• Title/Summary/Keyword: Volume Fraction

Search Result 2,453, Processing Time 0.026 seconds

Mechanical Properties and Wear Behaviour of $Al/SiC/Al_{2}O_{3}$ Composite Materials ($Al/SiC/Al_{2}O_{3}$복합재료의 기계적 성질 및 마멸특성)

  • 임흥준;김영한;한경섭
    • Transactions of the Korean Society of Mechanical Engineers
    • /
    • v.17 no.10
    • /
    • pp.2498-2508
    • /
    • 1993
  • $Al/SiC/Al_{2}O_{3}$ hybrid composites are fabricated by squeeze infiltration method. From the misconstructive of $Al/SiC/Al_{2}O_{3}$ hybrid composites fabricated by squeeze infiltration method, uniform distribution of reinforcements and good bondings are found. Hardness value of $Al/SiC/Al_{2}O_{3}$ hybrid composites increases linearly with the volume fraction of reinforcement because SiC whisker and $Al_{2}$O$_{3}$ fiber have an outstanding hardness. Optimal aging conditions are obtained by examining the hardness of $Al/SiC/Al_{2}O_{3}$ hybrid composites with different aging time. Tensile properties such as Young's modulus and ultimate tensile strength are improved up to 30% and 40% by the addition of reinforcements, respectively. Failure mode of $Al/SiC/Al_{2}O_{3}$ hybrid composites is ductile on microstructural level. Through the abrasive wear test and wear surface analysis, wear behaviour and mechanism of 6061 aluminum and $Al/SiC/Al_{2}O_{3}$ hybrid composites are characterized under various testing conditions. The addition of SiC whisker to $Al/SiC/Al_{2}O_{3}$ composites gives rise to improvement of the wear resistance. The wear resistance of $Al/SiC/Al_{2}O_{3}$ hybrid composites is superior to that of Al/SiC composites. The wear mechanism of aluminum alloy is mainly abrasive wear at low speed range and adhesive and melt wear at high speed range. In contrast, that of $Al/SiC/Al_{2}O_{3}$ hybrid composites is abrasive wear at all speed range, but severe wear when counter material is stainless steel. As the testing temperature increases, wear loss of aluminum alloy decreases because the matrix is getting more ductile, but that of $Al/SiC/Al_{2}O_{3}$ hybrid composites is hardly varied. Oil lubricant is more effective to reduce the wear loss of aluminum alloy and $Al/SiC/Al_{2}O_{3}$ hybrid composites at high speed range.

Microstructures and Dielectric Properties of Nanocrystalline $\textrm{La}^{3+}$-doped $\textrm{BaTiO}_3$ Ceramics (초미립 $\textrm{La}^{3+}$-doped $\textrm{BaTiO}_3$세라믹스의 미세구조 및 유전특성)

  • Cho, Ji-Man;Kim, Byong-Ho;Kim, Gyeung-Ho;Je, Hae-June;Lee, Hae-Won;Kim, Byung-Kook
    • Korean Journal of Materials Research
    • /
    • v.9 no.10
    • /
    • pp.956-961
    • /
    • 1999
  • When the 0-2 mol% of $\textrm{La}_{3+}$ were added to the nanocrystalline $BaTiO_3$ powders and sintered at $1200~1400^{\circ}C$, the nanocrystailine $BaTiO_3$ ceramics having the average grain size of 110-240 nm were obtained except for when no $\textrm{La}_{3+}$ was added and sintered at > $1350^{\circ}C$. As the average grain size decreased from 240 nm to 110 nm, the tetragonality (c/a) and volume fraction of the $90^{\circ}$ domain decreased, and all the properties such as relative dielectric constant at room temperature, maximum relative dielectric constant at the temperature of phase transformation $\textrm{T}_{c}$ and diffuseness of phase transformation at $\textrm{T}_{c}$ also decreased. The results were attributed to the internal stress induced by inhibition of the $90^{\circ}$ domain formation in the case of finer grain size.

