• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.16 no.1
• /
• pp.877-887
• /
• 2015

We have proposed a new method for estimating the viscosity of the composite. In this paper, we have developed a device for measuring the injection mold cavity pressure. This makes it possible to verify the accuracy of the viscosity in CAE D/B in real time by measuring the melt pressure in the mold, and comparing this with the simulated pressure from the CAE analysis. Materials used in this study is a PP(Polypropylene), PP/LGF30%(Polypropylene/long glass fiber 50% composite) and PA66/LGF50%(Polyamide 6,6/long glass fiber 50% composite). The viscosity data for PP and PP long fiber composite have already been built, but the one for PA66 long-fiber composite does not exist because it is a newly developed material. Thus we obtained the viscosity curve of PA66/LGF50% by this system. Then, the viscosity curves from conventional viscometer were also compared with the viscosity obtained by the our method. And, we proved the accuracy of the CAE data of PP. In case of PP/LGF50% which is highly viscous and complex material, we improved the existing CAE data.because there was a difference between the measuring data and the CAE data.

• Journal of Pharmaceutical Investigation
• /
• v.37 no.3
• /
• pp.137-148
• /
• 2007

Using a strain-controlled rheometer [Rheometrics Dynamic Analyzer (RDA II)], the steady shear flow properties of a semi-solid ointment base (vaseline) have been measured over a wide range of shear rates at temperature range of $25{\sim}60^{\circ}C$. In this article, the steady shear flow properties (shear stress, steady shear viscosity and yield stress) were reported from the experimentally obtained data and the effects of shear rate as well as temperature on these properties were discussed in detail. In addition, several inelastic-viscoplastic flow models including a yield stress parameter were employed to make a quantitative evaluation of the steady shear flow behavior, and then the applicability of these models was examined by calculating the various material parameters (yield stress, consistency index and flow behavior index). Main findings obtained from this study can be summarized as follows : (1) At temperature range lower than $40^{\circ}C$, vaseline is regarded as a viscoplastic material having a finite magnitude of yield stress and its flow behavior beyond a yield stress shows a shear-thinning (or pseudo-plastic) feature, indicating a decrease in steady shear viscosity as an increase in shear rate. At this temperature range, the flow curve of vaseline has two inflection points and the first inflection point occurring at relatively lower shear rate corresponds to a static yield stress. The static yield stress of vaseline is decreased with increasing temperature and takes place at a lower shear rate, due to a progressive breakdown of three dimensional network structure. (2) At temperature range higher than $45^{\circ}C$, vaseline becomes a viscous liquid with no yield stress and its flow character exhibits a Newtonian behavior, demonstrating a constant steady shear viscosity regardless of an increase in shear rate. With increasing temperature, vaseline begins to show a Newtonian behavior at a lower shear rate range, indicating that the microcrystalline structure is completely destroyed due to a synergic effect of high temperature and shear deformation. (3) Over a whole range of temperatures tested, the Herschel-Bulkley, Mizrahi-Berk, and Heinz-Casson models are all applicable and have an almostly equivalent ability to quantitatively describe the steady shear flow behavior of vaseline, whereas the Bingham, Casson,and Vocadlo models do not give a good ability.

• Journal of Applied Biological Chemistry
• /
• v.54 no.1
• /
• pp.1-6
• /
• 2011

${\gamma}$-PGA(poly-${\gamma}$-glutamic acid) is an unusual anionic polypeptide that is made of D- and L-glutamic acid units connected by amide linkages between ${\alpha}$-amino and ${\gamma}$-carboxylic acid groups. ${\gamma}$-PGA has been isolated from many kinds of organisms. Many Bacillus strains produce ${\gamma}$-PGA as a capsular material of an extracellular viscous material. It is safe for eating as a viscosity element of fermented soybean products such as Chungkookjang and Natto. It is biodegradable, edible and nontoxic toward humans and the environment and its molecular weight varies from ten thousand to several hundred thousand depending on the kinds of strains used. Therefore, potential applications of ${\gamma}$-PGA and its derivatives have been of interest in the past few years in a broad range of industrial fields such as food, cosmetics, medicine, water-treatment, etc. In this study, a bacterium, Bacillus subtilis GS-2 isolated from the Korean traditional seasoning food, Chungkookjang could produce a large amount of ${\gamma}$-PGA with high productivity and had a simple nutrient requirement. Based on carbon utilization pattern and partial 16S rRNA sequence analysis, the GS-2 strain was identified as B. subtilis. The determination of purified ${\gamma}$-PGA was confirmed with thin layer chromatography (TLC), high performance liquid chromatography (HPLC), fourier transform infrared (FT-IR) spectra, and $^1H$-nuclear magnetic resonance ($^1H$-NMR) spectroscopy.

