• Journal of Ocean Engineering and Technology
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• v.16 no.3
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• pp.54-58
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• 2002

This study investigates a relationship between fracture mechanics parameters (Stress Intensity Factor Range: ΔK, Maximum Stress Intensity Factor; Kmax) and X-ray parameters (residual stress:$\sigma$r half-value breadth: B) for SG365 steel at elevated temperature up to 30$0^{\circ}C$. The fatigue crack propagation test were carried out and X-ray diffraction technique according to the direction of crack length was applied to fatigue fractured surface. The residual stress on the fracture surface was found to increase at low ΔK region, to reach a maximum value at a certain value of Kmax or ΔK and then to decrease. Residual stress was independent of stress ratio by arrangement of ΔK and half value breadth were independent of the arrangement of Kmax. The equation of $\sigma$r-ΔK was established by the experimental data. therefore, fracture mechanics parameters could be estimated by the measurement of X-ray parameters.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.317-323
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• 2001

This study verified the relationship between fracture mechanics parameters$({\Delta}K,\;{\Delta}K_{eff},\;K_{max})$ and X-ray parameters $(\sigma_r,\;B)$ for SG365 steel at elevated temperature up to $300^{\circ}C$. The fatigue crack propagation test were carried out and X-ray diffraction technique according to crack length direction was applied to fatigue fractured surface. The residual stress on the fracture surface was found to increase low ${\Delta}K$ region, reach to a maximum value at a certain value of $K_{max}\;or\;{\Delta}K$ and then decrease. Residual stress were independent on stress ratio by arrangement of ${\Delta}K$ and half value breadth were independent by the arrangement of $K_{max}$. The equation of $\sigma_r-{\Delta}K$ was established by the experimental data. Therefore, fracture mechanics parameters could be estimated by the measurement of X-ray parameters.

• Nuclear Engineering and Technology
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• v.56 no.1
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• pp.114-122
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• 2024

Irradiation-induced defects and the precipitates in the wrapper material of the Indian Fast Breeder Test Reactor (FBTR), SS 316 are analyzed using the synchrotron source-based Angle Dispersive X-Ray Diffraction (ADXRD) technique with X-rays of energy 17.185 keV (wavelength ~0.72146 Å). The differences and similarities in the high displacement damage samples as a function of dpa (displacement per atom) and dpa rate in the range of 2.9 × 10^-7- 9 × 10^-7 dpa/s are studied. Ferrite and M₂₃C₆ are commonly observed in the present set of high displacement damage 40-74 dpa SS 316 samples irradiated at temperatures in the range of 400-483 ℃. Also, the dislocation density has increased as a function of the irradiation dose. The X-ray diffraction peak profile parameters quantified such as peak shift and asymmetry show that the irradiation-induced defects are sensitive to the dpa rate-irradiation temperature combinations. The increase in yield strength as a function of displacement damage is also correlated to the dislocation density.

• Journal of Ocean Engineering and Technology
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• v.8 no.1
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• pp.114-122
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• 1994

X-ray stress constant, K, was determined for the diffraction line of (211)plane by using Cr-K$\alpha$ radiation. K was -340.87 MPa/deg. Fatigue crack propagation tests of SS41 steel were conducted under stress ratios of 0.1, 0.3 and 0.5. The half-value breadth of X-ray diffraction profile was measured at and beneath the fracture surface. The half-value breadth, B, on the fracture surface was found to increase with increasing $K_max$. The value of B was influenced by stress ratio in SS41 steel. The half-value breadth took the maximum value at the borden of reversed plastic zone, while it approached to the initial (pre-fatigue) value near the boundary of monotonic plastic zone. The maximum depth of the plasticzone was evaluated on the basis of the half-value breadth distribution. The depth $\omega$$_y$ is related to $K_max$by the following equation : $\omega$$_y$ = $\alpha$($K_max$/$\sigma$$_y$$)^2$ where .sigma.$\sigma$$_y$ is the yield strength obtength obtained in tension test .alpha.is 0.136 for SS41 steel.

• Tribology and Lubricants
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• v.13 no.2
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• pp.39-45
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• 1997

The shot peening treatment were conducted for improving the strength of rolling contact fatigue of machine element like a gear. This paper was undertaken to analyze the influence of shot peening treatment for inner race of ball bearing on the rolling contact fatigue. Shot peening treatment were applied to the full hardened and the carbonitrided bearing. And the rolling contact fatigue life test and X-ray diffraction test were carried out. The results of this study showed that the fatigue life of ball bearing in the clean and the contaminated oil could be improved by shot peening treatment. This effect was found to be more pronounced to the full hardened bearing. These facts might be due to the generation of compressive residual stress and the strain hardening of surface layer by shot peening treatment. The failure of the shot peened bearing were presumed to initiate at surface.

