The tensile bond strengths from the fluoridated groups were significantly lower than those from the nonfluoridated group when the concentrations of phosphoric acid and the treatment periods of time were equal in all the groups (p<0.05). In general, the higher the concentration of phosphoric acid and the longer the treatment period of time for acid etching on the fluoride applied dentin surface, the higher were the bond strength values. Recovery of bond strength of the dentin bonding agent was better in the NaF applied group than in the $SnF_2$ applied one. SEM findings of NaF applied and $SnF_2$ applied dentin surfaces demonstrated reaction product-covered and partially or completely obstructed dentinal tubules. SEM findings of dentin surfaces fluoridated for 5 minutes followed by etching showed wider tubular openings and more clean dentin surfaces when dentin was etched with higher concentration of phosphoric acid for longer period of time. On the SEM observations of the fractured dentin-resin interface, the etched specimens of fluoridated group showed an adhesive failure mode when the concentration of phosphoric acid and the treatment period of time were same as in the nonfluoridated group. As the concentration of phosphoric acid and the treatment period of time increase during acid etching, the cohesive failure area increased. However, excessive acid etching caused adhesive failure.

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A Study on Concentration and Application Time of Lithium Sulfate-Contained Polyacrylic Acid for Adequate Crystal Growth (법랑질 표면에 크리스탈을 형성시키기 위해 사용한 황산리튬이 함유된 폴리아크릴산의 농도와 적용시간에 관한 연구)

  • Roh, Joung-Sub;Kim, Sang-Cheol;Tae, Ki-Chul
    • The korean journal of orthodontics
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    • v.28 no.6 s.71
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    • pp.947-954
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    • 1998
  • The purpose of this study was to compare shear bonding strengths and debonding patterns of the ceramic brackets attached on the crystal which were grown on the enamel surface of a tooth with different concentrations of lithium sulphate-contained polyacrylic acid in different application times. Four kinds of concentrations of mixed solutions were made and applied to the enamel surface on extracted human premolars. The solutions were made by adding 0.3M or 0.6M of lithium sulfate to $50\%\;or\;65\%$ of polyacrylic acid with 0.3M sulfuric acid. The solutions were applied for 30 or 60 seconds. After bonding, a universal testing machine was used to measure the shear bond strength, and then observations were made of debonding patterns through the stereoscope. And the enamel surface was observed through the scanning electron microscope to examine the pattern of crystal growth and debonding. The results were as follows: 1. Shear bond strength in the enamel surface treated with $50\%$ polyacrylic acid was higher than that with $65\%$ polyacrylic acid. 2. There were no statistical differences in shear bond strength according to concentration of lithium sulfate and application time of solutions . 3. Enamel surface was almost free of resin debris after debonding. 4. Enamel surface treated with $50\%$ polyacrylic acid showed higher density of crystal growth than that with $65\%$ polyacrylic acid under scanning electron microscope.

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A Study on the Improvement of Interfacial Bonding Shear Strength of Ti50-Ni50 Shape Memory Alloy Composite (Ti_{50}-Ni_{50} 형상기억합금 복합체의 계면 접학 전단강도 향상에 관한 연구)

  • Lee, Hyo-Jae;Hwang, Jae-Seok
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.10 s.181
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    • pp.2461-2468
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    • 2000
  • In this paper, single fiber pull-out test is used to measure the interfacial bonding shear strength of $Ti_{50}-Ni_{50}$ shape memory alloy composite with temperature. Fiber and matrix of $Ti_{50}-Ni_{50}$ shape memory alloy composite are respectively $Ti_{50}-Ni_{50}$ shape memory alloy and epoxy resin. To strengthen the interfacial bonding shear stress, various surface treatments are used. They are the hand-sanded surface treatment, the acid etched surface treatment and the silane coupled surface treatment etc.. The interfacial bonding shear strength of surface treated shape memory alloy fiber is greater than that of surface untreated shape memory alloy fiber by from 10% to 16%. It is assured that the hand-sanded surface treatment and the acid etched surface treatment are the best way to strengthen the interfacial bonding shear strength of $Ti_{50}-Ni_{50}$ shape memory composite. The best treatment condition of surface is 10% HNO$_3$ solution in the etching method to strengthen the interfacial bonding shear strength of $Ti_{50}-Ni_{50}$ shape memory alloy composite.