• Journal of Wetlands Research
• /
• v.24 no.4
• /
• pp.320-330
• /
• 2022

The Hangang river estuary, which is a natural estuary without structures such as estuary barrage, is an ecological pathway connecting the sea and rivers. Accordingly, Hangang river estuary has various species, and there is very valuable. Sediment classification in Hangang river estuary is three-dimensionally and diversely is distributed. Sediment classification in Hangang river estuary is also sensitively changed according to various factors such as climate change and river development. It is typically cause to landform and to develop a compound cross section. In Janghang wetland, the plant success is remarkable according to the morphological change at river bed. The purpose of this study is to identify the mechanism of wetland formation based on the observation on-site. As a result of the observation, Janghang wetland where was artificially created, has been grown according to the river bed change based on the flow rate and the plant success. The viscous surface layer material(fine grains of wash rod properties), which is not the main material(sand) of the river bed, but sub-materials of river bed, jas been settled on the pioneer plants(bolboschoenus planiculmis, etc.). It is an important role in the growth of a compound cross section and a wetland. After the wetland developed to the compound cross section, it is observed that the pioneer plants are transferred to other plant species.

• Journal of the Korean Geotechnical Society
• /
• v.22 no.9
• /
• pp.37-43
• /
• 2006

Dynamic numerical analysis of geotechnical problems requires a way to simulate the decrease of energy as the domain of interest gets larger. This phenomenon is usually referred to as radiation damping or geometric attenuation and it is distinguished from material damping in which elastic energy is actually dissipated by viscous, hysteretic, or other mechanism. The fact that the domain of analysis in numerical modeling must be chosen, however, causes a need for special attention at the boundary. This observation leads directly to the idea of determining the dynamic response of the interior region from a finite model consisting of the interior region subjected to a boundary condition which ensures that all energy arriving at the boundary is absorbed. This paper presents a simple methodology to simulate transmitting boundaries condition using viscoelastic infinite elements within the recently developed "OpenSees" finite element code. The methodology used here provides that the level of absorption for traveling waves is efficient enough for practical purposes, but unsatisfactory for the case of sharp incident angles. The effectiveness of the infinite elements for the absorption of incident waves at boundaries is evaluated via example analysis.

• Applied Biological Chemistry
• /
• v.40 no.6
• /
• pp.525-530
• /
• 1997

The changes in rheological properties of egg white stored in biodegradable package were investigated by pH change, failure stress and stress relaxation curve, and compared with control without package and complex PE. Initial pH of egg white stored in biodegradable package changed from 8.39 to 9.3 after 8 day storage, showing similar trend in pH change as that of control without package. Initial 14.25 N failure stress was changed into 6.76 N in biodegradable package and 9.31 N in control. Complex PE, having a relatively low gas permeability compared to biodegradable package, showed less pH changes from 8.30 to 8.81, but a greater decrease in failure stress into 5.29 N, indicating more deteriorating effect in complex PE package. Viscoelastic constants, such as elastic constant and viscous constant, obtained from stress-relaxation curve by three element Maxwell model were not significantly different between control and biodegradable package, but eggs stored in complex PE showed greater changes during storage. Therefore, the permeability seems to be the major factors to influence the rheological properties of egg and biodegradable packaging materials showed a potential substitute package for eggs.

