• 제목/요약/키워드: Ultrafine Grain

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이종 알루미늄의 ARB공정에 의한 초미세립 복합알루미늄합금판재의 제조 및 평가 (Fabrication and Estimation of an Ultrafine Grained Complex Aluminum Alloy Sheet by the ARB Process Using Dissimilar Aluminum Alloys)

  • 이성희;강창석
    • 대한금속재료학회지
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    • 제49권11호
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    • pp.893-899
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    • 2011
  • Fabrication of a complex aluminum alloy by the ARB process using dissimilar aluminum alloys has been carried out. Two-layer stack ARB was performed for up to six cycles at ambient temperature without a lubricant according to the conventional procedure. Dissimilar aluminum sheets of AA1050 and AA5052 with thickness of 1 mm were degreased and wire-brushed for the ARB process. The sheets were then stacked together and rolled to 50% reduction such that the thickness became 1 mm again. The sheet was then cut into two pieces of identical length and the same procedure was repeated for up to six cycles. A sound complex aluminum alloy sheet was successfully fabricated by the ARB process. The tensile strength increased as the number of ARB cycles was increased, reaching 298 MPa after 5 cycles, which is about 2.2 times that of the initial material. The average grain size was $24{\mu}m$ after 1 cycle, and became $1.8{\mu}m$ after 6 cycles.

IF-Steel의 ECAP 공정 중 채널 상태와 온도에 따른 마찰효과 (Effect of friction different channel conditions and temperatures during ECAP)

  • 류원선;서민홍;김형섭;백승철
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2003년도 추계학술대회논문집
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    • pp.179-182
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    • 2003
  • Equal channel angular pressing (ECAP) provides an efficient procedure for introducing an ultrafine grain size into a material. In this study, ECAP were conducted on IF-steel to investigate the effect of friction and processing temperatures on the deformation characteristics of the samples. Due to the blocking effect of the previously pressed samples residing in the exit channel, the shear pattern (especially on the bottom region) changes.

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저탄소강의 초기 미세조직에 따른 기계적 성질과 시멘타이트거동 (Effect of Prior Microstructures on the Behavior of Cementite and Mechanical Properties in Low Carbon Steels)

  • 이종철;강의구;이중원;오창석;김성준;남원종
    • 소성∙가공
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    • 제18권6호
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    • pp.471-475
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    • 2009
  • The effect of prior microstructures on mechanical properties in low carbon steels were examined by comparing the behavior of cementite and mechanical properties of cryo-rolled and subsequently annealed steels. Prior microstructures consisted of ferrite + pearlite, banite or martensite. Steels, consisting of bainitic microstructure, exhibited the better combination of strength - ductility than steels with other prior microstructures, such as ferrite + pearlite and martensite.

Hot Pressing에 의한 $Si_3N_4-SiC$ 나노복합체의 제조 (Fabrication of $Si_3N_4-SiC$ Nanocomposites by Hot Pressing)

  • 김성현;김인술;박홍채;오기동
    • 한국세라믹학회지
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    • 제31권9호
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    • pp.1021-1029
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    • 1994
  • SiC ultrafine particles of 1, 10, 20 and 30 vol% were dispersed in $\alpha$-Si3N4 matrix and hot-pressed under the condition of 30 MPa at 1800 and 190$0^{\circ}C$ respectively. Physical, mechanical properties and microstructures of sintered Si3N4-SiC nanocomposites were investigated. Flexural strength and density of Si3N4-10 vol% SiC nanocomposites hot-pressed at 190$0^{\circ}C$ represented the 1002 MPa and 97.9%T.D respectively, and it was confirmed as a remarkable improvement of 67% compared to Si3N4 monolith. Fracture toughness was shown as 7.2 MPa.m1/2 when the same composition was hot pressed at 180$0^{\circ}C$. This effect was supposed to be due to the improvement of microstructure by the adequate suppression of the excessive growth of Si3N4 grain with SiC nano-particles.

