• Title/Summary/Keyword: UV detection

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On a Detection of V-UV Segments of Speech Spectrum for the MBE Coding (MBE 부호화용 스펙트럼 V-UV 구간 검출에 관한 연구)

  • 김을제
    • Proceedings of the Acoustical Society of Korea Conference
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    • 1992.06a
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    • pp.43-48
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    • 1992
  • In the area of speech vocoder systems, the MBE vocoder allows the high quality and low bit rate. In the MBE parameters detection, the dicision methods of V/UV region proposed until now are dependent highly to the other parameters, fundamental frequency and formant information. In this paper, thus, we propose a new V/UV detection method that uses a zero-crossing rate of flatten harmonices spectrum. This method can reduce the influences of the other parameters for the V/UV regions detection.

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Simultaneous determination of betaine and choline using derivatization by HPLC with UV detection (HPLC-UV검출방법으로 유도체화를 통한 비테인과 콜린의 동시분석)

  • Rhee, Insook;Paeng, Ki-Jung
    • Analytical Science and Technology
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    • v.28 no.2
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    • pp.112-116
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    • 2015
  • Extraction of quaternary ammonium compounds (choline and betaine) from plant samples (spinach) using ion exchange resin (AG1, OH form) is a very simple and inexpensive approach. However, it is very hard to determine amounts of choline and betaine simultaneously using high-performance liquid chromatography-ultraviolet (HPLC-UV) detection. Unlike choline, betaine has low molar absorptivity in UV-visible (UV-Vis) region, which makes it difficult to carry out UV-Vis detection of betaine. The mixture of quaternary ammonium compounds (choline and betaine) was derivatized using 2-bromo acetophenone as a derivatizing agent. As a result, choline did not react with the derivatizing agent, whereas betaine formed a betaine derivative. This betaine derivative exhibited detectable UV absorption with baseline separation between choline and the betaine derivative. Thus, with this method, choline and betaine can be determined simultaneously by using the HPLCUV method through one-step derivatization, which is an easy, sensitive, and reliable method.

Design and Analysis of Flame Signal Detection with the Combination of UV/IR Sensors (UV/IR센서 결합에 의한 불꽃 영상검출의 설계 및 분석)

  • Kang, Daeseok;Kim, Eunchong;Moon, Piljae;Sin, Wonho;Kang, Min-goo
    • Journal of Internet Computing and Services
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    • v.14 no.2
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    • pp.45-51
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    • 2013
  • In this paper, the combination of ultraviolet and infrared sensors based design for flame signal detection algorithms was proposed with the application of light-wavelength from burning. And, the performance result of image detection was compared by an ultraviolet sensor, an infrared sensor, and the proposed dual-mode sensors(combination of ultraviolet and infrared sensors).

Influence of Dust Environment on the Detection Capability of Ultraviolet Flame Detector (UV 화염감지기의 감지성능에 대한 분진분위기의 영향)

  • Kim Hong;Hu Rui
    • Journal of the Korean Institute of Gas
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    • v.1 no.1
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    • pp.113-119
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    • 1997
  • The detection capability of UV flame detector in dust environment would be impaired. In this study, an experiment was conducted, in an effort to further understand the behavior of UV flame detector and to evaluate its detection capability in industry dust environment. Detergent powder, coal powder and dry extinguishing agent were selected as dust sources. Flaming sources include propane and gasoline flame. Experiment results indicate that dust can cause remarkable attenuation of UV flame radiation. The concentration of dust and the length of air layer where dust dispersed determine the reduction of radiation intensity. On the other hand, the attenuation of UV radiation also depends on the chemical and Physical properties of dust.