• Applied Biological Chemistry
• /
• v.50 no.2
• /
• pp.87-94
• /
• 2007

A bacterium which has high enzymatic activities such as amylase, cellulase and protease was isolated from Korean traditional soybean food, doenjang. The isolated bacterium was identified to Bacillus subtilis HS25 by the test of morphological and biochemical properties according to Bergey's Manual of Systematic Bacteriology and API 50 CHL kit, and by the 16S rDNA sequence. The isolated B. subtilis HS25 had a potent antibacterial activity against food born causative or pathogenic bacteria. B. subtilis HS25 is endospore forming cell and contained flagella and abundant viscous material at the out layer of cell wall. It was rod type bacterium $(0.5{\sim}0.8{\times}3{\sim}5{\mu}m)$ having biochemical characteristics such as gram staining(+), catalase(+), oxidase(-) and hydrolysis of esculin(+). The optimal medium compositions for production of antibacterial substance in the B. subtilis HS25 were 1% of soluble starch, 0.5% of yeast extract, 0.5% of peptone and 0.05% of MgCl$_2{\cdot}6H_{2}O$. The optimum temperature and pH of the growth of the B. subtilis HS25 was 35$^{\circ}C$ and pH 7.5, respectively. The antibacterial activity was more high in neutral to a little alkaline pH (6.5-10.5) than in acidic pH. The optimal shaking speed to grow and to produce antibacterial substance of the B. subtilis HS25 was 160${\sim}$200 rpm. The optimal culture time for antibacterial activities of the bacterium were shown to be in the range of 12-36 hr.

• Elastomers and Composites
• /
• v.39 no.1
• /
• pp.12-22
• /
• 2004

The plasma surface modification of natural rubber vulcanizate was carried out using chlorodifluoromethane in a radio-frequency (13.56 MHz) electrodeless bell type plasma reactor. The modification was qualitatively assessed by Fourier transform infrared spectroscopy. The frictional force of the plasma-treated surface was found to decrease with the time of plasma treatment. An increase in the surface polarity, as evidenced by the decrease in contact angle of a sessile drop of water and ethylene glycol on the natural rubber vulcanizate surface, was noted with the plasma modification. In the case of similar plasma treatment of glass surface, only a reduction in the polarity was observed. The use of geometric and harmonic mean methods was found to be useful to evaluate the London dispersive and specific components of surface free energy. Irrespective of the method used for evaluation, an increasing trend in the surface free energy was noted with increasing plasma treatment time. However, the harmonic mean method yielded comparatively higher values of surface free energy than the geometric mean method. The plasma surface modification was found to vary the frictional coefficient by influencing the interfacial, hysteresis and viscous components of friction in opposing dual manners.

• Journal of the Microelectronics and Packaging Society
• /
• v.16 no.3
• /
• pp.39-43
• /
• 2009

In this paper, the flow characteristics of underfill material driven by capillary action between flip-chip and substrate were investigated. Also, the effects of viscosity level and dispensing point of underfill on flow characteristics were investigated. Flip chip package size was $5mm{\times}5mm{\times}0.65^tmm$, the diameter of solder bump was 100 ${\mu}m$, and the pitch was 150 ${\mu}m$. It was full grid area-array type with 1024 I/Os. The glass substrate was used and the gap between the chip and substrate was 50 ${\mu}m$. For the experimental study, three different underfills with different viscous properties($2000{\sim}3700$ cps), and two different types of dispensing methods(center dot and edge dot) were used. The flow characteristics and filling time of underfill were investigated by using CCD camera. The results show that the edge flow was faster than center flow due to the edge effect, which was caused by the resistance of solder bumps. In case of edge dot dispensing type, the filling time was faster due to the large edge effect, compared to center dot dispensing type. Also, it was found that the underfill flow was faster and the filling time decreased as the viscosity level of underfill was decreased.

• Journal of Korean Tunnelling and Underground Space Association
• /
• v.24 no.6
• /
• pp.465-481
• /
• 2022

Rock grouting is important to improve the waterproof efficiency and mechanical strength of rock medium with joint for utilizing the underground rock space such as tunnel. The grouting materials typically has been used the cement materials, which represent Bingham fluid model. This model can express the relationship of viscosity and yield strength. In addition, it is dependent with elapsed time. The grouting injection performance can be deteriorated with an increase of viscosity and yield strength in the grouting process if the time dependence is ignored. Therefore, in this study, the characteristics of viscosity and yield strength were investigated according to water-cement ratio and time dependence in the laboratory test. Numerical simulation was carried out to investigate the grouting performance according to the time dependence of characteristics in terms of the viscosity model. Given the results, the grouting injected distance and cumulative grout volume were significantly decreased when the time dependence of grouting material was considered. This study, considering the characteristics according to the time dependence of viscosity and yield strength, will be meaningful to the design of grouting injection in field applications.