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MAGNETIC PROPERTIES OF NANOCRYSTALLINE (Fe,Co)-B-Al-M (M=Nb/Mo/Ta) ALLOYS

  • Kang, D.B.;Cho, W.S.;Kim, T.K.;Cho, Y.S.
    • 한국자기학회지
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    • 제5권5호
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    • pp.483-486
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    • 1995
  • Soft magnetic properties of Fe-based (Fe,Co)-B-Al-M (M=Nb, Mo or Ta) nanocrystalline alloy have been investigated. The alloy obtained directly form the rapid solidification process. Microstructure of the alloy is a mixtu re of ultrafine bcc Fe(Co) nanocrystallines and a small amount of retained amorphous phase. Heat treatment of as-prepared alloys improves soft magnetic properties in high frequency range. ${(Fe_{.85}Co_{.15})}_{70}B_{18}Al_{10}Ta_{6}$ alloy alloy annealed at $500^{\circ}C$ for 1 h shows the most improved soth magnetic properties among the alloy examined. Average grain size of the nanocystalline is about 10 nm.

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6층겹침ARB공정에 의해 강소성가공된 극저탄소IF강의 어닐링에 따른 미세조직 변화 (Microstructural Evolution with Annealing of Ultralow Carbon IF Steel Severely Deformed by Six-Layer Stack ARB Process)

  • 이성희
    • 한국재료학회지
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    • 제22권8호
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    • pp.403-408
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    • 2012
  • A sample of ultra low carbon IF steel was processed by six-layer stack accumulative roll-bonding (ARB) and annealed. The ARB was conducted at ambient temperature after deforming the as-received material to a thickness of 0.5 mm by 50% cold rolling. The ARB was performed for a six-layer stacked, i.e. a 3 mm thick sheet, up to 3 cycles (an equivalent strain of ~7.0). In each ARB cycle, the stacked sheets were, first, deformed to 1.5 mm thickness by 50% rolling and then reduced to 0.5 mm thickness, as the starting thickness, by multi-pass rolling without lubrication. The specimen after 3 cycles was then annealed for 0.5 h at various temperatures ranging from 673 to 973 K. The microstructural evolution with the annealing temperature for the 3-cycle ARB processed IF steel was investigated in detail by transmission electron microscopy observation. The ARB processed IF steel exhibited mainly a dislocation cell lamella structure with relatively high dislocation density in which the subgrains were partially observed. The selected area diffraction (SAD) patterns suggested that the misorientation between neighboring cells or subgrains was very small. The thickness of the grains increased in a gradual way up to 873 K, but above 898 K it increased drastically. As a result, the grains came to have an equiaxed morphology at 898 K, in which the width and the thickness of the grains were almost identical. The grain growth occurred actively at temperatures above 923 K.

Effect of stress-strain curve changing with equal channel angular pressing on ultimate strength of ship hull stiffened panels

  • Sekban, Dursun Murat;Olmez, Hasan
    • Structural Engineering and Mechanics
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    • 제78권4호
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    • pp.473-484
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    • 2021
  • Similar to other structures, ultimate strength values showing the maximum load that the structure can resist without damaging has great importance on ships. Therefore, increasing the ultimate strength values will be an important benefit for the structure. Low carbon steels used in ships due to their low cost and good weldability. Improving the ultimate strength values without interfering with the chemical composition to prevent of the weldability properties of these steels would be very beneficial for ships. Grain refinement via severe plastic deformation (SPD) is an essential strengthening mechanism without changing the chemical composition of metallic materials. Among SPD methods, equal channel angular pressing (ECAP) is one of the most commonly used one due to its capacity for achieving bulk ultrafine-grained (UFG) materials. When the literature is examined, it is seen that there is no study about ultimate strength calculation in ships after ECAP. Therefore, the mean purpose of this study is to apply ECAP to a shipbuilding low carbon steel to be able to achieve mechanical properties and investigate the alteration of ship hull girder grillage system's ultimate strength via finite element analysis approach. A fine-grained (FG) microstructure with a mean grain size of 6 ㎛ (initial grain size was 25 ㎛) was after ECAP. This microstructural evolution brought about a considerable increase in strength values. Both yield and tensile strength values increased from 280 MPa and 425 MPa to about 420 MPa and 785 MPa, respectively. This improvement in the strength values reflected a finite element method to determine the ultimate strength of ship hull girder grillage system. As a result of calculations, it was reached significantly higher ultimate strength values (237,876 MPa) compared the non-processed situation (192,986 MPa) on ship hull girder grillage system.

Fe-Al-Nb-B-(Cu)계 초미세결정합금의 자기적 특성 (Magnetic Properties of Ultrafine grained Fe-Al-Nb-B-(Cu) Alloys.)

