• 제목/요약/키워드: YBCO film

검색결과 304건 처리시간 0.024초

비냉각형 적외선 센서로 응용하기 위한 반도성 YBa2Cu3O6+x 박막의 열처리 온도에 따른 구조적 전기적 특성 (Structural and Electrical Properties of Semiconducting YBCO Thin Film Annealed at Various Temperatures for Uncooled Infrared Sensor Application)

  • 이태호;이성갑;여진호;정혜린
    • 한국전기전자재료학회논문지
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    • 제26권10호
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    • pp.731-735
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    • 2013
  • YBCO thin films on $SiO_2$/Si substrate were fabricated by spin-coaing of an alkoxide-derived precursor and heat treatment. The structural and electrical properties of the YBCO films were investigated as functions of annealing temperature at $600{\sim}800^{\circ}C$. Although YBCO single phase was not synthesized, dense films of YBCO matrix phase and minor second phases have been successfully fabricated at the annealing temperatures of $650{\sim}800^{\circ}C$. Thickness and temperature coefficient of resistance (TCR) of YBCO thin films with annealing temperature of $750^{\circ}C$ were 0.31 ${\mu}m$ and $-2.92%/^{\circ}C$, respectively.

Quench Characteristics of YBCO Film for Current Limiting Using Magnetic Field

  • 박권배;최효상;김혜림;현옥배;황시돌
    • Progress in Superconductivity
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    • 제3권2호
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    • pp.252-256
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    • 2002
  • We studied YBCO films for current limiting of the resistive type which utilizes a transition from superconducting to normal state caused by exceeding critical current. The films were deposited on sapphire substrates and covered by gold top layer. The current limiting element consists of 2 mm wide YBCO stripes connected in series. A serious problem in using YBCO films for current limiting is inhomogeneities caused by imperfect manufacturing. Therefore simultaneous quench is a difficult problem when elements for current limiting are connected in series. So some researchers have recently proposed using magnetic field and heating for simultaneous quench. We have measured extended exec trim field-current density(E-J) characteristics for current limiting elements of YBCO films in applied magnetic field of 0 - 130 mT. And we have investigated quench characteristics in current limiting elements and between elements of YBCO films in applied magnetic field. The result of the experiments show that the presence of applied magnetic fields induces uniform quench distribution fur the stripes in element at $50V_{rms}$, otherwise non-uniform quenches were observed. And simultaneous quenches between elements were investigated at $150V_{rms}$. We suggest that suppressing the critical current by increased fields due to fault current effectively forced the stripes of higher $J_{c}$(0) to quench, resulting in equalizing quench times.s.s.s.

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Modified melt-textured growth 법으로 제작한 타겟을 사용한 YBCO 박막의 펄스레이저 증착 (Pulsed laser deposition of YBCO thin films using modified melt-textured grown targets)

  • 김창훈;김인태;홍국선;김영환;최상삼;한택상
    • 한국초전도학회:학술대회논문집
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    • 한국초전도학회 1999년도 High Temperature Superconductivity Vol.IX
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    • pp.115-119
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    • 1999
  • Ba$_2Cu_3O_{7-{\delta}}$ (YBCO) thin films were deposited by pulsed laser deposition using differently prepared targets: One was a conventionally solid-state sintered (SSS) target and the other was a modified melt-textured grown (MTC) target. Compared with SSS targets, MTG targets showed a well-connected microstructure consisting of much larger grains and the surface was Bess roughened with the cumulative laser incidence. YBCO films deposited from MTC targets showed a denser and smoother surface of the basal film than the case of SSS targets. The investigations of ${\alpha}$-axis outgrowths in the films indicated that the deposition using MTG targets would result in a more homogeneous and stable film growth as compared to the SSS targets. Also, TEM analysis revealed that the film deposited from MTG targets had a less granular microstructure that would reduce weak-link effects in the film.

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DCA-MOD 방법으로 제조된 YBCO 박막의 미세조직에 미치는 열처리 효과 (Effects of Heat Treatments on the Microstructure of YBCO Films Prepared by DCA-MOD Method)

  • 김병주;김혜진;조한우;유석구;유정희;이희균;홍계원
    • Progress in Superconductivity
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    • 제9권1호
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    • pp.96-101
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    • 2007
  • [ $YBa_2Cu_3O_{7-{\delta}}$ ] films have been prepared on $LaAlO_3$ (100) single-crystal substrates by a metalorganic deposition using dichloroacetate precursors (DCA-MOD). Calcination conditions were varied in order to optimize the microstructure and the superconducting properties of YBCO film. Coated films were calcined at various temperatures ranging from $400{\sim}700^{\circ}C$ in flowing humid oxygen atmosphere. Ramping rate to calcination tempertures was $2.22^{\circ}C/min$. Conversion heat treatment was performed at $800^{\circ}C$ for 2 h in flowing Ar gas containing 1000 ppm oxygen with a humidity of 9.45%. Observations of surface and cross sectional SEM microstructure showed that the particle size in the calcined film increased in the range of 100-200 nm with heating rate and the calcination temperature. SEM EDS analysis showed that 13 a/o of chlorine was contained in the calcined film. It was also observed that the porosity increased with the heating rate and temperature. Porous microstructure was developed when YBCO films were prepared using porous calcined film. Dense microstructure and high $J_c$ over $1\;MA/cm^2$ was obtained when calcination was carried out at the temperature of $500^{\circ}C$ with a heating rate of $2.22^{\circ}C/min$.

