• 제목/요약/키워드: Ultrasonic dispersion

검색결과 165건 처리시간 0.038초

초음파 분산을 이용한 Epoxy-Organoclay 나노콤포지트 구조적 그리고 유전특성에 관한 연구 (Structural and Dielectric Properties of Epoxy-Organoclay Nanocomposites using Power Ultrasonic Dispersion)

  • 박재준
    • 전기학회논문지
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    • 제57권9호
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    • pp.1572-1578
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    • 2008
  • The effect of the organoclay_10A nanoparticles on the DSC and Structural and Dielectrics Properties(1Hz-1MHz) for epoxy/Organoclay_10A Nanocomposites has been studied. Dielectric properties of epoxy-Organoclay nanocomposites were investigated at 1, 3, 5, 7, 9 filler concentration by weight. Epoxy nanocomposites samples were prepared with good dispersion of layered silicate using power ultrasonic method in the particles. As structural analysis, the interlayer spacing have decreased with filled nanoparticles contents increase using power ultrasonic dispersion. The maximum increase interlayered spacing was observed to decease for above 5wt% clay loading. The other hand, as decrease with concentration filler of the layered silicate were increased dispersion degree of nanoparticles in the matrix. The interesting dielectric properties for epoxy based nanocomposites systems are attributed to the large volume fraction of interfacesin the bulk of the material and the ensuring interactions between the charged nanoparticle surface and the epoxy chains.

Evaluation of Elastic Properties of Anisotropic Cylindrical Tubes Using an Ultrasonic Resonance Scattering Spectroscopy

  • Kim, Jin-Yeon;Li, Zheng
    • 비파괴검사학회지
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    • 제30권6호
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    • pp.548-557
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    • 2010
  • An ultrasonic resonance scattering spectroscopy technique is developed and applied for reconstructing elastic constants of a transversely isotropic cylindrical component. Immersion ultrasonic measurements are performed on tube samples made from a boron/aluminum composite material to obtain resonance frequencies and dispersion curves of different guided wave modes propagating in the tube. Theoretical analysis on the acoustic resonance scattering from a transversely isotropic cylindrical tube is also performed, from which complete backscattering and resonance scattering spectra and theoretical dispersion curves are calculated. A sensitive change of the dispersion curves to the elastic properties of the composite tube is observed for both normal and oblique incidences; this is exploited for a systematic evaluation of damage and elastic constants of the composite tube samples. The elastic constants of two boron/aluminum composite tube samples manufactured under different conditions are reconstructed through an optimization procedure in which the residual between the experimental and theoretical phase velocities (dispersion curves) is minimized.

압전체를 이용한 약품 분사용 초음파 분사 노즐 시스템 (Ultrasonic Spray Nozzle System with Piezoelectric Device for Chemicals Dispersion)

  • 고재석;김용현;김형수;조순행;최승철
    • 마이크로전자및패키징학회지
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    • 제10권4호
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    • pp.65-71
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    • 2003
  • 압전 세라믹스를 이용하여 약품 분사용 초음파분사 노즐을 제작하였다. 정수장의 혼화 공정에 사용되는 약품(응집제)의 고효율 분산을 위해 분사 노즐을 설계하였으며 압전세라믹을 최적화하였다. 제작된 초음파 약품 분사 노즐을 패키징하여 정수장의 약품 혼화 과정에 적용하여 약품사용의 고 효율화와 사용량 저감을 위한 연구를 진행하였다. 압전체는 실리콘으로 마감처리를 하였으며 Al으로 패키징하였다. 본 초음파 분사 노즐 시스템을 적용하여 혼화지에 실험한 결과 약품의 순간 혼화를 촉진시키는 기술로 투입 약품량을 저감시킬 수 있을 것으로 판단된다. 초음파 발진 약품 분사시, 무발진과 비교하여 대장균 제거 효율에서 현저하게 높아졌다.