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Determination of trace bromate in various water samples by direct-injection ion chromatography and UV/Visible detection using post-column reaction with triiodide

  • Kim, Jungrae;Sul, Hyewon;Song, Jung-Min;Kim, Geon-Yoon;Kang, Chang-Hee
    • Analytical Science and Technology
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    • v.33 no.1
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    • pp.42-48
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    • 2020
  • Bromate is a disinfection by-product generated mainly from the oxidation of bromide during the ozonation and disinfection process in order to remove pathogenic microorganism of drinking water, and classified as a possible human carcinogen by International Agency for Research of Cancer (IARC) and World Health Organization (WHO). For the purpose of determining the trace level concentration of bromate, several sensitive techniques are applied mostly based on suppressed conductivity detection and UV/Visible detection after postcolumn reaction (PCR). In this study, the suppressed conductivity detection method and the PCR-UV/Visible detection method through the triiodide reaction were compared to analyze the trace bromate in water samples and estimated for the availability of these analytical methods. In addtion, the state-of-the-art techniques was applied for the determination of trace level bromate in various water matrices, i.e., soft drinking water, hard drinking water, mineral water, swimming pool water, and raw water. In comparison of two analytical methods, it was found that the conductivity detection had the suitable advantage to simultaneously analyze bromate and inorganic anions, however, the bromate might not be precisely quantified due to the matrix effect especially by chloride ion. On the other hand, the trace bromate was analyzed effectively by the method of PCR-UV/Visible detection through triiodide reaction to satisfactorily minimize the matrix interference of chloride ion in various water samples, showing the good linearity and reproducibility. Furthermore, the method detection limit (MDL) and recovery were 0.161 ㎍/L and 101.0-108.1 %, respectively, with a better availability compared to conductivity detection.

A Studies on Indirect Photometric Detection of Aliphatic Compounds by High-Performance Liquid Chromatography (고성능 액체 크로마토그래피에 의한 지방족 화합물의 간접 분광광도 측정에 관한 연구)

  • Sam-Woo Kang;Jeon-Tag Kang
    • Journal of the Korean Chemical Society
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    • v.33 no.4
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    • pp.406-412
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    • 1989
  • Indirect photometric detection of aliphatic compounds such as alcohols, ketones and esters was investigated in high-performance liquid chromatography, These samples possessing nonchromophore or weak chromophore could be indirectly detected by a UV detector with addition of UV absorbing, p-chlorophenol or p-nitrophenol in mobile phase as detection reagent, and submicrogram detection limits were achieved. Some mixtures of samples were also able to be separated and quantitated with good resolution and comparatively high sensitivity under optimum conditions.

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A Study of Liquid Chromatographic Detection Method for Thiocarbamates by Using Photochemical Reaction (광화학 반응을 이용한 티오카바메이트류의 액체 크로마토그래피 검출법에 관한 연구)

  • Dai Woon Lee;Young Hun Park;Yong Wook Choi
    • Journal of the Korean Chemical Society
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    • v.37 no.4
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    • pp.453-461
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    • 1993
  • Detection method was developed using a simply designed photochemical reactor made of teflon coil and low pressure mercury lamp. This method of UV photolysis of analytes followed by UV, fluorescence and electrochemical detection was found to be useful for four thiocarbamates. Analytes eluting from the column are irradiated with a high flux of 254 nm UV light, so that they change to either fluorescent active forms or highly electrochemically sensitive products. Appling this technique to the UV detection, thiocarbamates were converted into long wavelength absorbing products upon UV irradiation. In fluorescence detector four thiocarbamates are not detected at nonirradiated condition but fluorescence signals of MPTC, CPTC photolysates are appeared after irradiation with UV light. The electrochemical detection for the determination of thiocarbamates was enhanced up to 5∼20 fold signal after UV irradiation, compared to that of the nonirradiated. The detection limit of thiocarbamates on electrochemical detector was 13.3∼0.02 ng under pH 7.0, ionic strength $0.5{\times}10^{-2}$ M, phosphate buffer solution. Adducts produced by reaction of photolysates and OPA-MERC in the reaction coil were monitored at 425 nm with fluorescence detector, and one of the photolysates was primary amine.

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Fast Human Detection Method in Range Data using Adaptive UV-histogram and Template Matching (적응적 UV-histogram과 템플릿 매칭을 이용한 거리 영상에서의 고속 인간 검출 방법)

  • Yoon, Bumsik;Kim, Whoi-Yul
    • Journal of the Institute of Electronics and Information Engineers
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    • v.51 no.9
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    • pp.119-128
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    • 2014
  • In this paper, a fast human detection method using adaptive UV-histogram and template matching is proposed. The proposed method improves the detection rate in the scene of complex environment. The method firstly generates U-histogram to extract human candidates and adaptively generates V-histogram for each labled U-histogram, thus it could extract humans correctly, which was impossible in the previous method. The method tries to match the human candidates with the adaptively sized omega shape template to the focal length and distance in order to improve the detection accuracy. It also detects false positives by rematching the template with accumulated foreground images and hence is robust to the occlusion. Experimental results showed that the proposed method has superior performance to the Bae's method in the complex environment with about 15% improvement in precision and 80% in recall and has 20 times faster processing time than Xia's method.

