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$a-Si_{1-x}Ge_x:H$ 박막의 고상결정화에 따른 스핀밀도의 변화

  • 노옥환;윤인호;이정근
    • Proceedings of the Korean Vacuum Society Conference
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    • 1999.07a
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    • pp.64-64
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    • 1999
  • 다결정 실리콘-게르마늄(poly-SiGe)은 태양전지 및 TFT-LCD와 같은 소자 응용에 있어서 중요하게 연구되고 있는 물질이다. 우리는 수소화된 비정질 실리콘-게르마늄 (a-Si1-xGex:H) 박막을 증착시키고 고상결정화시키며 XRD(x-ray diffraction) 및 ESR (electron spin resonance) 측정을 수행하였다. PECVD 증착가스는 SiH4과 GeH4가스를 사용하였고 Ge의 성분비는 x=0.0, 0.1, 0.5 정도로 조절되었다. 기판은 Corning 1737 glass를 사용하였고, 기판 온도는 20$0^{\circ}C$ 이었다. 증착압력과 r.f. 전력은 각각 0.6Torr와 3W이었다. 증착된 SiGe 박막은 고상결정화를 위해 $600^{\circ}C$ N2 분위기에서 가열되고, 그에 따른 XRD 및 ESR spectrum의 변화를 관찰하였다. ESR 측정은 X-band 그리고 상온에서 행해졌다. 먼저 XRD 측정으로부터 박막의 고상결정화 정도를 알 수 있었고, 고상결정화 과정이 초기 핵형성 단계와 결정화 단계, 그리고 더 이상 결정화가 일어나지 않는 완료 단계로 구분될 수 있음을 보여주었다. X값이 증가함에 따라 결정화 시간은 훨씬 단축되었다. ESR로 측정된 스핀 밀도는 a-Si1-xGex:H 박막이 처음 가열됨에 따라 전체적으로 크게 증가했다가, 결정화가 일어나면서 다시 감소하여 나중에는 거의 변화가 없었다. ESR 신호의 초기 증가는 수소 이탈에 의한 dangling bond의 증가에 기인하며, 다음 단계의 감소 및 안정 상태는 결정화에 따른 결정경계 영역의 감소와 결함들의 안정성에 기인하는 것으로 생각된다. 그러나 흥미로운 것은 Si1-xGex 합금의 경우 가열시간이 증가됨에 따라 Si-db(Si-dangling bond)와 Ge-db에 의한 신호가 서로 분리되어 나타났으며, 이 Si-db 스핀 밀도와 Ge-db 스핀밀도의 변화정도는 x값에 크게 의존함을 보여준 것이다. 즉 순수한 a-Si:H의 경우 Si-db 의 스핀밀도의 증가시간은 4시간 정도였고, 그리고 다시 감소하였으며, x=0.1 인 박막에서 Si-db와 Ge-db의 변화 시간은 순수 S-db 변화의 경우와 거의 유사하였다. 그러나 x=0.5 샘플에서는 Si-db의 변화가 빨라져서 0.1 시간 안에 증가되었고, Ge-db의 변화는 더 빠르게 수 분 동안에 증가 된후 다시 감소하였다. 이것은 수소의 Si에 대한 친화력 뿐 만아니라 Si-H과 Ge-H 결합에너지가 주위 원자들의 구성에 크게 영향받을 수 있는 가능성을 제시해준다.

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Evolution of Next Generation Mobile Network Based on CDMA2000-1X Network (CDMA 2000-1X를 기반으로한 차세대 이동망의 진화)

  • Son, Dong Chul;Kim, J.W.;Ryu, C.S.
    • The Journal of the Korea institute of electronic communication sciences
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    • v.1 no.1
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    • pp.70-80
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    • 2006
  • The large portion of communication service areas move from a legacy wire-line voice service to mobile data service. For the purpose of satisfaction on market need, many communication systems should be installed and upgraded based on a mobile wide-band transmission facility. Recently, large part of communication service is based on internet protocol by packet switch techniques and required new technologies such as multimedia processing, QoS achievement, and mobility managememobile communication network such as IS-95A/B and CDMA2000-1X. In this paper, I analyzed the network architecture and service provision methods. in CDMA2000-1X nt. In korea, a CDMA communication technique is standardized for digital mobile communication systems. By using the analysed results, I will extract an efficient method for network evolution and a core technique for next generation mobile communication network.

