• 제목/요약/키워드: Xray Analysis

검색결과 18건 처리시간 0.018초

Study on Nondestructive Analysis Techniques for Semiconductor Chips in Communication Device Development

  • Yongho Choi
    • International Journal of Internet, Broadcasting and Communication
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    • 제16권4호
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    • pp.265-272
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    • 2024
  • Semiconductors are crucial components in communication technology, playing important roles in various communication systems. They are essential for signal processing, data transmission, and ensuring the stability of communication networks. In particular, high-performance semiconductor chipsets and processors enable ultra-fast data transmission and ultra-low latency in communication technology. For example, semiconductors are indispensable in smartphones, wireless networks, and satellite communication systems. For semiconductor packaging products, nondestructive internal analysis for defect analysis and process improvement without causing deformation of system packaging is an important part of the product development process. In this study, nondestructive analysis techniques using X-ray equipment are discussed. The results of this study can provide fast and accurate nondestructive analysis of semiconductor packaging products and can play a significant role in supporting the growth of the communication industry.

X-RAY SOURCES WITH NO COUNTERPARTS IN OTHER WAVELENGTH BANDS

  • Kim, Chulhee;Moon, Byung-Kwon;Park, Hong Soo
    • 천문학회지
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    • 제47권5호
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    • pp.163-166
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    • 2014
  • In order to identify peculiar X-ray sources, we select 442 sources with no counterparts in other wavelength bands (as of the year 1999) from the ROSAT All-Sky Survey Bright Source Catalog. We cross-correlate this initial list with the NASA/IPAC Extragalactic Database, the USNO and WISE catalogs, and the HEASARC XRAY Master Catalog. Eventually, we are left with four unidentified sources with no counterparts in other wavelength bands. We present these four sources and their X-ray properties in this paper.

비소 및 중금속 오염토양 안정화 분야에서의 X선 흡수분광법(XAS) 활용 (Application of X-ray Absorption Spectroscopy (XAS) in the Field of Stabilization of As and Heavy Metal Contaminated Soil)

  • 임정은;문덕현;김권래;옥용식
    • Journal of Applied Biological Chemistry
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    • 제58권1호
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    • pp.65-74
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    • 2015
  • X선 흡수분광법(X-ray absorption spectroscopy, XAS)을 이용하는 X선 흡수미세구조(X-ray absorption fine structure, XAFS)의 분석은 다양한 학문분야에서 적용되고 있다. 본 연구에서는 XAFS 분석을 위한 토양 시료의 준비에서부터 XAFS 측정 후 X선 흡수 끝머리 부근 미세구조(X-ray absorption near edge structure, XANES) 및 광범위 X선 흡수 미세구조(extended Xray absorption fine structure, EXAFS) 데이터를 추출하여 연구에 활용하는 것에 대해 간략하게 소개하였다. 특히 토양환경 분야에서 XANES 및 EXAFS 분석을 활용한 선행연구들에 대해 비소(As) 및 중금속 주요 원소(Cd, Cu, Ni, Pb, Zn)별로 그 내용을 정리하였다. 토양환경 분야에서 XAFS의 응용은 납(Pb)의 화학종 규명에 관한 연구가 가장 많은 것으로 나타났다. 이와 함께 대부분의 연구들은 오염토양 내 중금속 화학종의 규명을 통해 중금속의 유입 원인 등에 대해 기술하고 있으며, 이를 정화하기 위한 다양한 방법들(개량제 처리, 식물정화)을 적용한 후, 안정화된 중금속 화학종을 XANES 및 EXAFS 분석을 통해 규명하여 정화 방법들의 효율성과 안정성에 대해 보고하였다.

Crystal Structures and Thermal Properties of Two Binuclear Cd(II) Supramolecular Complexes Based on Quinolinecarboxylate Ligand

