• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2008년도 추계학술대회 논문집
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• pp.260-261
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• 2008

• 접착 및 계면
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• 제1권1호
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• pp.47-55
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• 2000

In this article, the characterization of the interface of hybrid composites was discussed. Interfacial interaction in organic/inorganic hybrid composites, especially silica-containing hybrids can be characterized by fluorescence spectroscopy, small angle X-ray scattering (SAXS), scanning electron microscopy (SEM), atomic force microscopy (AFM), and $^{29}Si$ NMR spectroscopy measurements.

• 한국산학기술학회논문지
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• 제15권1호
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• pp.39-46
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• 2014

미얀마 Kayah산 녹색 투어말린의 특성을 X-선 형광분석, 자외선-가시광선 그리고 중적외선 분광분석을 통하여 타산지의 녹색 투어말린과 비교하였다. 화학성분 분류에 의해 미얀마 투어말린이 속한 그룹을 조사 하였다. 미얀마 투어말린은 V 원소를 많이 함유하고 있었고 X 사이트에 Ca 원소를 반 이상 함유한 Calcic 그룹에 속했고 우바이트 (Uvite)로 명명되었다. 자외선-가시광선 분석결과 $V^{3+}$ 이온에 의한 415와 611 nm에 강한 흡수밴드가 나타나 녹색 투어말린의 원인이 되었다. $Fe^{2+}$ 이나 $Cu^{2+}$ 이온에 의해 녹색이 나타나는 타산지의 녹색 투어말린과 차이가 있었다. 중적외선 분석에서는 수산기와 금속들 간의 진동에 의한 흡수가 일어났는데 1100 $cm^{-1}$ 근처에서 스트레칭 모드, 3500 $cm^{-1}$ 주변에서 벤딩 모드 그리고 4600과 4200 $cm^{-1}$ 사이에서 스트레칭과 벤딩 모드의 혼합 밴드가 나타났다.

• Environmental Sciences Bulletin of The Korean Environmental Sciences Society
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• 제4권4호
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• pp.215-220
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• 2000

This study on the incineration ash and sintering pellet from sewage sludge was carried out to evaluate the possibility of recycling in sewage sludge disposal. The samples used in this experiment were raw sewage sludge, its incineration ash, and sintering pellet. The characteristics of the three sample types were identified using X-ray diffraction(XRD), X-ray fluorescence(XRF), atomic absorption spectroscopy(AAS), and inductively coupled plasma spectroscopy(ICP). The chemical compositions of all three sample types were similar in their clay component, however, the sewage sludge had a high content of organic materials. From an analysis of the mineral content of the three sample types, the conversion of their compositions was found to be relative to temperature. Accordingly, incineration ash and sintering pellet both have potential for use as a functional construction material.

• 한국재료학회지
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• 제18권3호
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• pp.143-147
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• 2008

Fe compounds in scoria as distributed in the south-western area of Jeju Island were investigated using X-ray fluorescence spectroscopy, X-ray diffractometry, and $^{57}Fe$ $M{\ddot{o}}ssbauer$ spectroscopy. The samples were prepared from four parasite volcanoes. It was found that these samples are typical basalt comprised of $SiO_2$, $Al_2O_3$, Fe, and silicate minerals. The $M{\ddot{o}}ssbauer$ spectra showed doublets for olivine, pyroxene, and ilmenite as well as sextets for hematite and magnetite. The valence state of Fe is chiefly a 3+ charge state with a slight 2+ charge state. It is expected that these results will add to the body of information related to the formation mechanisms of Jeju Island.

• Journal of Ceramic Processing Research
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• 제13권spc2호
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• pp.403-406
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• 2012

Effect of thickness on ZnO properties including the compositional ratio and crystallinity has been systematically investigated using a variety of characterization tools of x-ray diffraction, field emission scanning electron microscopy, x-ray fluorescence and x-ray photoelectron spectroscopy. Interestingly, it was observed that ZnO films below 80 nm in thickness were in oxygen deficiency, while the oxygen ratio was increased in the films above the thickness, although the compositional ratio of ZnO film was not linearly varied with increasing film thickness. Also, ZnO crystallinity, which is characterized by (002) diffraction pattern, was clearly improved with increasing film thickness. The properties of ZnO film with different sputtering time and the nature of direct current reactive sputtering process were discussed in terms of compositional ratio, especially oxygen ratio in ZnO film.