  • PDF

Purification and Assay of Extracellular Autolysin from Moraxella sp. CK-l (Moraxella sp. CK-1의 세포외 Autolysin의 분리 정제 및 활성도 측정)

  • 오영상;이장현;한명수;윤문영
    • Korean Journal of Microbiology
    • /
    • v.39 no.3
    • /
    • pp.148-154
    • /
    • 2003
  • Moraxella sp. CK-l is known to inhibits the growth of Anabaena cylindrica, a cyanobacterium. It has been documented that the ability of this growth inhibition of Anabaena cylindrica was attributed to extracellular autolysin from Moraxella sp. CK-l. However, it remains to be elucidated identification and characterization of autolysin have yet been elucidated. In this study, we tried to purify and identify autolysin secreted from Moraxella sp. CK-l. Cells were grown in a complex liquid medium (BGC-11) and culture supernatants were collected, followed by ammonium sulfate fractionation. Fractions were further separated with anion exchange column, Mono-Q, in FPLC system and analyzed by SDS/PAGE. The fraction containing high autolysin activity showed a single distinct protein peak in anion column and molecular mass of about 17 kDa in SDS/PAGE. Nterminal amino acid sequencing of the protein was analyzed, of which result showed the homology with some proteases, including extracellular serine protease, Dichelobacter nodosus.

Effect of V and Sb on the Corrosion Behavior and Precipitate Characteristics of Zr-based Alloys for Nuclear Fuel Cladding (핵연료 피복관용 Zr합금의 부식거동 및 석출물 특성에 미치는 V, Sb 첨가의 영향)

  • Jeon, Chi-Jung;Kim, Seon-Jin;Jeong, Yong-Hwan
    • Korean Journal of Materials Research
    • /
    • v.8 no.12
    • /
    • pp.1099-1109
    • /
    • 1998
  • To investigate the effect of V and Sb on the corrosion behavior of Zr- based alloys, corrosion tests were performed on 6 kinds of Zr alloys in an autoclave at $360^{\circ}C$ for 100 days. The transition of the corrosion rate occurred in the sample containing 0.1wt.%V after 10 days but did not occur in the samples containing 0.2wt.%V and 0.4wt.%V. The corrosion resistance of V containing alloys increased with increasing V contents from 0.1 to 0.4wt.% and the alloys containing 0.4wt.%V showed the best corrosion resistance. In the ternary alloys containing 0.1wt.%Sb and 0.4wt.%Sb, the corrosion rate increased significantly from the short exposure time. It was observed that the optimal Sb content for corrosion resistance was 0.2wt.%. The size and volume fraction of precipitates increased with increasing V and Sb contents. The superior corrosion resistance was observed in the Zr alloy having precipitate size of 0.11-0.13$\mu\textrm{m}$. From the result of corrosion behavior and the obserbation of precipitates, the optimal size of the precipitate appear to control the electron conduction in the cathodic reaction and play an important role in maintaining a stable oxide microstructure.

  • PDF

The Hydrogenated Micro-crystalline Silicon(${\mu} c-Si:H$) Films Deposited by Hot Wire CVD Method (Hot Wire CVD법에 의한 수소화된 미세결정 실리콘(${\mu} c-Si:H$) 박막 증착)

  • Lee, Jeong-Cheol;Song, Jin-Su;Park, Lee-Jun
    • Journal of the Institute of Electronics Engineers of Korea SD
    • /
    • v.37 no.8
    • /
    • pp.17-27
    • /
    • 2000
  • This paper presents deposition and characterization of hydrogenated microcrystalline silicon (${\mu}c$ -Si:H) films on low cost glass substrate by Hot Wire CVD(HWCVD). The HWCVD ${\mu}c$ -Si:H films had deposition rates ranging from 2${\AA}$/sec to 35${\AA}$/sec with the variations of preparation conditions, which was 10 times higher than that of the films obtained from the conventional PECVD method. From the Raman spectroscopy, the prepared silicon films were found to be composed of the mixture of crystalline and amorphous phases. The crystalline volume fraction and average crystallite size, obtained from the Raman To mode peak near 520cm$^{-1}$, were 37-63% and 6-10 nm, respectively. The conductivity activation energy($E_a$) of the ${\mu}c$ -Si:H films, representing the difference of conduction band and Fermi level in an intrinsic semiconductors, increased from 0.22eV to 0.68eV with increasing pressure from 30mTorr to 300mTorr. The increase of $E_a$ with pressure indicates that the deposited films have properties close to intrinsic semiconductors, which is also proved with low dark conductivity of the ${\mu}c$ -Si:H deposited at 300mTorr. The tungsten concentration incorporated into films was about $6{\times}10^{16}atoms/cm^3$ in the samples prepared at wire temperature of 1800$^{\circ}C$.

