• Title/Summary/Keyword: Xray Analysis

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Study on Nondestructive Analysis Techniques for Semiconductor Chips in Communication Device Development

  • Yongho Choi
    • International Journal of Internet, Broadcasting and Communication
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    • v.16 no.4
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    • pp.265-272
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    • 2024
  • Semiconductors are crucial components in communication technology, playing important roles in various communication systems. They are essential for signal processing, data transmission, and ensuring the stability of communication networks. In particular, high-performance semiconductor chipsets and processors enable ultra-fast data transmission and ultra-low latency in communication technology. For example, semiconductors are indispensable in smartphones, wireless networks, and satellite communication systems. For semiconductor packaging products, nondestructive internal analysis for defect analysis and process improvement without causing deformation of system packaging is an important part of the product development process. In this study, nondestructive analysis techniques using X-ray equipment are discussed. The results of this study can provide fast and accurate nondestructive analysis of semiconductor packaging products and can play a significant role in supporting the growth of the communication industry.

X-RAY SOURCES WITH NO COUNTERPARTS IN OTHER WAVELENGTH BANDS

  • Kim, Chulhee;Moon, Byung-Kwon;Park, Hong Soo
    • Journal of The Korean Astronomical Society
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    • v.47 no.5
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    • pp.163-166
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    • 2014
  • In order to identify peculiar X-ray sources, we select 442 sources with no counterparts in other wavelength bands (as of the year 1999) from the ROSAT All-Sky Survey Bright Source Catalog. We cross-correlate this initial list with the NASA/IPAC Extragalactic Database, the USNO and WISE catalogs, and the HEASARC XRAY Master Catalog. Eventually, we are left with four unidentified sources with no counterparts in other wavelength bands. We present these four sources and their X-ray properties in this paper.

Application of X-ray Absorption Spectroscopy (XAS) in the Field of Stabilization of As and Heavy Metal Contaminated Soil (비소 및 중금속 오염토양 안정화 분야에서의 X선 흡수분광법(XAS) 활용)

  • Lim, Jung Eun;Moon, Deok Hyun;Kim, Kwon-Rae;Ok, Yong Sik
    • Journal of Applied Biological Chemistry
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    • v.58 no.1
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    • pp.65-74
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    • 2015
  • X-ray absorption fine structure (XAFS) analysis using X-ray absorption spectroscopy is being applied as a state-of-the-art method in a wide range of disciplines. This review article summarizes the overall procedure of XAFS analysis from the preparation of soil samples to the analysis of data in X-ray absorption near edge structure (XANES) region and extended Xray absorption fine structure (EXAFS) region. The previous studies on application of XANES and EXAFS techniques in environmental soil science field are discussed and classified them according to metal(loid)s (As, Cd, Cu, Ni, Pb, and Zn). A significant number of previous studies of XAFS application in the environmental soil science field have focused on the identification of Pb chemical species in soil. Moreover, XANES and EXAFS techniques have been widely used to investigate the contamination source via identification of metal species. Similarly, these techniques were applied to identify the mechanisms of metal stabilization in soil after application of various amendments, phytoremediation, etc.

Crystal Structures and Thermal Properties of Two Binuclear Cd(II) Supramolecular Complexes Based on Quinolinecarboxylate Ligand

  • Hao, Hu-Jun;Yin, Xian-Hong;Lin, Cui-Wu;Wei, Shui-Qiang
    • Bulletin of the Korean Chemical Society
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    • v.32 no.9
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    • pp.3255-3260
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    • 2011
  • Two novel binuclear metal-organic coordination complexes $[Cd_2(L)_2(bpy)_2(H_2O)_2]{\cdot}6H_2O$ (1), $[Cd_2(L)_2(phen)_2-(H_2O)_2]{\cdot}2H_2O$ (2) (where L = 2-methylquinoline-3,4-dicarboxylate dianion, bpy = 2,2'-bipyridine, phen = 1,10-phenanthroline) have been synthesized under hydrothermal conditions and characterized by single crystal Xray diffraction, spectral method (IR), elemental analysis and thermal gravimetric analysis (TGA). Both 1 and 2 consist of two Cd(II) atoms bridged by two monoatomic bridging carboxylate groups from two L ligands, and the second carboxylate group of each L is monodentately coordinated to Cd(II), creating a sevenmembered chelating ring. The coordination at each metal nucleus is completed by a water molecule and a chelating bidentate molecule. The 3D structures of the complexes are stabilized by ${\pi}-{\pi}$ stacking interactions and hydrogen-bonds.