  • Hao, Hu-Jun;Yin, Xian-Hong;Lin, Cui-Wu;Wei, Shui-Qiang
    • Bulletin of the Korean Chemical Society
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    • 제32권9호
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    • pp.3255-3260
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    • 2011
  • Two novel binuclear metal-organic coordination complexes $[Cd_2(L)_2(bpy)_2(H_2O)_2]{\cdot}6H_2O$ (1), $[Cd_2(L)_2(phen)_2-(H_2O)_2]{\cdot}2H_2O$ (2) (where L = 2-methylquinoline-3,4-dicarboxylate dianion, bpy = 2,2'-bipyridine, phen = 1,10-phenanthroline) have been synthesized under hydrothermal conditions and characterized by single crystal Xray diffraction, spectral method (IR), elemental analysis and thermal gravimetric analysis (TGA). Both 1 and 2 consist of two Cd(II) atoms bridged by two monoatomic bridging carboxylate groups from two L ligands, and the second carboxylate group of each L is monodentately coordinated to Cd(II), creating a sevenmembered chelating ring. The coordination at each metal nucleus is completed by a water molecule and a chelating bidentate molecule. The 3D structures of the complexes are stabilized by ${\pi}-{\pi}$ stacking interactions and hydrogen-bonds.

Barge의 천골 기저부 X-ray에 대한 연구 (Study about sacral base X-ray of Barge)

  • 민영광
    • 척추신경추나의학회지
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    • 제6권1호
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    • pp.19-26
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    • 2011
  • Objectives : The purpose of this study is to research the necessity of sacral base X-ray that Barge insisted. Methods : I have done a comparative analysis in side of short leg and side of sacral inferior with sacral base X-ray and pelvis A-P Xray pictures of 42 patients with lower back pain from December 1, 2010 to March 31, 2011. Results : Even though most of the subjects in study were male, 36 people had plateau of sacral base and 29 people had symmetry in sacral base X-ray. There was no statistical significance in the side of short leg and side of sacral base inferior in Sacral base X-ray, but there was a statistical significance in pelvis A-P x-ray. 22 people had same side of short leg and side of sacral base inferior in sacral base X-ray and pelvis A-P X-ray and 14 people didn't. 29 people had same side of sacral base inferior in sacral base X-ray and pelvis A-P X-ray and 13 people didn't. Conclusions : According to the result of the study, sacral base X-ray is necessary for correct sacral base inferior analysis.

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Preparation and Cyclic Performance of Li1.2(Fe0.16Mn0.32Ni0.32)O2 Layered Cathode Material by the Mixed Hydroxide Method

  • Karthikeyan, K.;Nam, K.W.;Hu, E.Y.;Yang, X.Q.;Lee, Y.S.
    • Bulletin of the Korean Chemical Society
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    • 제34권7호
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    • pp.1995-2000
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    • 2013
  • Layered $Li_{1.2}(Fe_{0.16}Mn_{0.32}Ni_{0.32})O_2$ was prepared by the mixed hydroxide method at various temperatures. Xray diffraction (XRD) pattern shows that this material has a ${\alpha}-NaFeO_2$ layered structure with $R{\bar{3}}m$ space group and that cation mixing is reduced with increasing synthesis temperature. Scanning electron microscopy (SEM) reveals that nano-sized $Li_{1.2}(Fe_{0.16}Mn_{0.32}Ni_{0.32})O_2$ powder has uniform particle size distribution. X-ray absorption near edge structure (XANES) analysis is used to study the local electronic structure changes around the Mn, Fe, and Ni atoms in this material. The sample prepared at $700^{\circ}C$ delivers the highest discharge capacity of 207 $mAhg^{-1}$ between 2-4.5 V at 0.1 $mAcm^{-2}$ with good capacity retention of 80% after 20 cycles.

공기 분위기에서 스파크 방전을 이용한 은 나노입자 생성 (Generation of Silver Nanoparticles by Spark Discharge Aerosol Generator Using Air as a Carrier Gas)

  • 오현철;정재희;박형호;지준호;김상수
    • 대한기계학회논문집B
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    • 제30권2호
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    • pp.170-176
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    • 2006
  • A spark discharge aerosol generator using air as a carrier gas has successfully been applied to silver nanoparticle production. The spark discharge between two silver electrodes, which was periodically obtained by discharging the capacitor, produced sufficient high temperatures to evaporate a small fraction of the silver electrodes. The silver vapor was subsequently supersaturated by rapid cooling and condensed to silver nanoparticles by nucleation and condensation. The morphology of the generated particles observed by transmission electron microscope was spherical. The element composition of the nanoparticles was silver, which was determined by energy dispersive X-ray spectroscopy. The crystal phase of the particles spark-generated under air atmosphere was composed of silver and silver oxides phase, which was determined by Xray diffraction analysis. While the nanoparticles generated under nitrogen atmosphere had only silver phase. This XRD data indicates that some fraction of the evaporated silver vapor could be oxidized in air atmosphere by the reaction with oxygen. A stable operation of the spark discharge generator has been achieved. The size and concentration of the particles can be easily controlled by altering the repetition frequency, capacitance, gap distance and flow rate of the spark discharge system.