• Journal of the Korean Society of Clothing and Textiles
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• v.29 no.2
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• pp.347-355
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• 2005

Biodegradability of cotton/polyester blend fabric was investigated employing activated sluge test, soil burial test and enzyme hydrolysis. Surface changes of the degraded sample were observed through a microscopy. Changes in X-ray diffraction patterns and crystallinity were examined using X-ray diffractometer. Experimental results revealed that biodegradability of cotton/polyester blend fabric was proportional to the blending ratio of cotton, not showing any synergy effect. Polyester 100% hardly degraded in this study. Through the comparison of the experimental method it was shown that the biodegradabilities determined from activated sludge test and enzymatic hydrolysis except soil burial test were linearly related to the blending ratio of cotton in the blent fabrics. It is probably because the biodegradability determined from the retention of tensile strength of fabrics buried in soil was affected by the stress distribution of polyesters throughout the fabric. From the microscopic observations it was revealed that fungi were grown on the fabric surface and the colors turned yellow, brown and black. X-ray diffraction patterns showed that the heights of crystalline peak coming from cotton part in blend fabrics decreased whereas those coming from polyester part increased comperatively as time passed by. Crystallinities of cotton 100% fabric increased slightly at the begining and then decreased continuously.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.258-265
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• 2001

Turbine blade is subject to force of three type ; torsional force by torsion-mount, centrifugal force by rotation of rotor and cyclic bending force by steam pressure. Cyclic bending force of them is main factor on fatigue fracture. In the X-ray diffraction method, the change in the values related to plastic deformation and residual stress near the fracture surface mat be determined, and information of internal structure of material can be obtained. Therefore, to find a fracture mechanism of torsion-mounted blade in nuclear plant, based on the information from the fracture surface obtained by fatigue test, the correlation of X-ray parameter and fracture mechanics parameter was determined, and then the load applied to actual broken turbine blade parts was predicted. Failure analysis is performed by finite element method and Goodman diagram on torsion-mounted blade.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1996.10a
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• pp.207-212
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• 1996

The shotpeening treatment were conducted for improving the strength of rolling contact fatigue of machine element like a gear. This paper was undertaken to analyze the influence of shotpeening treatment for inner race of ball bearing on the roiling contact fatigue. Shotpeening treatment were applied to the full hardened and the carbonitrided bearing. And the rolling contact fatigue life test and X-ray diffraction test were carried out. The results of this study showed that the fatigue life of ball bearing in the clean and the contaminated oil could be improved by shotpeening treatment. This effect was found to be more pronounced to the full hardened bearing.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.2
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• pp.311-320
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• 1998

The cryogenic fracture behaviors of austenitic stainless steel HN2 developed for nuclear fusion reactor were evaluated quantitatively by using the small punch(SP) test. The electrochemical polarization test was applied to study thermal aging degradation of HN2 steel. The X-ray diffraction(XRD) analysis was conducted to detect carbides and nitrides precipitated on the grain boundary of the heat treated HN2 steel. The mechanical properties of the HN2 steel significantly decreased with increasing time and temperature of heat treatment or with decreasing testing temperature. The integrated charge(Q) obtained from electrochemical polarization test showed a good correlation with the SP energy(ESP) obtained by means of SP tests. From the results observed in the x-ray diffraction and anodic polarization curve, it was known that the material the grain boundary. Combining SP test and electrochemical polarization test, it could be useful tools to non-destructively evaluate the cryogenic fracture behaviors and the aging degradation for cryogenic structural material.

• The Journal of Advanced Prosthodontics
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• v.13 no.4
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• pp.258-267
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• 2021

PURPOSE. The purpose of this study was to compare the surface roughness, phase transformation, and surface topography of dental zirconia with three different yttrium oxide compositions under same grinding and polishing conditions. MATERIALS AND METHODS. Three zirconia disks (IPS e.max ZirCAD LT, MT, MT multi, Ivoclar Vivadent AG, Schaan, Liechtenstein) were selected for experimental materials. Sixty-nine bar-shaped specimens were fabricated as 12.0 × 6.0 × 4.0 mm using a milling machine and glazing was conducted on 12.0 × 6.0 mm surface by same operator. With a custom polishing device, 12.0 × 6.0 mm surfaces were polished under same condition. Surface roughness (Ra[㎛]) was measured before grinding (C), after grinding (G), and at every 3 steps of polishing (P1, P2, P3). X-ray diffraction and FE-SEM observation was conducted before grinding, after grinding, and after fine polishing (P3). Statistical analysis of surface roughness was performed using Kruskal-Wallis test and Mann-Whitney-U test was used as a post hoc test (α = .05). RESULTS. There were no significant differences of surface roughness between LT, MT, and MM groups. In LT, MT, and MM groups, P3 groups showed significantly lower surface roughness than C groups. X-ray diffraction showed grinding and polishing didn't lead to phase transformation on zirconia surface. In FE-SEM images, growths in grain size of zirconia were observed as yttrium oxide composition increases. CONCLUSION. Polished zirconia surface showed clinically acceptable surface roughness, but difference in yttrium oxide composition had no significant influence on the surface roughness. Therefore, in clinical situation, zirconia polishing burs could be used regardless of yttrium oxide composition.