• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.3
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• pp.381-389
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• 2001

The objective of this paper is to evaluate the fracture resistance characteristics of SA508 Cl.1a to SA508 Cl.3 welds manufactured for the reactor coolant loop piping system of nuclear power plants. The effect of the crack plane orientation to the welding process orientation and the preheat temperature on the fracture resistance characteristics were discussed. Results of the fracture resistance test showed that the effect of the crack plane orientation to the welding process orientation of the fracture toughness is significant, while that of preheat temperature on the fracture toughness is negligible. The micro Vickers hardness test, the metallographic observation and the fractography analysis were conducted to analyse the crack jump phenomenon on the L-R crack plane orientation in the multi-pass welding zone. As these results, it is shown that the crack jump phenomenon was produced because of the inhomogeneity between welding beads and the crack plane orientation must be considered for the safety of the welding zone in the piping system.

• Journal of the Korean Society for Heat Treatment
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• v.23 no.6
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• pp.301-308
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• 2010

A steel with chemical composition, 0.22% C, 0.25% Si, 1.26% Mn, 0.22% Cr, 0.04% Ti, 0.0042% B, and a microstructure of ferrite and spheroidized cementite has been press-formed to automotive center pillar followed by local-hardening heat-treatment. Hardness, tensile properties, fractography, microstructure and surface roughness of local-hardening heat-treated automotive center pillar have been examined. The directly heated and quenched area had fully martensitic structure with Vickers hardenss in the range of 500 to 510. The heat affected area close to the directly heated area showed dual-phase structure of ferrite and martensite. The width of the heat-treated and heat-affected areas after the local-hardening heat treatment was ranging from 32 mm to 50 mm. The surface of the local-hardening heat-treated center pillar revealed some temper color as a consequence of the oxidation during the heat treatment, but the surface roughness was not affected by the local-hardening heat treatment.

• Journal of the Korean Ceramic Society
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• v.31 no.5
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• pp.552-560
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• 1994

A composite of TiB2-Al2O3 system was successfully prepared from a mixture of TiO2, B2O3, and Al by self-propagating high temperature synthesis (SHS) with a novel characteristic, utilizing the internal oxidation heat of aluminium metal of the mixture, instead of by a conventional technique, externally heating a mixture of Ti, B and Al2O3. From a mixture with B/Ti molar ratio of =2.0, pure two phases of TiB2 and $\alpha$-Al2O3 with good crystallinity and small, uniform sizes were formed. However, when the B/Ti molar ratio of the mixture goes to a value less than 2.0, in addition to the above main minerals, a small smounts of metastable phases such as TiB and Ti3B4 were formed. It was found that about 60%, the optimum green density of compacts gave their highest reaction rate and temperature during SHS process. TiB2-Al2O3 system composite with B/Ti molar ratio of =2.0 could be pressurelessly sintered even at 190$0^{\circ}C$ under Ar gas flows without any addition of sintering aids, showing their good properties such as 91.2% in relative density, 2750 kgf/$\textrm{mm}^2$ in Vickers hardness and 2620 kgf/$\textrm{cm}^2$ in flexural strength.

• Journal of the Korean Ceramic Society
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• v.45 no.12
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• pp.815-820
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• 2008

The microstructure and mechanical properties of $TiB_2/Si$ nanocomposites based on the Ti-Si-B system, consolidated by spark plasma sintering of mechanically alloyed activated nanopowders, have been characterized. Mechanical Alloying was carried out in a planetary ball mill for 180 min with 350 rev $min^{-1}$. The powders were pressed in vacuum at a pressure of 60 MPa, generating a maximum temperature in the graphite mould of $1400^{\circ}C$. Analysis of the synthesized nanocomposites by SEM, XRD and TEM showed them to consist of $TiB_2$ second phase, sub-micron in size, with no third phase. Composites consolidated from powders mechanically alloyed from an initial elemental powder mix of 0.3 mol Si, 0.7 mol Ti, and 2.0 mol B achieved the best relative density (97%) and bending strength (774 MPa); the highest Vickers hardness of 14.7 GPa was achieved for the 0.1-0.9-2.0 mol starting composition.

• Journal of the Korean Ceramic Society
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• v.50 no.3
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• pp.180-185
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• 2013

We investigated the characteristics of hot-pressed pure yttria ceramics, and annealed them in an oxidation atmosphere. Regardless of the heat treatment in the oxidation atmosphere, XRD analysis showed that all the samples had a $Y_2O_3$ phase without structural change. Even though the color variation of the hot-pressed $Y_2O_3$ ceramics was due to the sintering temperatures, the oxidation process turned the color of the $Y_2O_3$ ceramics into white. The color change during oxidation treatment appears to be related to oxygen defects. In addition, oxygen defects also affected the weight change and microstructure of the $Y_2O_3$ ceramics. The $Y_2O_3$ ceramic sintered at $1600^{\circ}C$ had a $5.03g/cm^3$ density, which is close to the theoretical density of $Y_2O_3$. As the sintering temperature increased, small homogeneous grains grew to large grains which affected the Vickers hardness. $Y_2O_3$ ceramics hot-pressed at $1600^{\circ}C$ and annealed at $1200^{\circ}C$ had a flexural strength of 140MPa.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.12
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• pp.1107-1114
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• 2008

