• 한국광학회지
• /
• 제28권6호
• /
• pp.339-345
• /
• 2017

기준 평면의 평면도는 간섭계 교정에서부터 반도체, 플랫 패널 디스플레이, 실리콘 기판에 필요한 기준면 제공 등에 매우 중요한 역할을 한다. 특히 기준 평면의 평면도 측정을 해외에서 수행해 올 경우 시간적인 지연과 함께 금전적인 손해가 크므로 국내에서 측정 기술을 구축할 필요가 있다. 본 논문에서는 국내에서 처음으로 절대 측정 방법인 three-flat test 방법을 사용해 기준 평면의 평면도를 정확하게 구하고 측정불확도를 계산하였다. Three-flat test는 간섭계를 사용하여 세 개의 기준 평면을 상호 비교 측정하여 얻은 결과에서 각 평면의 평면도를 정확하게 구하는 방법이다. Three-flat test 방법들 중 실험실에 구축된 장비로 실험 가능하며 간단한 계산 과정으로 낮은 측정불확도를 얻을 수 있는 Griesmann 방법을 적용하여 실험하였다. 그 결과, 세 광학 평면에 대한 평면도를 얻을 수 있었고, 측정불확도는 각 광학 평면에 대해 0.5 nm rms 이내의 신뢰 수준임을 확인하여 높은 수준으로 자체 평면도 측정이 가능함을 확인하였다.

• 한국정밀공학회지
• /
• 제26권8호
• /
• pp.72-78
• /
• 2009

We developed a line standards measurement system using an optical microscope and measured two kinds of line standards. It consists of three main parts: an optical microscope module including a CCD camera, a stage system with a linear encoder, and a measurement program for a microscopic image processing. The magnification of microscope part was calibrated using one-dimensional gratings and the angular motion of stage was measured to estimate the Abbe error. The threshold level in line width measurement was determined by comparing with certified values of a line width reference specimen, and its validity was proved through the measurement of another line width specimen. The expanded uncertainty (k=2) was about 100 nm in the measurements of $1{\mu}m{\sim}10{\mu}m$ line width. In the comparison results of line spacing measurement, two kinds of values were coincide within the expanded uncertainty, which were obtained by the one-dimensional measuring machine in KRISS and the line standards measurement system. The expanded uncertainty (k=2) in the line spacing measurement was estimated as $\sqrt{(0.098{\mu}m)^2+(1.8{\times}10^{-4}{\times}L)^2}$. Therefore, it will be applied effectively to the calibration of line standards, such as line width and line spacing, with the expanded uncertainty of several hundreds nanometer.

• 분석과학
• /
• 제26권2호
• /
• pp.125-134
• /
• 2013

본 연구는 액체크로마토그래피를 이용하여 사골농축액 시료 중에 23종의 아미노산 정량분석 시 발생할 수 있는 측정불확도를 평가하였다. 아미노산 분석에 관여하는 측정불확도 인자로 시료량, 최종 무게, 표준품 무게, 표준품 순도, 검정곡선, 회수율 및 재현성 등을 확인하였다. GUM(Guide to the expression of uncertainty in measurement)과 EURACHEM에 근거하여 측정불확도에 대한 수학적 계산 및 통계분석을 수행하였다. 사골농축액 시료 중 총 아미노산 함량은 36.18 g/100 g이었으며, 95% 신뢰수준(k, 2.05~2.36)에서 확장불확도는 3.81 g/100 g이었다. 측정불확도의 주요 요인은 분석시의 회수율과 반복성(25.2%) > 시료전처리(24.5%) > 검정곡선(24.0%) 순으로 나타났다. 따라서 아미노산 분석 시 불확도를 줄이기 위해서는 실험자들의 주의와 개인적인 숙력도의 향상이 요구된다.

• 대한기계학회논문집A
• /
• 제34권1호
• /
• pp.73-78
• /
• 2010

재료의 인장 물성 측정 불확도 평가가 수행되었다. 인장 물성 측정에 영향을 주는 불확도의 요인이 구분되어 분석되었고 인장 시험으로부터 측정되는 측정량, 즉 탄성계수, 항복 강도 그리고 인장 강도의 불확도 평가 모델이 본 연구에서 제시되었고 각 측정량에 대한 대응하는 수학적 모델과 측정치로부터 각 측정치의 감도계수를 계산함으로서 유도 되었다. 각 모델에 근거하여 ISO 6892에 따라 결정되는 SUS316LN의 실험적 데이터로부터 인장 물성의 불확도가 평가되었다.

• 한국생산제조학회지
• /
• 제24권5호
• /
• pp.496-501
• /
• 2015

In this study, calibration procedure of power assembly tools is suggested and methods are developed for calculating measurement uncertainty. Fist of all, the calibration of joint simulator bench (JSB) was carried out for maintaining traceability and the uncertainty components of JSB were analyzed. The influences of tool speed, tolerance, temperature and length of the adapter were examined by the torque measurement values through experiments. From this research, credibility for calibration results could be enhanced. This experimental results, being used as an effective tool for calibration of power assembly tools, will provide and improve the accuracy of the use of the power assembly tools.