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마이크로파 공진기를 이용한 YBCO 박막 두께의 비파괴적 측정: 캘리브레이션 박막 두께의 불확도의 역할 (Non-invasive Measurements of the Thickness of YBCO Thin Films by Using Microwave Resonators: Roles of the Uncertainty in the Calibration Film Thickness)

  • 김명수;정호상;양우일;이상영
    • Progress in Superconductivity
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    • 제14권1호
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    • pp.45-51
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    • 2012
  • 마이크로파 측정법으로 ~40 GHz의 공진주파수를 지닌 공진기를 이용하여 비파괴적으로 YBCO 초전도체 박막의 두께를 측정할 경우 calibration용 YBCO 박막의 두께의 불확도가 마이크로파로 측정된 두께의 불확도에 미치는 영향을 70 - 360 nm 두께를 지닌 5 개의 YBCO 박막에 대해 연구하였다. Calibration용 박막으로는 약 150 nm의 두께를 지닌 박막이 사용되었는데, 이 박막의 두께의 불확도는 박막 표면의 거칠기를 고려하여 결정하였다. 본 연구 결과, calibration용 박막의 불확도가 마이크로파로 측정된 박막의 두께에 상당한 영향을 준다는 것을 확인하였으며, ~ 40 GHz에서 연구에 사용된 모든 박막에 대해 측정 두께가 5% 이내의 상대 불확도를 지니기 위해서는 calibration용 박막의 두께의 상대 표준불확도가 2.7% 이내의 값을 가져야 함을 알 수 있었다. 본 연구 결과는 마이크로파를 이용하여 박막의 두께를 측정할 경우 측정 두께의 상대 불확도의 목표치를 구현하기 위해서는 표면 거칠기로 인한 두께의 불확도가 일정 값 이하인 박막 만이 calibration용 박막으로 사용될 수 있음을 보여준다.

나노분말 첨가에 따른 YBCO 초전도 박막의 미셀구조 및 초전도 특성변화 연구 (Effect of nano-sized powder addition on the microstructure and superconducting properties of the YBCO thin film.)

  • 박진아;김병주;임선원;안지현;김호진;홍계원;이희균
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2005년도 제36회 하계학술대회 논문집 C
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    • pp.1998-2000
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    • 2005
  • The effects of the addition of nanocrystalline Y2O3 powder on the microstructure and superconducting properties have been investigated in YBCO films prepared by TFA-MOD process. Precursor solution doped with extra $Y_2O_3$ Powder was prepared by adding $Y_2O_3$ powder into a stoichiometic precursor solution with a cation ratio of Y:Ba:Cu=1:2:3. Coating solutions with and without $Y_2O_3$ doping were coated on $LaAlO_3(100)$ single crystal by a dip coating method, cacination and conversion heat treatments were performed at the controlled atmosphere containing water vapor Current carry capacity(Jc) of YBCO film was enhanced about 50% by $Y_2O_3$ doping. It is thought that the enhancement of Jc is due to the better connectivity of YBCO grains and/or the flux pinning by the presence of nanocrystalline $Y_2O_3$ Particles embedded in YBCO grains.

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세라믹 분말재료의 EPD 후막형성 기술 (EPD Thick Film Formation of Ceramic Powder Materials)

  • 소대화;전용우
    • 동굴
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    • 제75호
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    • pp.49-54
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    • 2006
  • Electrophoretic Deposition (EPD) is the most convenient technology to deposit natural or oxide powders of nonconductive materials in alcoholic suspension solution with adding electrolyte of iodine to form ceramic thick film on metal substrate under applied electric field with double electric layer between electrode and metal substrate. In this research work, the important parameters and technical ways were studied to form EPD thick films of typical oxide ceramics of Al2O3, YBCO and tourmaline powders.

레이저 증착법을 이용한 금속기판상 고온초전도 박막증착 및 특성분석 (Fabrication and Characterization of High Temperature Superconducting Thin Film on Metallic Substrate Using Laser Ablation)

  • 이상렬
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1995년도 추계학술대회 논문집 학회본부
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    • pp.329-331
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    • 1995
  • Laser ablation was used to fabricate superconducting $YBa_2Cu_3O_{7-x}$ (YBCO) thin films on metallic substrates with an YSZ buffer layer. An ArF excimer laser with an wavelength of 193 nm was used to deposit both YSZ buffer layer and superconducting thin film. The characterizations of thin films were performed and compared. With a 200 nm YSZ buffer layer, c-axis orientation and $T_c$=85 K were obtained for a 200 nm-thick YBCO film.

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