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Mechanical Properties of Vapor Grown Carbon Fiber/Epoxy Nanocomposites With Different Dispersion Methods

  • Khuyen, Nguyen Quang;Kim, Byung-Sun;Kim, Jin-Bong;Lee, Soo
    • 한국응용과학기술학회지
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    • 제24권3호
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    • pp.264-271
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    • 2007
  • Effect of dispersion methods for Vapor Grown Carbon Fibers (VGCF) in epoxy caused the change in mechanical properties of VGCF/epoxy nanocomposites, such as tensile modulus and tensile strength. The influence of VGCF types - atmospheric plasma treated (APT) VGCF and raw VGCF - and their contents was discussed in detail. Treating VGCF with atmospheric plasma enhanced the surface energy, therefore improved the bonding strength with epoxy matrix. Two different methods used to disperse VGCF were ultrasonic and mechanical homogenizer methods. When using dispersion solutions, the VGCF demonstrated good dispersion in ethanol in both homogenizer and ultrasonic method. The uniform dispersion of VGCF was investigated by scanning electron microscopy (SEM) which showed well-dispersion of VGCF in epoxy matrix. The tensile modulus of raw VGCF/epoxy nanocomposites obtained by ultrasonic method was higher than that of one obtained by homogenizer method. APT VGCF/epoxy nanocomposites showed higher tensile strength than that of raw VGCF/epoxy nanocomposites.

Homogenizer+Ultrasonic을 이용한 Epoxy-Layered Silicate Nanocomposites의 구조적, 열적, 전기적 특성연구 (Morphology, Thermal, Electrical Properties for Epoxy-Layered Silicate Nanocomposites using Homogenizer +Ultrasonic Dispersion Method)

  • 박재준;엄지용;이창훈;김민규;백관현
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.287-288
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    • 2008
  • 에폭시-층상실리케이트 나노콤포지트의 균질분산과 층상실리케이트내로 침투되는 박리정도를 향상시키기 위해 친환경적 분산기법인 물리적방법으로 Homogenizer와 Power Ultrasonic를 적용한 기법을 실시하였다. Homogenizer의 최적속도를 얻기 위해 분산시킨 나노콤포지트의 박리정도, 유리천이온도를 구할 수 있었고, Homogenizer와 Ultrasonic을 동시에 적용하여 최적시간을 구하기 위해 적용된 나노콤포지트를 절연파괴 강도의 Weibull Plots을 통하여 판단할 수 있는 좋은 결과를 얻을 수 있었다.

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분산법이 무전해 Ni-CNT 복합도금막 형성에 미치는 영향 (Effect of Dispersion Method on Formation of Electroless Ni-CNT Coatings)

  • 배규식
    • 반도체디스플레이기술학회지
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    • 제13권3호
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    • pp.51-55
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    • 2014
  • Ni-CNT(Carbon Nanotubes) composite coating is often used for the surface treatment of mechanical/electronic devices to improve the properties of the Ni coating. For the Ni-CNT coating, the dispersion of CNT fibers is a critical process. In this study, ultrasonic treatment instead of the conventional ball milling was attempted as a dispersion method for the electroless Ni-CNT coating. SEM-EDX analysis was performed and contact angle, sheet resistance, and micro-hardness were measured. Results showed that the ultrasonic treatment was comparable to the ball milling, as a dispersion method, but the difference was negligible. However, combined ball milling and ultrasonic treatment(double treatment) showed much improved micro-hardness value, above 350Hv(close to the value obtained by the Ni-CNT electroplating). In addition, electroless Ni-CNT(double-treated) coatings formed on the thin Ni film deposited by the electroless plating(double coating) showed better mechanical properties. Thus, double treatment and double coating are suggested as an improved electroless Ni-CNT coating method.

압전체를 이용한 약품 분사용 초음파 분사노즐 시스템 (Ultrasonic Spray Nozzle System with Piezoelectric Device for Chemicals Dispersion)

  • 고재석;김용현;최승철
    • 한국마이크로전자및패키징학회:학술대회논문집
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    • 한국마이크로전자및패키징학회 2003년도 기술심포지움 논문집
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    • pp.278-281
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    • 2003
  • A new type of ultrasonic spray nozzle was fabricated with piezoelectric devices. The spray nozzle was designed for the chemicals dispersion in the water purification bath. The piezoelectric properties in ultrasonic spray nozzles were optimized for the better dispersion of chemicals for purification process. Ultrasonic spray nozzle was packaged in metal case with silicone resin for the water proof application.