  • 박진영;서수정;김규진;김광윤;노태환
    • 한국자기학회지
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    • 제6권4호
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    • pp.218-224
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    • 1996
  • 새로운 고성능 자심용 연자성 합금을 개발하기 위해, 급냉응고 방식에 의해 제조된 $Fe_{83-x}Al_{x}Nb_{5}B_{12}(X=1~5at%)$ 합금의 결정화거동 및 자기적 특성을 조사하였다. 3at% Al의 $Fe_{80}Al_{3}Nb_{5}B_{12}$ 합금이 조사된 Fe-Al-Nb-B계 합금중에서 가장 우수한 연자기 특성을 가지며, 이때 미세한 $\alpha-Fe$상 결정립 조직을 가지는 것으로 판명되었다. 또, 이 조성의 합금에 1 at%의 Cu를 첨가하면, 약 6~7 nm정도의 크기를 가지는 극히 미세한 결정립의 $\alpha-Fe$ 상조직이 얻어졌으며 이에 따라 대단히 현저한 연자기 특성의 향상이 실현되었다. 이때 초미세 결정구조 $Fe_{79}Al_{3}Nb_{5}B_{12}Cu_{1}$ 합금의 자기적 특성은 다음과 같다 : ${\mu}_{eff}(1\;kHz)=26,000,\;B_{10}=1.45\;T,\;H_{c}=25\;mOe,\;P_{c}(100\;kHz,\;0.2\;T)=55\;W/kg$.

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고압비틀림 공정을 통한 급속응고 MgZn4.3Y0.7 합금 분말의 치밀화 및 기계적 거동 (Consolidation and Mechanical Behavior of Gas Atomized MgZn4.3Y0.7 Alloy Powders using High Pressure Torsion)

  • 윤은유;채홍준;김택수;이종수;김형섭
    • 한국분말재료학회지
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    • 제17권3호
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    • pp.190-196
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    • 2010
  • In this paper, rapid solidified Mg-4.3Zn-0.7Y (at.%) alloy powders were prepared using an inert gas atomizer, followed by a severe plastic deformation technique of high pressure torsion (HPT) for consolidation of the powders. The gas atomized powders were almost spherical in shape, and grain size was as fine as less than $5\;{\mu}m$ due to rapid solidification. Plastic deformation responses during HPT were simulated using the finite element method, which shows in good agreement with the analytical solutions of a strain expression in torsion. Varying the HPT processing temperature from ambient to 473 K, the behavior of powder consolidation, matrix microstructural evolution and mechanical properties of the compacts was investigated. The gas atomized powders were deformed plastically as well as fully densified, resulting in effective grain size refinements and enhanced microhardness values.

ECAP공법으로 제조된 무산소동의 미세조직 및 기계적 성질 이방성에 대한 고찰 (A Study on the Microstructure and Anisotropic Mechanical Properties of Oxygen-Free Copper Fabricated by Equal Channel Angular Pressing)

  • 이재근;홍영곤;김형섭;박성혁
    • 한국군사과학기술학회지
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    • 제22권4호
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    • pp.492-500
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    • 2019
  • Equal channel angular pressing(ECAP) is a severe plastic deformation technique capable of introducing large shear strain in bulk metal materials. However, if an ECAPed material has an inhomogeneous microstructure and anisotropic mechanical properties, this material is difficult to apply as structural components subjected to multi-axial stress during use. In this study, extruded oxygen-free copper(OFC) rods with a large diameter of 42 mm are extruded through ECAP by route Bc up to 12 passes. The variations in the microstructure, hardness, tensile properties, and microstructural and mechanical homogeneity of the ECAPed samples are systematically analyzed. High-strength OFC rods with a homogeneous and equiaxed-ultrafine grain structure are obtained by the repeated application of ECAP up to 8 and 12 passes. ECAPed samples with 4 and 8 passes exhibit much smaller differences in terms of the average grain sizes on the cross-sectional area and the tensile strengths along the axial and circumferential directions, as compared to the samples with 1 and 2 passes. Therefore, it is considered that the OFC materials, which are fabricated via the ECAP process with pass numbers of a multiple of 4, are suitable to be applied as high-strength structural parts used under multi-axial stress conditions.