• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.200.2-200.2
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• 2016

Carbon-based materials have been known as ablative material and have been used for thermal protection systems. Ablation is an erosive phenomenon that results in thermochemical and thermomechanical changes on materials. Ablation resistance is one of the key properties that determines performance and life-time of the thermal protection material under ablative conditions. In this study, ablation properties of graphite, 3-dimensional (C/C) composites (needle-punched type and rod type) were investigated byusing a plasma wind tunnel which produce a supersonic plasma flow from a segmented arc heater with the power level of 0.4 MW. The mass losses and surface roughness changes which contain main result of the ablation are measured. A morphological analysis ofthe carbon-based materials, before and after the ablation test, are performed through field emission scanning electron microscopy (FE-SEM) and non-contact 3D surface measuring system. Electronic balance and a portable surface roughness tester were used for evaluation of the recession and mass loss of the test samples.

• Carbon letters
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• v.9 no.4
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• pp.316-323
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• 2008

The factors that influence ablation resistance in fiber composites are properties of the reinforced fiber and matrix, plugging quantity of fiber, geometrical arrangement, crack, pore size, and their distributions. To examine ablation resistance according to distribution of crack and pore size that exist in carbon/carbon composites, this study produced various sizes of unit cells of preforms. They were densified using high pressure impregnation and carbonization process. Reinforced fiber is PAN based carbon fiber and composites were heat-treated up to $2800^{\circ}C$. The finally acquired density of carbon/carbon composites reached more than $1.932\;g/cm^3$. The ablation test was performed by a solid propellant rocket engine. The erosion rate of samples is below 0.0286 mm/s. In conclusion, in terms of ablation properties, the higher degree of graphitization is, the more fibers that are arranged vertically to the direction of combustion flame are, and the less interface between reinforced fiber bundle and matrix is, the better ablation resistance is shown.

• Carbon letters
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• v.2 no.1
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• pp.27-36
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• 2001

The pack-cementation process is the method which is formed SiC coating layer to improve weak oxidation properties of CFRCs (carbon fiber-reinforced carbons). This method develops the anti-oxidation coating layer having no dimensional changes and good wetting properties. In this study to improve the oxidative resistance of the prepared 4D CFRCs, the surface of CFRCs is coated by SiC using pack cementation method. The mechanical properties of SiC-coated 4D CFRCs are measured by the 3-point bending test, and their ablation properties are investigated by the arc torch plasma test. From the results, it is found that both mechanical and ablation properties of SiC-coated 4D CFRCs are much better than bare CFRCs.

• Proceedings of the Korean Magnestics Society Conference
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• 1993.11a
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• pp.58-59
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• 1993

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.47 no.9
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• pp.642-648
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• 2019

In this study, Image-based computational analysis using the developed models was performed to predict the degradation of effective properties by ablation. The ablation tests of carbon/phenolic composites were performed using a 0.4 MW arc-heated wind tunnel. The carbon/phenolic composite samples were scanned using the micro-computed tomography (Micro-CT) to analyze the ablation characteristics according to a duration time of the ablation test. By calibrating the scanned images, computational models were developed that reflect the actual microstructure of the ablation composites. Also, nine computational models that reflect the actual pore shape were developed using the created cross-sectional images. Image-based computational analysis using the developed models was performed to predict the degradation of effective properties by ablation and the decrease of effective properties was confirmed with increase of porosity.

• Korean Journal of Radiology
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• v.23 no.1
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• pp.42-51
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• 2022

Objective: This study aimed to investigate the direction of tissue contraction after microwave ablation in ex vivo bovine liver models. Materials and Methods: Ablation procedures were conducted in a total of 90 sites in ex vivo bovine liver models, including the surface (n = 60) and parenchyma (n = 30), to examine the direction of contraction of the tissue in the peripheral and central regions from the microwave antenna. Three commercially available 2.45-GHz microwave systems (Emprint, Neuwave, and Surblate) were used. For surface ablation, the lengths of two overlapped square markers were measured after 2.5- and 5-minutes ablations (n = 10 ablations for each system for each ablation time). For parenchyma ablation, seven predetermined distances between the markers were measured on the cutting plane after 5- and 10-minutes ablations (n = 5 ablations for each system for each ablation time). The contraction in the radial and longitudinal directions and the sphericity index (SI) of the ablation zones were compared between the three systems using analysis of variance. Results: In the surface ablation experiment, the mean longitudinal contraction ratio and SI from a 5-minutes ablation using the Emprint, Neuwave, and Surblate systems were 28.92% and 1.04, 20.10% and 0.53, and 24.90% and 0.45, respectively (p < 0.001). A positive correlation between longitudinal contraction and SI was noted, and a similar radial contraction was observed. In the parenchyma ablation experiment, the mean longitudinal contraction ratio and SI from a 10-minutes ablation using the three pieces of equipment were 38.60% and 1.06, 32.45% and 0.61, and 28.50% and 0.50, respectively (p < 0.001). There was a significant difference in the longitudinal contraction properties, whereas there was no significant difference in the radial contraction properties. Conclusion: The degree of longitudinal contraction showed significant differences depending on the microwave ablation equipment, which may affect the SI of the ablation zone.

• Journal of Photoscience
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• v.6 no.3
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• pp.103-108
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• 1999

We present recent results on ablation mechanism, single-pulse laser micropatterning , pulsed-laser deposition(PLD) and particulates formation accompanying laser ablation, with special emplasis on polymers, in particular polymide, (PI), and polytetrafluoroethylene, (PTFE). Ablation of polymers is described on the basis of photothermal bond breaking within the bulk material. Here, we assume a first order chemical reaction, which can be described by an Arrhenius law. Ablation starts when the density of broken bonds at the surface reaches a certain critical value. Single-pulse laser ablation of polyimide shows a clear-length dependence of the threshold fluence. This experimental result strongly supports a thermal ablation model. We discuss the various possibilities and drawbacks of PLD and describe the morphology, physical properties and applications of PTFE films.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.15 no.7
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• pp.634-639
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• 2002

Using laser ablation technique carbon thin films were deposited on Si(100) substrate as a function of substrate temperature. In this study, the surface morphologic, structural and field emission properties of these carbon thin films were investigated using Raman spectroscopy, scanning electron microscopy, and a diode technique, respectively. With increasing of the substrate temperature, the surface morphologies were changed significantly. Moreover, the intensity of D-band and the full width at half maximum of these bands were dependent on substrate temperatures. As the substrate temperature was increased, the field emission properties were improved. As the result, we find that the field emission properties of the films were changed significantly with the substrate temperature and structural features of carbon than films.

• Proceedings of the Korean Magnestics Society Conference
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• 1997.11a
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• pp.64-65
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• 1997

• Proceedings of the Korean Magnestics Society Conference
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• 1995.05a
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• pp.62-63
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• 1995