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Migration Activity of Chicken Gonadal Primordial Germ Cells (gPGCs) and Post-transfer Localization of LacZ-transfected gPGCs in the Embryonic Gonads

  • Jeong, D.K.;Han, J.Y.
    • Asian-Australasian Journal of Animal Sciences
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    • v.15 no.9
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    • pp.1227-1231
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    • 2002
  • A powerful tool for chicken transgenesis could be established by employing a germline chimera production through primordial germ cell transplantation. This study was conducted to examine whether foreign gene-transfected gonadal primordial germ cells (gPGCs) have a migration activity into the gonad after transfer to recipient embryos. In Experiment 1, gPGCs of Korean Ogol Chicken were retrieved from 5.5-day-old embryos and subsequently transferred to the dorsal aorta of 2.5-day-old White Leghorn embryos after being labeled with PKH26 fluorescent dye. To confirm migration activity after transplantation, recipient embryos were sacrificed and examined on 3 days after transfer. Sex determination was concomitantly undertaken to examine whether sex of recipient embryos could affect the migration activity of gPGCs. All of embryonic gonads examined showed positive signals with PKH26 fluorescence and W-chromosome specific band by polymerase chain reaction (PCR) was detected in male embryos when gPGCs with ZW chromosome were transferred to recipient embryos. In Experiment 2, retrieved gPGCs were transfected with LacZ gene-containing cytomegalovirus promoter ($pCMV{\beta}$) by electroporation and subsequently transferred to recipient embryos. LacZ gene expression was identified in the gonads of 6 or 10-day-old recipient embryos and hatched-chicks. A total of 20 embryos and 12 hatched-chicks were examined and 11 of them (10 embryos and one hatched chicken; 11/32=34.4%) expressed $\beta$-galactosidase, a marker substance of LacZ gene. The results of this study demonstrated that foreign gene-transfected gPGCs can migrate and settle down into the gonad after being transferred into the blood vessel of the recipient embryos. This established technique will contribute to developing a peer biotechnology for transgenic chicken.

COMPUTATIONAL INVESTIGATION OF NOZZLE FLOWFIELD IN A MICRO TURBOJET ENGINE AND ITS SCALING CHARACTERISTICS (마이크로 터보제트 엔진 노즐 유동장에 관한 CFD 전산해석 및 스케일링 특성 연구)

  • Lee, H.J.;An, C.H.;Myong, R.S.;Choi, S.M.;Kim, W.C.
    • Journal of computational fluids engineering
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    • v.22 no.1
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    • pp.43-50
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    • 2017
  • Thermal flowfield of a micro turbojet engine was computationally investigated for exhaust nozzles with different aspect ratio and curvature. Special attention was paid to maximum and average temperature of the nozzle surface and the exhaust nozzle plume. The IR signatures of the micro turbojet engine nozzle were then calculated through the narrow-band model based on thermal flowfield data obtained through CFD analysis. Finally, in order to check the similarity of thermal flowfields and IR signature of the sub-scale micro turbojet engine model and the full-scale UCAV propulsion system, several non-dimensional parameters associated with temperature and optical property of plume were introduced. It was shown that, in spite of some differences in actual values of non-dimensional parameters, the scaling characteristics on spectral feature of IR signature and effects of aspect ratio and curvature of nozzle configuration remain similar in sub-scale and full-scale cases.