Study about sacral base X-ray of Barge (Barge의 천골 기저부 X-ray에 대한 연구)

  • Min, Young-Kwang
    • The Journal of Churna Manual Medicine for Spine and Nerves
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    • v.6 no.1
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    • pp.19-26
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    • 2011
  • Objectives : The purpose of this study is to research the necessity of sacral base X-ray that Barge insisted. Methods : I have done a comparative analysis in side of short leg and side of sacral inferior with sacral base X-ray and pelvis A-P Xray pictures of 42 patients with lower back pain from December 1, 2010 to March 31, 2011. Results : Even though most of the subjects in study were male, 36 people had plateau of sacral base and 29 people had symmetry in sacral base X-ray. There was no statistical significance in the side of short leg and side of sacral base inferior in Sacral base X-ray, but there was a statistical significance in pelvis A-P x-ray. 22 people had same side of short leg and side of sacral base inferior in sacral base X-ray and pelvis A-P X-ray and 14 people didn't. 29 people had same side of sacral base inferior in sacral base X-ray and pelvis A-P X-ray and 13 people didn't. Conclusions : According to the result of the study, sacral base X-ray is necessary for correct sacral base inferior analysis.

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Preparation and Cyclic Performance of Li1.2(Fe0.16Mn0.32Ni0.32)O2 Layered Cathode Material by the Mixed Hydroxide Method

  • Karthikeyan, K.;Nam, K.W.;Hu, E.Y.;Yang, X.Q.;Lee, Y.S.
    • Bulletin of the Korean Chemical Society
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    • v.34 no.7
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    • pp.1995-2000
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    • 2013
  • Layered $Li_{1.2}(Fe_{0.16}Mn_{0.32}Ni_{0.32})O_2$ was prepared by the mixed hydroxide method at various temperatures. Xray diffraction (XRD) pattern shows that this material has a ${\alpha}-NaFeO_2$ layered structure with $R{\bar{3}}m$ space group and that cation mixing is reduced with increasing synthesis temperature. Scanning electron microscopy (SEM) reveals that nano-sized $Li_{1.2}(Fe_{0.16}Mn_{0.32}Ni_{0.32})O_2$ powder has uniform particle size distribution. X-ray absorption near edge structure (XANES) analysis is used to study the local electronic structure changes around the Mn, Fe, and Ni atoms in this material. The sample prepared at $700^{\circ}C$ delivers the highest discharge capacity of 207 $mAhg^{-1}$ between 2-4.5 V at 0.1 $mAcm^{-2}$ with good capacity retention of 80% after 20 cycles.

Generation of Silver Nanoparticles by Spark Discharge Aerosol Generator Using Air as a Carrier Gas (공기 분위기에서 스파크 방전을 이용한 은 나노입자 생성)

  • Oh, Hyun-Cheol;Jung, Jae-Hee;Park, Hyung-Ho;Ji, Jun-Ho;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.30 no.2 s.245
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    • pp.170-176
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    • 2006
  • A spark discharge aerosol generator using air as a carrier gas has successfully been applied to silver nanoparticle production. The spark discharge between two silver electrodes, which was periodically obtained by discharging the capacitor, produced sufficient high temperatures to evaporate a small fraction of the silver electrodes. The silver vapor was subsequently supersaturated by rapid cooling and condensed to silver nanoparticles by nucleation and condensation. The morphology of the generated particles observed by transmission electron microscope was spherical. The element composition of the nanoparticles was silver, which was determined by energy dispersive X-ray spectroscopy. The crystal phase of the particles spark-generated under air atmosphere was composed of silver and silver oxides phase, which was determined by Xray diffraction analysis. While the nanoparticles generated under nitrogen atmosphere had only silver phase. This XRD data indicates that some fraction of the evaporated silver vapor could be oxidized in air atmosphere by the reaction with oxygen. A stable operation of the spark discharge generator has been achieved. The size and concentration of the particles can be easily controlled by altering the repetition frequency, capacitance, gap distance and flow rate of the spark discharge system.