  • PDF

The Behaviour of Dust Concentrations During Sand Storm in Seoul Area (황사기간 중 PM2.5, PM10, TSP 농도 특성에 관한 연구)

  • Kim, Min-Young;Kim, Kwang-Rae;Lee, Min-Hwan;Cho, Seog-Ju
    • Journal of the Korean earth science society
    • /
    • v.24 no.4
    • /
    • pp.315-324
    • /
    • 2003
  • The characteristics of particles were evaluated through the measurement data of PM$_{2.5}$, PM$_{10}$ and TSP instruments located in air quality monitoring stations installed and operated by Seoul Metropolitan city. The data of particulate mass on the filter was collected bv a high volume air sampler during the sand storm period. The number of days of sand storm in Seoul showed a different pattern from 1990 to November 2002, We can see a trend of increased occurrence and duration of sand storms. The ratio of PM$_{10}$ to TSP was shown as 52.9% and 59.4% during the sand storm period in 2000 and 2001. respectively. It was indicated that the particles larger than 10${\mu}$m increased by approximately 10% in sand storm periods compared to no sand storm period. While PM$_{10}$ size fraction reached 71.4% in 2002, the contribution of sand storm to total particulate concentration was estimated to be 11.9% for PM$_{2.5}$, 23.1% for PM$_{10}$, 19% for TSP in 2002, respectively and sand storms highly correlated with annual total particulate concentration.

Heart-Model-Based Automated Method for Left Ventricular Measurements in Cardiac MR: Comparison with Manual and Semi-automated Methods (자동화 방식 모델 기반 좌심방 파라미터 측정법: 수동 및 반자동 방식과의 비교)

  • Chae, Seung Hoon;Lee, Whal;Park, Eun-Ah;Chung, Jin Wook
    • Investigative Magnetic Resonance Imaging
    • /
    • v.17 no.3
    • /
    • pp.200-206
    • /
    • 2013
  • Purpose : To assess the effect of applying an automated heart model based measurements of left ventricle (LV) and compare with manual and semi-automated measurements at Cardiovascular MR Imaging. Materials and Methods: Sixty-two patients who underwent cardiac 1.5T MR imaging were included. Steady state free precession cine images of 20 phases per cardiac cycle were obtained in short axis views and both 2-chamber and 4-chamber views. Epicardial and endocardial contours were drawn in manual, automated, and semi-automated ways. Based on these acquired contour sets, the end-diastolic (ED) and end-systolic (ES) volumes, ejection fraction (EF), systolic volume (SV) and LV mass were calculated and compared. Results: In EDV and ESV, the differences among three measurement methods were not statistically significant (P = .399 and .145, respectively). However, in EF, SV, and LV mass, the differences were statistically significant (P=.001, <001, <001, respectively) and the measured value from automated method tend to be consistently higher than the values from other two methods. Conclusion: An automatic heart model-based method grossly overestimate EF, SV and LV mass compared with manual or semi-automated methods. Even though the method saves a considerable amount of efforts, further manual adjustment should be considered in critical clinical cases.