Design of $2{\times}1$ Array Antenna Using Stack Structure for IEEE 802.11a (적층구조를 이용한 IEEE 802.11a용 $2{\times}1$ 배열 안테나 설계)

  • Park, Jung-Ah;Bu, Chong-Bae;Kim, Kab-Ki
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2007.10a
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    • pp.849-852
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    • 2007
  • In this paper, the high gain and the broadband microstrip patch antenna, which is applicable to 5 GHz band wireless LAN, is designed in order to integrate IEEE 802.11a's detailed standards($a:5.15{\sim}5.25$, $b:5.25{\sim}5.35$, $c:5.725{\sim}5.875$ [GHz]). Designed patch antenna has settled resonance frequency by insert substance(polyurethane: ${\varepsilon}_r=6.5$) between the separated parasitic patch and radiation patch for the purpose of miniaturize. And the form (${\varepsilon}_r=1.03$) were to fix the separated radiation patch and ground plans by air. Designed frequency bandwidth(VSWR 2:1) of the antenna showed broadband characteristic of $4.9[GHz]{\sim}6.1[GHz]$ to about 1.2[GHz]. Also the E-plan and H-plan profit 12[dBi] above, the 3[dB] beamwidth showed the characteristic over the E-plan $30^{\circ}$ and H-plan $60^{\circ}$ to be improved.

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A Study on Frequency Hopping Signal Detection Using a Polyphase DFT Filterbank (다상 DFT 필터뱅크를 이용한 도약신호 검출에 관한 연구)

  • Kwon, Jeong-A;Lee, Cho-Ho;Jeong, Eui-Rim
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.17 no.4
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    • pp.789-796
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    • 2013
  • It is known that the detection of hopping signals without any information about hopping duration and hopping frequency is rather difficult. This paper considers the blind detection of hopping signal's information such as hopping duration and hopping frequency from the sampled wideband signals. In order to find hopping information from the wideband signals, multiple narrow-band filters are required in general, which leads to huge implementation complexity. Instead, this paper employs the polyphase DFT(discrete Fourier transform) filterbank to reduce the implementation complexity. This paper propose hopping signal detection algorithm from the polyphase DFT filterbank output. Specifically, based on the binary image processing, the proposed algorithm is developed to decrease the memory size and H/W complexity. The performance of the proposed algorithm is evaluated through the computer simulation and FPGA (field programmable gate array) implementation.

The structural, optical and photocatalytic properties of $TiO_2$ thin films fabricated by do magnetron sputtering (직류 마그네트론 스퍼터링법으로 제조된 $TiO_2$ 박막의 구조적, 광학적 특성 및 광촉매 효과)

  • Lim, J.M.;Yang, H.H.;Kim, Y.J.;Park, J.Y.;Jeong, W.J.;Park, G.C.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.420-423
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    • 2003
  • [ $TiO_2$ ] thin films were fabricated by DC magnetron sputtering system at by controlling deposition times, ratios of $Ar:O_2$ partial presser ratio and substrate conditions. And the surface, cross-section morphology, microstructure, and composition ratio of the films were analyzed by FE-SEM, TEM and XPS. Besides, the optical absorption and transmittance of the $TiO_2$ films were measured by a UV-VIS-NIR Spectrophotometer, and photocatalytic properties were studied by G C Analyzer & Data Analysis system. As the result, when $TiO_2$ thin film was made at deposition time of 120[min] and $Ar:O_2$ ratio of 60:40, the best structural and optical properties among many thin films could be accepted. The best results of properties were as follows: thickness; $360{\sim}370[nm]$, grain size; 40[m], gap between two peak binding energy, $5.8{\pm}0.05[eV]$ ($2p_{3/2}$ peak and $2p_{1/2}$ peak of Ti was show at $458.3{\pm}0.05[eV]$ and $464.1{\pm}0.05[eV]$ respectively), binding energy; $530{\pm}0.05\;[eV]$, opticalenergy band gap; 3.4[eV].

