• Proceedings of the KSME Conference
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• 2004.04a
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• pp.336-341
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• 2004

This research investigates the feasibility of ultrasonic microscope for nondestructive assessment of thermal degradation in artificially aged commercial Co-base superalloy, FSX414. This alloy has been used for high temperature structure applications such as stationary gas turbine blade and nozzle chamber in fossil plant. Microstructural change was found that the fine carbides became coarser and spheroidized in matrix as aging time increased. The leaky surface acoustic wave velocity gradually decreases by a maximum of 4.7% with increasing aging time up to 4,000hours. However, the longitudinal wave velocity has a little change. Also, it has a good correlation between leaky surface acoustic wave velocity and Vickers hardness. Consequently, LSAW can be used to examine the degree of degradation in thermally aged Co-base superalloy.

• Proceedings of the KSR Conference
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• 2005.11a
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• pp.344-349
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• 2005

Cast steels have been mainly in rod type couplers which connect railway vehicles. These components, as important members, are exposed to repeat to repeated stresses and impact loading during stop and departure service for a long tie. The coupler suffers fatigue crack initiations and demage that cause need to repair weldment due to these loading conditions. Therefore, the heat affected zone of cast steel couple in rod type were evaluated in view of metallurgical weld characteristics after repair welding at laboratory. The specimens with two different welding techniques were evaluated after several welding conditions and post-heat treatments. Micro-vickers hardness and tensile tests and microstructural observations were conducted on heat affected zone of the weldment according to repair weld and post-heat treatment.

• Journal of the Korean Ceramic Society
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• v.26 no.3
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• pp.409-415
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• 1989

Si3N4-TiN electro-conductive ceramic composites with 7wt% Al2O3＋3wt% Y2O3 or 5wt% MgO as sintering aids were fabricated by pressureless sintering at 1,80$0^{\circ}C$ for 1h. The 3pt. flexural strength, KIC and Vickers hardness were measrued in order to investigate the effects of TiN on the mechanical properties. Also oxidation behavior was observed by measuring the weight gain after exposure to air at 1,10$0^{\circ}C$ for 100h. the reaction products between Si3N4 and TiN was not detected by XRD and EDS. Mechanical properties of the composites were not influenced by the addition of TiN less than 30vol%, but oxidation resistance of the composites was rapidly decreased with the amount of added TiN.

• Journal of the Korean institute of surface engineering
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• v.35 no.2
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• pp.122-128
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• 2002

This study was conducted to synthesize the diamond like carbon films by plasma enhanced chemical vapor deposition (PECVD). The effects of gas composition on growth and mechanical properties of the films were investigated. A little amount of hydrogen or oxygen were added to base gas mixture of methane and argon. Methane dissociation and diamond like carbon nucleation were enhanced by installing negatively bias grid near substrate. The deposited films were indentified as hard diamond like carbon films by micro-Raman spectroscopy. The surface and fractured cross section of the films which were observed by scanning electron microscopy showed that film growth is very slow as about 0.3$\mu\textrm{m}$/hour, and relatively uniform with hydrogen addition. Vickers hardness of tungsten carbide (WC) cutting tool increased from about 1000 to 1600~1800 by deposition of DLC film, that of commercial TiN coated tool was about 1270. In cutting test of aluminum 6061 alloy, DLC coated cutting tool showed 1/3 or lower crater and flank wear than TiN coated or non-coated WC cutting tools.

• Proceedings of the KIEE Conference
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• 2003.07c
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• pp.1469-1471
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• 2003

The effect of heat treatment on torsion characteristics of high nitrogen steel wire has been studied by using torsion test, micro vickers hardness and scanning electron microscopy. After heat treatment at $600{\sim}700^{\circ}C$, torsion cycle was increased with increasing temperature. Especially, in case of high nitrogen steel wire heat treated at $650^{\circ}C$, torsion cycle was sharply increased. It is estimated that the cold-worked high nitrogen steel wire started to recrystallize around at $640^{\circ}C$ in air atmosphere.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.51-52
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• 2006

[ $Ti_{45}Zr_{38}Ni_{17}$ ] powders were thermally sprayed onto mild steel substrates in air and under a reduced pressure of argon. Several oxides were formed after thermally-spraying the mechanically-alloyed powders in air. After spraying in a reduced pressure of argon, the coating layers obtained from the gently mixed powders consisted of the elemental metals, but an amorphous phase primarily appeared in the thermally-sprayed mechanically-alloyed powders, which transformed into the icosahedral quasicrystal phase and a minor $Ti_2Ni-type$ crystal phase after annealing at 828 K. The Vickers hardness and the contact angle with pure water for the quasicrystal layers were about 7 GPa and $92^{\circ}$ respectively.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.24-25
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• 2006

High-Speed Centrifugal Compaction Process is one of slip-using compacting method originally developed for processing of oxide ceramics. In this study, we apply the HCP to ultra-fine (0.1 micron) WC powder. Organic liquid of heptane was chosen as dispersing media to avoid possible oxidation of WC. The mixing apparatus was a key to obtain dense compacts. Only the slips mixed by high energy planetary ball mill were packed up to 55% by the HCP, and sintered to almost full density at 1673 K without any sintering aids. This sintered compact marked Vickers hardness of Hv 2750 at maximum.

• Journal of Power System Engineering
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• v.10 no.1
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• pp.77-82
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• 2006

In this study, dissimilar friction welding were produced using 15mm diameter solid bar in chrome molybedenum steel(SCM440) to carbon steel(S45C) to investigate their mechanical properties and the relationship between the weld parameters and the nondestructive coefficients, such as AE counts and ultrasonic attenuation coefficient. The main friction welding parameters were selected to endure good quality welds on the basis of visual examination, tensile tests, Vickers hardness surveys of the bond of area and heat affected zone. The specimens were tested as-welded and post weld heat treated(PWHT). The tensile strength of the friction welded steel bars was increased up to 100％ of the S45C base metal under the condition of all heating time. The ductility of PWHT specimens is higher than as-welded.

• Journal of Welding and Joining
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• v.18 no.2
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• pp.184-184
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• 2000

In this study, the lap welding between austenitic stainless steel and carbon steel was carried out using arc spot welding process and weldability of welded specimens was estimated. From the tensile-shear strength test, micro Vickers hardness test, and microstructure observation, specimen of 6.5mm(hole of upper plate) showed the best results in terms of tensile-shear strength and nugget shape. And there was an unmixed zone in fusion boundary between the carbon steel base metal and bulk weld metal. This zone had very thin width with the hard microstructure. The shape of weld nugget in arc spot welding of dissimilar metal welds was predicted by searching thermal history of a weld joint through a three-dimensional finite element model. From the numerical analysis, predicted the shape of weld nugget showed good agreement with the experiment(Received August 24, 1999)

• Korean Journal of Materials Research
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• v.15 no.9
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• pp.608-612
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• 2005

Microstructure and mechanical properties of fibrous $A1_2O_3-(m-ZrO_2)/t-ZrO_2$ composite were investigated depending on the dimensional array. By the change of stacking arrangement of fibrous filaments, 2 and 3-dimensional fibrous composites were successfully obtained without bulk defects such as shrinkage cavity and cracks. The maximum mechanical properties were achieved In the 3-dimensional array composite, due to the fine fibrous and dense microstructure control, in which the values of vickers hardness, fracture toughness and bending strength were about 1507 Hv, $7.2MPa{\cdot}m^{1/2}$ and 650 MPa, respectively.