A Precipitation Behavior of Nano-Oxide Particles in Mechanically Alloyed Fe-5Y2O3 Powders (기계적 합금화하여 제조한 Fe-5Y2O3 합금분말의 나노산화물 석출거동)

  • Kim, Ga Eon;Noh, Sanghoon;Choi, Ji Eun;Kim, Young Do;Kim, Tae Kyu
    • Journal of Powder Materials
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    • v.22 no.1
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    • pp.46-51
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    • 2015
  • A precipitation behavior of nano-oxide particle in Fe-$5Y_2O_3$ alloy powders is studied. The mechanically alloyed Fe-$5Y_2O_3$ powders are pressed at $750^{\circ}C$ for 1h, $850^{\circ}C$ for 1h and $1150^{\circ}C$ for 1h, respectively. The results of Xray diffraction pattern analysis indicate that the $Y_2O_3$ diffraction peak disappear after mechanically alloying process, but $Y_2O_3$ and $YFe_2O_4$ complex oxide precipitates peak are observed in the powders pressed at $1150^{\circ}C$. The differential scanning calorimetry study results reveal that the formation of precipitates occur at around $1054^{\circ}C$. Based on the transmission electron microscopy analysis result, the oxide particles with a composition of Y-Fe-O are found in the Fe-$5Y_2O_3$ alloy powders pressed at 1150oC. It is thus conclude that the mechanically alloyed Fe-$5Y_2O_3$ powders have no precipitates and the oxide particles in the powders are formed by a high temperature heat-treatment.

Catalytic Mechanism for Growth of Carbon Nanotubes under CO-H2 Gas Mixture

  • Chung, Uoo-Chang;Kim, Yong-Hwan;Lee, Deok-Bo;Jeong, Yeon-Uk;Chung, Won-Sub;Cho, Young-Rae;Park, Ik-Min
    • Bulletin of the Korean Chemical Society
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    • v.26 no.1
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    • pp.103-106
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    • 2005
  • In order to investigate the catalytic mechanism for the growth of carbon nanotubes (CNTs), a comprehensive study was conducted using carbon materials synthesized at 680 ${^{\circ}C}$ with a gas mixture of CO-H$_2$ after reduction at 800 ${^{\circ}C}$ by H$_2$ gas from iron oxide, and metal Pt. The resulting material was observed by scanning electron microscopy (SEM) and X-ray diffraction patterns (XRD) after a variety of reaction times. The carbon materials synthesized by metal Pt were little affected by reaction time and the sintered particles did not form CNTs. Xray analysis revealed that metal Fe was completely converted to iron carbide (Fe$_3$C) without Fe peaks in the early stage. After 5 min, iron carbide (Fe$_3$C) and carbon (C) phases were observed at the beginning of CNTs growth. It was found that the intensity of the carbon(C) peak gradually increased with the continuous growth of CNTs as reaction time increases. It was also found that the catalyst of growth of CNTs was metal carbide.

A Study on the MOCVD $PbTiO_3$ Thin Films (MOCVD $PbTiO_3$ 박막의 특성에 관한 연구)

  • 송한상;최두진;유광수;정형진;김창은
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.2 no.2
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    • pp.40-52
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    • 1992
  • $PbTi0_3$ thin films were deposited at $550^{\circ}C$ by MOCVD method using titanium-iso-propoxide [$Ti(OC_3H_7)_4$] and tetra-ethyl-lead $[Pb(C_2H_5)_4]$as starting materials. In the present study, Ar and $O_2$were used as a carrier gas and a reaction gas, respectively, and the change of thickness and refractive index, Xray diffraction analysis, and CV characteristic measurements of the films were systematically investigated. As a result of CV characteristic analysis of the annealed $PbTiO_3$ thin films, it is assumed that the films interact with Si substrate at the interface, and X-ray diffraction patterns of the films show characteristic peaks for $PbTiO_3$ With increasing the annealing temperature and time, the thickness of the films tends to decrease but their refractive index increases.

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