기계적 합금화하여 제조한 Fe-5Y2O3 합금분말의 나노산화물 석출거동 (A Precipitation Behavior of Nano-Oxide Particles in Mechanically Alloyed Fe-5Y2O3 Powders)

  • 김가언;노상훈;최지은;김영도;김태규
    • 한국분말재료학회지
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    • 제22권1호
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    • pp.46-51
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    • 2015
  • A precipitation behavior of nano-oxide particle in Fe-$5Y_2O_3$ alloy powders is studied. The mechanically alloyed Fe-$5Y_2O_3$ powders are pressed at $750^{\circ}C$ for 1h, $850^{\circ}C$ for 1h and $1150^{\circ}C$ for 1h, respectively. The results of Xray diffraction pattern analysis indicate that the $Y_2O_3$ diffraction peak disappear after mechanically alloying process, but $Y_2O_3$ and $YFe_2O_4$ complex oxide precipitates peak are observed in the powders pressed at $1150^{\circ}C$. The differential scanning calorimetry study results reveal that the formation of precipitates occur at around $1054^{\circ}C$. Based on the transmission electron microscopy analysis result, the oxide particles with a composition of Y-Fe-O are found in the Fe-$5Y_2O_3$ alloy powders pressed at 1150oC. It is thus conclude that the mechanically alloyed Fe-$5Y_2O_3$ powders have no precipitates and the oxide particles in the powders are formed by a high temperature heat-treatment.

Catalytic Mechanism for Growth of Carbon Nanotubes under CO-H2 Gas Mixture

  • Chung, Uoo-Chang;Kim, Yong-Hwan;Lee, Deok-Bo;Jeong, Yeon-Uk;Chung, Won-Sub;Cho, Young-Rae;Park, Ik-Min
    • Bulletin of the Korean Chemical Society
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    • 제26권1호
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    • pp.103-106
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    • 2005
  • In order to investigate the catalytic mechanism for the growth of carbon nanotubes (CNTs), a comprehensive study was conducted using carbon materials synthesized at 680 ${^{\circ}C}$ with a gas mixture of CO-H$_2$ after reduction at 800 ${^{\circ}C}$ by H$_2$ gas from iron oxide, and metal Pt. The resulting material was observed by scanning electron microscopy (SEM) and X-ray diffraction patterns (XRD) after a variety of reaction times. The carbon materials synthesized by metal Pt were little affected by reaction time and the sintered particles did not form CNTs. Xray analysis revealed that metal Fe was completely converted to iron carbide (Fe$_3$C) without Fe peaks in the early stage. After 5 min, iron carbide (Fe$_3$C) and carbon (C) phases were observed at the beginning of CNTs growth. It was found that the intensity of the carbon(C) peak gradually increased with the continuous growth of CNTs as reaction time increases. It was also found that the catalyst of growth of CNTs was metal carbide.

MOCVD $PbTiO_3$ 박막의 특성에 관한 연구 (A Study on the MOCVD $PbTiO_3$ Thin Films)

  • 송한상;최두진;유광수;정형진;김창은
    • 한국결정성장학회지
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    • 제2권2호
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    • pp.40-52
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    • 1992
  • Titanium-iso-propoxide[$Ti(OC_3H_7)_4$]와 Tetra-ethyl-lead $[Pb({C_2}{H_5})_4]$를 사용한 MOCVD법으로 PbTi$O_3$박막을 55$0^{\circ}C$에서 증착하였다. Ar과 $O_2$를 각각 운반 및 반응기체로 사용하였으며, 열처리에 따른 박막의 두께와 굴절지수의 변화, Xtjs 회절 분석, CV 특성 측정등을 행하였다. 열처리에 따른 CV 특성 측정 결과 PbTi$O_3$는 Si기판과 계면 반응을 하는 것으로 생각되며, X선 회절 분석 결과 $PbTiO_3$의 특성 peak들이 관찰되었다. 열처리 시간 및 온도의 증가에 따라 박막의 두께는 감소하고, 굴절지수는 증가하는 경향을 보여 주었다.

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