• Bulletin of the Korean Chemical Society
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• 제33권12호
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• pp.4052-4058
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• 2012

The composite photocatalyst, N-$TiO_2$ loaded with $Ni_2O_3$, was prepared by $N_2$ plasma treatment. X-ray diffraction, X-ray fluorescence, $N_2$ adsorption, UV-vis spectroscopy, photoluminescence, and X-ray photoelectron spectroscopy were used to characterize the prepared $TiO_2$ samples. The results indicated that the band gap energy was decreased obviously by nitrogen doping, whereas loading of $Ni_2O_3$ did not influence the band gap and visible light absorption. The photocatalytic activities were tested in the degradation of 2,4,6-trichlorophenol (TCP) under visible light. The photocatalytic activity and stability of composite photocatalyst were much higher than that of catalyst modified with nitrogen or $Ni_2O_3$ alone. The synergistic effect of doping nitrogen and $Ni_2O_3$ over $TiO_2$ was investigated.

• 한국산학기술학회논문지
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• 제13권5호
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• pp.2291-2297
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• 2012

X-선 스펙트럼 데이터는 물질의 성분과 관련이 없는 신호(백그라운드, 노이즈)들을 포함 하고 있다. XRF는 스펙트럼에서 가우시안 형태의 피크 위치와 크기를 이용하여 시료의 성분을 분석하며, 시료의 성분을 정확히 분석하기 위해서는 노이즈와 백그라운드를 제거 하여야 한다. 백그라운드를 제거하기 위한 방법으로는 SNIP, Threshold, Morphology 방법 등을 적용하고 있으며, Threshold 기법을 중에서 블록별로 각기 다른 임계값을 적용하는 Interval Threshold기법이 하나의 임계값을 적용하는 Level Threshold 방법보다 더 좋은 성능을 발휘한다. 본 논문에서는 Interval Threshold를 적용하기 위하여 웨이블릿을 이용하여 블록을 분리하는 알고리즘을 제안하였다.

• 대한화학회지
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• 제59권2호
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• pp.136-141
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• 2015

We have discovered that quercetin, once coated on the CdSe and CdSe-CdS quantum dots (QDs), becoming highly water soluble. In the present work, we have successfully synthesized CdSe/CdS/N-Acetyl-L-Cysteine(NAC)/Quercetin nano-composites in the aqueous solution. The products were characterized using UV-vis spectroscopy, X-ray powder diffraction, fluorescence spectroscopy, and Fourier transform infrared spectroscopy. The transmission electron microscopy (TEM) tests indicated that our nano-composite products are highly stable with homogeneous particle size and great monodispersity. Quercetin coated nano-composite CdSe/CdS/NAC/Quercetin showed different fluorescence behavior from that of CdSe/CdS/NAC. Most amazingly, the synthesized CdSe/CdS/NAC/Quercetin nano-composite exhibits strong antibacterial activity. The combination of the strong fluorescence and its antibacterial activity makes the quercetin modified quantum dots as a potential candidate for cancer targeted therapy and other cancer treatments.

• Nuclear Engineering and Technology
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• 제53권6호
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• pp.2025-2037
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• 2021

The influence of lead cations on natural quartz (QZ) from Egypt as a glass shielding material for the composition with nominal formula (10Na₂O - (90 - x) QZ - xPbO (where x = 30, 35, 40, 45 and 50 mol %)) was examined. The studied samples are synthesized via the melt quenching method at 1050 ℃. The X-ray diffraction XRD patterns were confirmed the glass nature for studied samples. Moreover, the optical properties, and the transparency for all compositions were examined by UV-Vis spectroscopy. Also, the major elemental composition of the natural quartz were estimated via the X-ray fluorescence (XRF) technique. Further, the density and molar volume were determined. Furthermore, the nuclear shielding parameters such as, mass attenuation coefficient, effective atomic number, electronic density, the total atomic, and electronic cross sections as well as the mean free path, and the half value layer with different gamma ray energies (81 keV-1407 keV) were calculated. Besides, the results showed that the shielding behavior towards the gamma ray radiation for all glass samples was increased as the increment in PbO concentration in the glass system.