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Oil in Water 에멀전에서 오일 입자 크기가 분산 안정성에 미치는 영향 (Effect of oil particle size on dispersion stability in oil in water emulsion)

  • 황보선애;추민철;문창권
    • 한국입자에어로졸학회지
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    • 제13권3호
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    • pp.133-139
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    • 2017
  • In this paper, we proposed an emulsification method without using an emulsifier and investigated the effects of particle size distribution in fluids on dispersion stability. Surfactant-free oil in water emulsion was prepared with 1 % (w/w) of olive oil by using high speed agitation, high pressure and ultrasonic dispersion methods. The particle size, microscopic observation, and dispersion stability of each sample were evaluated and dispersion stability according to various dispersion methods was compared. As a result, the emulsion dispersed by the ultrasonic dispersion method showed the smallest particle size and uniform distribution of $0.07{\sim} 0.3{\mu}m$ and was the most stable in a 7 days stability evaluation. In the above experiment, four olive oil emulsions having different particle sizes were prepared using ultrasonic dispersion technology that was capable of producing stable emulsions. The dispersion stability of each samples with oil droplet sizes of (A) 0.1 to $0.5{\mu}m$, (B) 0.3 to $4{\mu}m$, (C) 1 to $10.5{\mu}m$ and (D) 2 to $120{\mu}m$, was observed for 7 days, and the relationship between the stability and performance was studied. Emulsion (A) with particle size less than $0.5{\mu}m$ displayed the dispersion stability showing below 5 % change in a 7 days stability evaluation. In the case of (B), (C), and (D) that had larger particle than $0.5{\mu}m$, the changes of dispersion stability were 10 %, 13 % and 35 % respectively. From these results, it was proved that dispersion stability of emulsion with uniform particle size of $0.5{\mu}m$ or less was confirmed to be very stable.

수성 폴리머 도료를 이용한 초음파 스프레이 공정으로 형성된 폴리머 절연층 미세구조 특성 (Morphology Characteristics of Insulating Laser based on Aqueous Polymer Resin Fabricated by Ultrasonic Spray Coating Process)

  • 유정모;박채원;엄현진
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2016년도 추계학술대회 논문집
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    • pp.136-136
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    • 2016
  • Commonly used oil-based polymer resin has environmental and safety issues. Many researches for replacing the harmful solvent-borne resins to water-borne resins have been investigated to purify harmful environmental resources and follow the export and import of hazardous materials regulations. In this research, ultrasonic spray coatings of aqueous polymer resin were studied to fabricate thin insulating layer (${\sim}{\mu}m$) on the rectangular copper wire. It needs to have appropriate wettability between resin and substrate during the ultrasonic spray coating process to coat aqueous polymer uniformly. Furthermore, stabilities of coating solution and fabricating process are required to form thin insulating layer on the substrate. In here, physical characteristics such as viscosity of 6 types of commercial polymer dispersions and emersions were analyzed to confirm compatibility for ultrasonic spray coating process. These resins were dissolved in isopropyl alcohol, used for true solvent, and were diluted with ethanol, utilized for diluent. Also, solubilities, dispersion characteristics, and viscosities of these diluted polymer resin solutions were confirmed. Dispersion characteristic and viscosity of coating solution affects jetting of ultrasonic spray coating and these jetting characteristics influence morphologies of insulating layer. In conclusion, we have known that aqueous polymer solution should have outstanding dispersion characteristic and certain range of viscosity to fabricate thin polymer insulating layer uniformly with ultrasonic spray coating.

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Propagation characteristics of ultrasonic guided waves in tram rails

  • Sun, Kui;Chen, Hua-peng;Feng, Qingsong;Lei, Xiaoyan
    • Structural Engineering and Mechanics
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    • 제75권4호
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    • pp.435-444
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    • 2020
  • Ultrasonic guided wave testing is a very promising non-destructive testing method for rails, which is of great significance for ensuring the safe operation of railways. On the basis of the semi-analytical finite element (SAFE) method, a analytical model of 59R2 grooved rail was proposed, which is commonly used in the ballastless track of modern tram. The dispersion curves of ultrasonic guided waves in free rail and supported rail were obtained. Sensitivity analysis was then undertaken to evaluate the effect of rail elastic modulus on the phase velocity and group velocity dispersion curves of ultrasonic guided waves. The optimal guided wave mode, optimal excitation point and excitation direction suitable for detecting rail integrity were identified by analyzing the frequency, number of modes, and mode shapes. A sinusoidal signal modulated by a Hanning window with a center frequency of 25 kHz was used as the excitation source, and the propagation characteristics of high-frequency ultrasonic guided waves in the rail were obtained. The results show that the rail pad has a relatively little influence on the dispersion curves of ultrasonic guided waves in the high frequency band, and has a relatively large influence on the dispersion curves of ultrasonic guided waves in the low frequency band below 4 kHz. The rail elastic modulus has significant influence on the phase velocity in the high frequency band, while the group velocity is greatly affected by the rail elastic modulus in the low frequency band.