The UV LED Bar Optimal Design with Human Detection and Control Function (인체 감지 제어 기능을 갖는 UV LED Bar의 최적 설계)

  • Kim, Chang-Sun;Lee, Jae-Hak;Goh, Young-Jin
    • The Journal of the Korea institute of electronic communication sciences
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    • v.12 no.6
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    • pp.1219-1226
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    • 2017
  • In this paper, it is performed the optimal design of the UV LED bar which can be used variously. The UV LED Bar emits ultraviolet rays, so it is important to emit ultraviolet rays constantly for the purpose of use. In order to emit a certain amount of ultraviolet rays as ever, the ultraviolet ray emission should be driven by a constant current source within the operable input voltage range. And also the heat dissipation is particularly important because of the long ultraviolet emission retention time due to the UV utilization characteristics. In addition, since human body protection is essential, the algorithm is configured to operate according to human body detection using distance sensor and Bluetooth. Three 365nm UV LEDs were used in series to emit ultraviolet UVA, operating at the constant current of 500mA with an efficiency of 87.5% and a power consumption of 6.006W. The ultraviolet radiation dose was measured at $5.35mW/cm^2$ at the distance of 10 cm when measured by the Lutron ultraviolet measuring instruments.

Determination of Aflatoxins Using High-Performance Liquid Chromatography and Fluorescence or UV Absorbence Detection (HPLC에 의한 aflatoxin 분석법에 관한 연구 형광 및 자외선 흡광 검출의 비교)

  • 김종규;강회양;민경진
    • Journal of Environmental Health Sciences
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    • v.22 no.1
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    • pp.36-44
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    • 1996
  • A comparison was made of two detection methods(UV absorbence detection and fluorescence detection with pre-column derivatization, with trifluoroacetic acid) coupled with HPLC for the simultaneous determination of aflatoxin $B_1, B_2, G_1$ and $G_2$. A good separation of the four aflatoxins was achieved on a reversed-phase $C_{18}$ column (30 cm x 3.9 mm) with methanol-acetonitrile-water(20+20+60) for absorbence detection or acetonitrile-water(25+75) for fluorescence detection at the flow rate of 1.0 ml/min. The calibration graphs were linear over the ranges 100 ppb-1 ppm for $B_1/G_1$ and 30~300 ppb for $B_2/G_1$ with absorbence detection, and 1~500 ppb for $B_1/G_1$ and 0.3~150 ppb for $B_2/G_2$ with fluorescence detection. The correlation coefficients were greater than 0.94 and 0.99 for absorbance detection and for fluorescence detection, respectively. The detection limit was 100 ng for $B_1/G_1$ and 30 ng for $B_2/G_2$ with absorbence detection, and 1 ng for $B_1/G_1$ and 0.3 ng for $B_2/G_2$ with fluorescence detection. Recovery rates of aflatoxin $B_1, B_2, G_1$ and $G_2$ added to yeast-extract sucrose broth medium were 66.6%, 59.4%, 67.5% and 59.2%, respectively, for absorbence detection and 82.9%, 71.5%, 80.0% and 69.3%, respectively, for fluorescence detection. The four aflatoxins in culture medium were quantitatively detected by the two methods. The aflatoxins in the rice sample were not detected the absorbence detection method, but were below 10 ppb using the fluorescence detection method. Analysis of aflatoxins by both the absorbence and fluorescence methods coupled with HPLC showed acceptable linearity and good recovery. The absorbence detection was less timeconsuming and safer for treatment. The fluorescence detection was more elective and sensitive though elevated $B_1$ and $G_1$ contents were determined from the TFA-induced conversion of $B_1$ to $B_{2a}$ and $G_1$ to $G_{2a}$.

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