• Journal of Mechanical Science and Technology
• /
• 제18권4호
• /
• pp.689-698
• /
• 2004

Uncertainties generated from the individual measured variables have an influence on the uncertainty of the experimental result through a data reduction equation. In this study, a performance test of a single stage axial type turbine is conducted, and total-to-total efficiencies are measured at the various off-design points In the low pressure and cold state. Based on an experimental apparatus, a data reduction equation for turbine efficiency is formulated and six measured variables are selected. Codes are written to calculate the efficiency, the uncertainty of the efficiency, and the sensitivity of the efficiency uncertainty by each of the measured quantities. The influence of each measured variable on the experimental result is figured out. Results show that the largest uncertainty magnification factor (UMF) value is obtained by the inlet total pressure among the six measured variables, and its value is always greater than one. The UMF values of the inlet total temperature, the torque, and the RPM are always one. The uncertainty percentage contribution (UPC) of the RPM shows th, lowest influence on the uncertainty of the turbine efficiency, but the UPC of the torque has the largest influence to the result among the measured variables. These results are applied to find the correct direction for meeting an uncertainty requirement of the experimental result in the planning or development Phase of experiment, and also to offer ideas for preparing a measurement system in the planning phase.

• 설비공학논문집
• /
• 제12권11호
• /
• pp.1012-1019
• /
• 2000

A proficiency test is one of programs which Korea Research Institute of Standards and Science(KRISS), as national metrology institute, is putting in operation for the mutual recognition arrangement. The Fluid Flow Group of KRISS evaluated the measurement capability for liquid flowmeter calibrator of the national calibration and test organizations. The uncertainty of national standard system was estimated in accordance with Guide to The Expression of Uncertainty in Measurement (ISO), and the turbine flowmeter, which was used for the round-robin test as a reference flowmeter, was characterized. The round-robin tests with the turbine flowmeter package were carried out in 1995 and 1999. The test results of the organizations and those of KRISS agreed within $\pm0.2$%. It is found thus that the organizations have the traceability of the national standard for liquid flow measurement.

• 한국식품과학회지
• /
• 제35권6호
• /
• pp.1053-1059
• /
• 2003

분석 중 소실되기 쉬운 야채음료의 비타민 C 함량을 HPLC를 이용하여 측정하였으며, 불확도인자로서 표준품의 무게, 순도, 분자량, 희석 등과 시료의 무게, 검정곡선, 회수율 및 정밀성 등이 작용하였다. 이러한 미심쩍음 정도와 더불어 계통오차와 우연오차 등 일련의 과정을 GUM(Guide to the expression of Uncertainty in Measurement)과 EURACHEM에 근거하여 수학적 처리 및 통계방법을 이용하여 측정불확도를 추정하였다. 추정방법은 각각의 인자들에 대하여 A-type또는 B-type으로 산출된 표준불확도 값을 합성하여 합성표준불확도를 산출하고, 확장불확도는 유효자유도로 산출된 포함인자를 곱하여 계산하였다. 야채와 과일이 혼합된 음료 중 비타민 C 함량은 27.53mg/100g이었으며, 포함인자(2.06)를 곱한 확장불확도는 0.63mg/100g로서 95% 신뢰도구간에서의 비타민C의 결과는 $27.53{\pm}0.63mg/100g$(95% 신뢰도 구간)과 같이 수치화하여 표현하였다. 비타민 C 분석의 경우 HPLC를 이용한 시료 분석의 회수율 및 정밀성(33%), 표준품 순도(23%), 표준용액 희석시(18%), 표준품 무게(10%), 시료 측정시(10%), 검정곡선(6%) 순으로 불확도를 추정할 수 있었다. 또한, 이를 통해서 시험원의 분석과정 중 불확도가 높게 산출된 실험과정에 대해서는 좀더 세심한 주의가 요구되며, 시료의 반복실험 시 재현성 있는 결과가 산출될 수 있도록 숙련도를 높일 필요가 있다.

• 한국연초학회지
• /
• 제23권1호
• /
• pp.45-52
• /
• 2001

This study was carried out to evaluate the uncertainty in the analysis of total alkaloids and reducing sugar content in flue-cured tobacco. The sources of uncertainty associated with the analysis of total alkaloids and reducing sugar were the weighing of sample, the preparation of extracting solution, the addition of extracting solution into the sample, the preparation of standard solution, the precision of calibration curve for standard solution, the reproducibility of analysis, and the determination of water content in tobacco, etc. For the calculating uncertainties, Type A of uncertainty was evaluated by the statistical analysis of a series of observation, and Type B by the information based on supplier’s catalogue and/or certificated of calibration. It was shown that the main source of uncertainty was caused by the calibration curve of standard solution, the reproducibility of analysis, the volume measurement of 1$m\ell$, and the purity of nicotine reference material in the preparation of standard solution. The uncertainty in the addition of extracting solution, the sample weighing, the volume measurement of 100$m\ell$, and the determination of water content of tobacco contributed relatively little to the overall uncertainty. The expanded uncertainty of total alkaloids and reducing sugar in flue-cured tobacco at 95% level of confidence was $\pm$0.12% and $\pm$0.54%, respectively.

• 한국수자원학회:학술대회논문집
• /
• 한국수자원학회 2005년도 학술발표회 논문집
• /
• pp.1538-1542
• /
• 2005

This study is to secure more accurate data of the discharge on the measurement by gaining a reliable hydrological data through the comparison the present method of measuring them and the other way that is based ISO. This study suggests the applicable measurement method of the discharge that has reliance through general elements and the analysis of uncertainty by comparing and assaying the data of the Hyung San River that is measured by the present standard. The result of this study makes us realize that we should complement the measurement method of the discharge securing the reliable and accurate hydrological data Hydrological data is very important things to perform domestic river works or install some structure in river or coast. Securing reliable and accurate hydro-data and making a thesis should go on in other to do any construction in river or coast.