This paper is aimed to understand the effect of different galvannealing temperatures on the frictional properties and Fe-Zn intermetallic phases of the galvannealed (GA) coatings on steel sheets. Their galvannealing treatments were conducted at 465, 505, 515 and $540^{\circ}C$ for about 10s in the additional heating furnace of an industrial continuous hot-dip galvanizing line. The mechanical and the frictional properties of the coatings were estimated using nanoindentation, nanoscratch, micro vickers hardness tests and flat friction tests, which were performed at contact pressures of 4, 20 and 80MPa. Also, the correlation between the microstructure and the frictional properties of the GA coatings were investigated by SEM observation for the cross-section of the GA coating after and before flat friction tests. The results showed that the mechanical and the frictional properties of the coatings are strongly dependent on their phase distributions and microstructure. Especially, in low contact pressure of 4MPa the frictional properties of the coatings were dependent on the surface phases and morphology, while in high contact pressure of 80MPa it was influenced by their mechanical properties based on the dominant phase distributions.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.19 no.3
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• pp.29-35
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• 2020

This paper studies the main parameters of tube-to-bar dissimilar material and shape friction welding for piping materials. The weldability of joint parts was investigated with respect to tensile tests, micro-Vickers hardness, the bond of area, and optical microstructure. The specimens are tested as-welded. Optimal welding conditions are n = 2000 rpm, HP = 50 MPa, UP = 100 MPa, HT = 5 sec, and UT = 10 sec when the metal loss (Mo) is 11 mm. Moreover, the same two materials for friction welding are strongly mixed with a well-combined structure of micro-particles without any molten material, particle growth, or defects. Therefore, the expected result of dissimilar material friction welding includes a reduction of cost and material in the welding process.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.14 no.12
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• pp.979-986
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• 2001

This paper was researched the effect of slurry stability on the mechanical and electrical property of the porcelain insulator with various raw materials such as feldspar, quartz, clay and l7wt% alumina. The slurry was fabricated after ball milling the mixed raw materials. Green compacts were made by the extrusion and were sintered at 1300$\^{C}$ for 60min in the tunnel kiln. All of the specimens were densified 96% of the theoretical density. The 3-point flexural strength($\sigma$$\_$B/) of the specimen stabilized slurry pH 7.8 was 1650 k9/㎠ and the vickers hardness(Hv) and the fracture toughness(K$\_$IC/) were 27.5 GPa and 2.2 MPa$.$m$\^$$\sfrac{1}{2}$/, respectively. The mechanical properties of the specimen stabilized slurry PH 9.3 were 1716 kg/㎠($\sigma$$\_$B/), 27.6 GPa(Hv) and 3.0 MPa$.$m$\^$$\sfrac{1}{2}$/(K$\_$IC/), respectively. The dielectric strength was increased from 8.3kV/mm to 13.2kV/mm as the increase of the slurry pH from 7.8 to 9.3. Therefore the physical properties of the specimen stabilized slurry pH 9.3 were improved.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.11 no.1
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• pp.53-60
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• 2015

This study was investigated to develop process technology of laser cladding with austenite stainless steel for Weld Inlay repair of dissimilar metal weld in reactor vessel in/outlet nozzles. Weld Inlay experiments were performed by laser cladding repair system consisting of common manipulator, laser apparatus and welding process scheduler, etc. Single pass welding experiments were conducted in order to obtain the optimum welding process parameters for filler wires of ER309L and Alloy 52M before multi-layer laser cladding. Based on the above obtained results, multi-layer laser cladding experiments were carried out, and welding qualities for weld specimens were estimated by PT, OM, SEM and EDS analysis. Consequently, it was revealed that multi-layer laser cladding on austenite stainless steel using filler wires of ER309L and Alloy 52M could be possible to meet ASME Code standard without any weld defect.

• Journal of the Korean Society of Industry Convergence
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• v.23 no.1
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• pp.73-81
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• 2020

This study analyzed the causes of failure of SCM435 bolts that fix the springs of automobile air brakes that have been fractured during use. The cause of failure was analyzed using SEM, EDS, metallogical microscope and Vickers hardness tester. In the fracture, the ratchet mark began at the outer boundary of crack origin, and the grains at crack origin were found to have clear intergranular corrosion. One SCM435 bolt was subjected to a stress of 398 MPa, it's a stress of about 80% of the fatigue limit. As a result of such a large applied stress, cracks occurred at the corrosion origin and were fractured. In order to prevent the SCM435 bolt from fracture, it is necessary to use the correct composition, the accuracy of heat treatment, preventing damage by external impact, preventing corrosion of the damage part by moisture, and introduction a compressive residual stress by peening.