Numerical Modeling of Dehydration of Subducting Slab and Behavior of Expelled Water: A Preliminary Study (섭입해양판의 탈수 및 탈수된 물의 거동 수치모델링: 선행 연구)

  • Lee, Changyeol
    • Geophysics and Geophysical Exploration
    • /
    • v.21 no.3
    • /
    • pp.198-206
    • /
    • 2018
  • In this preliminary study, dehydration of the subducting slab and behavior of the expelled water are numerically modeled using 2-dimensional model scheme. The hydrated minerals in the oceanic crust of the subducting slab experience dehydration by increases in temperature and pressure and expel their water into the overlying mantle wedge. Behavior of the expelled water is governed by both the corner flow in the mantle wedge and porous flow of the expelled water through the pores of the mantle minerals. The effects of convergence rate and age of the subducting slab as well as grain size of the minerals on the dehydration of the subducting slab and behavior of the expelled water are evaluated. The water solubility of the oceanic crust measured from the laboratory experiments is considered for modeling dehydration of the oceanic crust. The model calculations show most of the hydrated minerals in the oceanic crust is dehydrated by a depth of 100 km and the effects of the convergence rate and age of the subducting slab on the dehydration of the subducting slab and behavior of the expelled water are not significant. The larger grain size allows faster porous flow of the expelled water through the oceanic crust, mantle wedge and overlying continental crust and reduces the volume fraction of the expelled water there. The developed technique will be used for future studies on arc volcanism and has a potential implication for the other fields such as seismic tomographic study.

The Effect of a Au Based Bonding Agent Coating on Non-Precious Metals-Ceramic Bond Strength (비귀금속 합금에 적용한 Au Based Bonding Agent가 금속-도재 결합에 미치는 영향)

  • Lee, Jung-Hwan;Ahn, Jae-Seok
    • Journal of dental hygiene science
    • /
    • v.9 no.4
    • /
    • pp.405-412
    • /
    • 2009
  • The purpose of this study investigated the effect of Au coating on adhesion between porcelain matrix and metal substructure interface. Titanium, Ni-Cr alloy and Co-Cr alloy are well known as proper metal for the dental restorations. The success of a porcelain fused to metal (PFM) restoration depends upon the quality of the porcelain-metal bond. However, adhesion between dental alloys and porcelain is related to diffusion of oxygen during ceramic firing. The excessive oxidized layers make hard adhesion between dental alloy and ceramic. Ni-Cr and Co-Cr specimens were divided into test and a control group and Titanium specimens were divided into three test groups and a control group. Each group had 20 specimens. The adhesion characteristics of porcelain and metal with Au coating layer and without Au coating layer were observed with scanning electron microscopy(SEM). The adhesion was evaluated by a biaxial flexure test and volume fraction of adherent porcelain was determined by SEM/EDS analysis. Result of this study suggest that Au coating layer is effective barrier to diffuse oxide layer completely protect non-precious alloys from oxidation during the porcelain firing. The SEM photomicrographs of cross-section specimens showed a smooth interface between Au coating layer and metals and porcelain which suggested proper chemical bonding, and no gap, porosity were observed. The mode of failure was mainly adhesive for Ti tested specimens, but mixed failures with adhesive and cohesive were observed in Ni-Cr and Co-Cr specimens. The adhesion between non-precious metals and porcelain would not be improved by Au coating agent. However, It is suggested that the continuous study is required further investigation and development.

  • PDF

3-D Free Vibration Analysis of Exponential and Power-law Functionally Graded Material(FGM) Plates (지수 및 멱 법칙 점진기능재료 판의 3차원 자유진동해석)

  • Lee, Won-Hong;Han, Sung-Cheon;Ahn, Jin-Hee;Park, Weon-Tae
    • Journal of the Computational Structural Engineering Institute of Korea
    • /
    • v.28 no.5
    • /
    • pp.553-561
    • /
    • 2015
  • The exponential and power law functionally graded material(FGM) theory is reformulated considering the refined shear and normal deformation theory. This theory has ability to capture the both normal deformation effect and exponential and power law function in terms of the volume fraction of the constituents for material properties through the plate thickness. Navier's method has been used to solve the governing equations for all edges simply supported plates on Pasternak elastic foundation. Numerical solutions of vibration analysis of FGM plates are presented using this theory to illustrate the effects of power law index and 3-D theory of exponential and power law function on natural frequency. The relations between 3-D and 2-D higher-order shear deformation theory are discussed by numerical results. Further, effects of (i) power law index, (ii) side-to-thickness ratio, and (iii) elastic foundation parameter on nondimensional natural frequency are studied. To validate the present solutions, the reference solutions are discussed.