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Drying Characteristics by Infrared Heating of agricultural products (원적외선 가열에 의한 농산물의 건조특성)

  • Sang, Hie-Sun;Bae, Nae-Kyung
    • Journal of the Korean Society of Industry Convergence
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    • v.8 no.1
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    • pp.47-55
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    • 2005
  • Infrared heating has been traditionally used in industrial applications for processes such as dehydration of food industrial. This heating method involves the application of radiation in the wavelength range of 2 to 50 micrometers. In this work, simultaneous heat balance equations were developed to simulate the infrared radiation heating of agricultural products. The equations assume that moisture diffuses to the outer boundaries of the material in liquid form and evaporation occurs at the surface of the agricultural products. Energy for moisture evaporation is supplied by the infrared radiant energy. The optimum temperature and drying time for the best drying conditions of changing the red peppers with the moisture content of 18% and the restore rate of 80~85% are $80^{\circ}C$ and 44 hours. The performance of radiation tubes coating with the radiation paint developed in this research has the energy of $2.27{\times}103W/m^2{\mu}m$, $150^{\circ}C$ within the scope of radiation wave length of $2{\sim}30{\mu}m$ and has the radiation 0.92~0.93, which is superior to the general radiation tubes. The extinction coefficient according to the band pass filter using the 4 flux theory ha higher dependability on wave length, accounting for $2{\sim}17{\mu}m$ and $5{\times}105{\sim}106m-1$. A comparison between the theoretical energy transfer whose figures are interpreted according to 4 flux theory and the experimental energy transfer of far infrared dryer leads to the findings of the agreement less than 5%.

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Effect of Microwave Irradiation on Exfoliation of Graphene Oxide (마이크로파 조사가 산화그래핀의 화학적 박리에 미치는 효과)

  • Lee, Jae-Hee;Hwang, Ki-Wan;Jeong, Young-Hoon;Kim, Eui-Tae
    • Korean Journal of Materials Research
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    • v.23 no.12
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    • pp.708-713
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    • 2013
  • Graphene oxide has been synthesized by microwave-assisted exfoliation of graphite oxide prepared by modified Hummers method. Graphite was oxidized in a solution of $H_2O_2$ and $KMnO_4$ at $65{\sim}80^{\circ}C$, followed by 10 % $H_2O_2$ solution treatment at $80{\sim}90^{\circ}C$. The graphite oxide was exfoliated under microwave irradiation of 1 kW and was reduced to graphene effectively by hydrazine hydrate ($H_4N_2{\cdot}H_2O$) treatment. The exfoliation of graphene oxide was significantly affected by the microwave irradiation on (heating)/off (cooling) period. An on/off period of 10 s/20 s resulted in much more effective exfoliation than that of 5 s/10 s with the same total treatment time of 10 min. This can be explained by the higher exfoliation temperature of 10 s/20 s. Repetition of the graphite oxidation and exfoliation processes also enhanced the exfoliation of graphene oxide. The thickness of the final graphene products was estimated to be several layers. The D band peaks of the Raman spectra of the final graphene products were quite low, suggesting a high crystal quality.

Growth Properties of Sputtered ZnO Thin Films Affected by Oxygen Partial Pressure Ratio (산소분압비에 따른 ZnO 박막의 성장특성)

  • Kang, Man-Il;Kim, Moon-Won;Kim, Yong-Gi;Ryu, Ji-Wook;Jang, Han-O
    • Journal of the Korean Vacuum Society
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    • v.17 no.3
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    • pp.204-210
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    • 2008
  • ZnO thin films were grown on a glass by RF sputtering system with RF power 100W and oxygen partial pressure of $0%{/sim}30%$. Elliptic constants were measured by using a phase modulated spectroscopic ellipsometer and analyzed with the Tauc-Lorentz dispersion formula and best fit method in the range of 1.5 to 3.8eV. Also, scanning electron microscope(SEM) was used for the analysis of surface crystallization condition. From elliptic constants spectra, optical constants, thickness and roughness of ZnO films were evaluated. Total thickness of ZnO films obtained by ellipsometry showed good agreement with SEM data. It was found that the grain size of the films were getting smaller with increasing oxygen partial pressure. Band-gap of ZnO films increase with the oxygen partial pressure. These findings clearly indicate that optical properties of ZnO films are strongly dependent on the oxygen partial pressure. It could be explained that increasing the oxygen partial pressure induced high crystalline imperfection in the ZnO films.